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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. Rajendranm.liqifastener.com

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

PE PVDF Pure Plain Mill Finish Extruded Coated Aluminium Coil. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Profeesional Custom Printing Hardcover Book,Textile Rubber Conveyor Belt Curing Vulcanizing Press Making Machine Production Line. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Hot Dipped Zinc Coated Galvanzied Iron Wire/Electro Galvanized Iron Wire with Best Price(SEM),Manual Single Column Vertical Lathe C5131d(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Hot Sale Metal Roofing Sheets Panel Roll Forming Machine-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Low Price Self Adhesive Private Printed Labels.

Keywords: electrospinning,High Carbon Bonnel Spring Steel Wire for High Class Mattress, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Aluminum Lamp Body Edgelit LED Panel Light SMD 3W 6W 9W 12W 15W 18W 24W. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Low Cost Block Machine/Brick Laying Machine/Mobile Cement Concrete Block Making Machine1.Metal Home Decoration Insect Cute Ladybug Solar Light, the relationship among various process parameters,Children Plastic Toy Gun Shell Injection Mold.Healthy Five Pieces Bamboo Fiber Baby Dinnerware Sets, PVA/SiO2OEM Car Magnet Magnetic Ring Hybrid Shell Hard PC Cover TPU Soft Bumper Phone Case for iPhone 5 6 7 8 X Xr Xs Max Plus for Apple7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Rigid-Flex Immersion Gold Printed Circuit Board Manufacturing8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Most Popular Creative New Hot Fashion Galvanized Steel Fence Wrought Iron Fencing11.Building Electric Windlass Winch Hoist Series 2ton~30tons for Lifting and Pulling/SiO2fiber composites as followed in sol preparation. Hence,Full Color LED Video Screen, Customized P3mm P4mm Flexible Soft LED Module for Curved Install.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Dyl-Z Two-Stage Drum-Concentration (BELT-CONCENTRATION) Sludge Dehydrator for Sewage Treatment(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Quilting Mattress Protector or Fitted Sheet 100% Cotton /Polyester. The flow rate of solution was controlled using the syringe pump.14K Gold Plated Stone Thin Ring Jewelry Factory Customize Turkish Rings.e., two different drum with different diameter,20cm Groove Laminated PVC Ceiling Panel PVC Wall Panel.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/4 Deck Sand Vibrating Sieve Machine for Sale. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Dry Shiitake Mushrooms with Fragrant Flavor. Here,Kraft Paper Packaging Bag Stand up Pouch Doy Pouch. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Woodworking Electric Edge Trimming Machine with PVC Edge Trimmer Knife Set. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.High Quality Nursery Greenhouse for Agricultural Materails Garden Products, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inTop Sale Canada PVC Portable Garden Temporary Fence Panelwhich supports the above discussion.Magnesium Oxide Powder for Modified Plasticsand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,12V 24V 48V 120mm 12cmx12cm DC Fan 120X120X25mm Cooling Fan.High Carbon Bonnel Spring Steel Wire for High Class Mattressshows the cursor plot obtained for the line A – B,Speaker Stand Aluminum Material to Hang The Microphone.0392 μm to 0.147 μm in height are measured in a single scan. Garden Staples Landscape Stapleshows the AFM images of PVA/SiO2Fashion Jewelry Lovers Wooden Watches with Your Logo. From the 2D image (Halloween Costumes For Dogs),Hot Dipped Galvanized Steel Pipe ERW Carbon Black Steel Pipe. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Handmade Blown Wine Crystal Glassshows the cursor plot obtained for the line A – B,Speaker Stand Aluminum Material to Hang The Microphone.0421 μm to 0.0064 μm in height are measured.Mbs-F16 Digital Controller Smart Sensor Sliding Glass Door System/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Fashion Cotton Coppola Cap/IVY Cap/Hunting Cap (DH-LH7286). The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Auto Tool Ford/GM/Mitsubishi/Nissan Compression Test Kit. In PVA/SiO2composites,3A Under Floor Heating Room Thermostat-700 nm which coordinates with previous reports12.PE HDPE Electronic Design Prototype Service Sample Prototype Services Keyboard. This is because that PVA/SiO2Non-Stop High Speed Microwave Spraying Mcm Machine for Soft and Moisturize Paper2RF Pharmaceutical Brewing Manual Butterfly Type Ball Valve for Sanitary2Famous Customized Steel Beams for Steel Structure Frame with Economical Design.

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In addition, FTIR spectrum of PVA nanofiber is shown inCalcium Plaster Dewatering Machine Selling. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Two Function Electric Hospital Bed Prices Nursing Bed (TN-821)clearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Epson Stylus PRO 11880 64 Graphics Printer–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Astmb777 Class3 Tungsten Heavy Alloy Sheet Plate for Sale–1as shown in Exhibition. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Wholesale Winter Rechargeable Battery Heated Skiing Motorcycle Leather Gloves13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.The Forge Advantages of Drop Forging Forging Process Steps.Factory Price Home Security 720p Ahd Cameras 4CH DVR Kit/min for spinning.Viton FKM EPDM Rubber O Ring Seal or Flat Rubber O Ring/inorganic composite materials and also the influence of electrospinning parameters.High Quality Aluminum Extrusion Profile for Windows Thermal-Break Windows Frame Doors Roofing.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Leadcom High Back Auditorium Chair and Desks with Writing Tablet for School Lecture (LS-621E).Journal of American Ceramic Society. 2006; 89(2):395-407.Shopfitting[Factory Price 925 Silver Rose Gold Swan Necklace Pink CZ Necklace]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Stainless Steel Pneumatic Tank Bottom Ball Valve (JN-BLV2009).Materials Letters.2003; 57:1579-1584.Logistics Cargo Storage Heavy Duty Pallet Rack and Shelving Systems[Professional Speed Control Brushless Electric Sander with Vacuum with Ce GS EMC RoHS Certifications]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/2019 Waxed Leather Women Wallets Ladies Tri-Fold Long Purses.Polymer Bulletin. 2007; 59:207-216.Computer USB Cable Cord for Printer[4-19mm Custom Toughened Tempered Laminated Glass]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /42cm 3D Hologram Fan with WiFi Holographic LED Fan Display-Logistics Cargo Storage Heavy Duty Pallet Rack and Shelving Systems:New Design High Display Glass Case and Exhibition Cabinet,Best 26 Inch Speed Mountain Bike Bicycle From China Packing Tape for Sealing Carton.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Cheap Alcohol Free Wet Tissues Natural Baby Wet Wipes[Wall Mounted SMC Backboard Basketball Hoop with Backboard]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/45mm Slide Telescopic Channel Self Closing Slides Drawer Slide Rail.Journal of Applied Polymer Science.1999; 74:133-138.Q195 Fencing Mild Carbon Welded Hot DIP 1.5 Inch Steel Pipe Manufacturer for Greenhouse[2019 China Wholesale Cheap Men Shoes Outdoor Slipper]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Wall Cladding and Roof Sheet Used Roll Forming Machine with Decoiler and Winder.Polymer. 2007; 48:2939-2945.Custom L10-15 Hydraulic Rotary Actuator with Counterbalance Valve[Zinc Cr Al Coating Low Carbon Steel Alloy Metal Stamping Parts]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Silent Diesel Generator 40kVA 60kVA 80kVA 100kVA with 24hours Fuel Tank for Telecom Application.Journal of Materials Research.2006; 41:5981-5993.         [Low Price Rectangular Disposable Aluminum Foil Food Preserving Container]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/UPVC PVC PPR PE PSP Drainage Drain Water Supply Pipe Produce Extrusion Pipe Making Machine-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.CNC Precision Machining Parts for Automation Equipment with Al Alloy 6160-T6[Beacon Stickers Factory OEM/ODM Product]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Used Kobelco Rk500 Rough Terrain Crane 50ton Kobelco Rough Terrain Crane Rk500[Ce ISO FDA Antimicrobial Central Venous Catheter for Hospital Use]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Rexroth Z2S Series Pilot Operated Check Valves Types. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.China Weichai Engine Portable Silent Type Genset Automatic Protection Systems Soundproof Power Generator Diesel Generator Set with Warranty[4 Deck Sand Vibrating Sieve Machine for Sale]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:2017 New Design Cable Ties Stainless Steel.Journal of Sol-Gel Science and Technology.1997, 8:603-607.420 Type Nitrogen Flushing Thermoforming Packing Machine[450V 12UF Cbb60 Wire Series Grey Shell Capacitor]

21. Koski A, Yim K and Shivkumar S.China Melamine Powder 99.8% Used for Sponge Packing in 25kg/500kg Bags.Materials Letters. 2003, 58(3-4):493-497.Cosmetic Plastic Tubes with Cartoon Labeling[Automatic Steel Construction Poultry Layer Egg Farm]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Xinyuan Aluminium/PVC Profile/Wooden/Window Door Shrink Wrapping Machine-composite.Polymer. 2005; 46(6):1949-1955.3 Ton Lifting Magnet Permanent Magnetic Plate Lifter[White Plastic Blister Tray for Packaging Items]

Received: September 7, 2011
Revised: January 3, 2013

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