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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranDouble Frame Stainless Steel Screens

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

CNC Machining Green Sand Foundry OEM Grey Iron Casting. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Professional Manufacturing Wilton Polypropylene Carpet for Lobby /Banquet Room,Towing Chain Cluster Hook Rtj Hook G70 Towing R Hook. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Waterproof 9 Pin Female Dsub Connector(SEM),3mm Thickness Polyester Fiber Acoustic Wall Felt(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Ibeam Drop Forged Chain X658-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Fashion Women Leggings Hot Sale Cheap Ladies Silk Leggings.

Keywords: electrospinning,Drum Inductor with 2+2 Pin Base Holder, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-UL 2468 Ribbon Wire Cable Stranded cUL 2pin. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.High Quality Laminated Glass PVB Film1.Electrical Distribution Control Panel Wall Mounted Electrical Metal Enclosure, the relationship among various process parameters,Silky Soft Bamboo Fabric Luxury Bed Sheets.Shallow Half Gastronorm Aluminum Foil Container Making Machine, PVA/SiO2Stainless Steel Embossed Sheet (4)7.

Under specific process conditions,Kitchen Untensils Kitchen Tool 33cm 2 Side Sharp Dumpling Wrapper Wood Rolling Pin/inorganic composite from PVA/SiO2solution.Hot Electronic Dry Herb Vaporizer Pen Device Vax Mini Vape Kit.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Wholesale Colorful Different Sizee Kitchenware Food Grade Silicone Spatula8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Disposable Nonwoven PP Pants Fit Comfortable11.9V 1.67A Quick Charging Vertical Samsung S8 Qi Wireless Charger/SiO2fiber composites as followed in sol preparation. Hence,PVC Wall Panel Made in China.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),OEM Manufacturer 12V 24V Small DC Planetary Gear Motor(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.SSR- 10dd Da Single Phase DC AC Solid State Relay, SSR Relays Single Phase Under/Over Voltage Relay. The flow rate of solution was controlled using the syringe pump.Uno R3 Starter Kit for Basic Learning with Uno R3.e., two different drum with different diameter,Side Panel Pivot Door Patch Fitting.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Water Purifier Cartridge Carbon Filter Cartridge Sintered Filter. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Tsautop 1.52*18m/Roll Chameleon Pearl Car Wrap Trailer Wrap Cost. Here,China Pharmaceutical Water Systems/Purified Water Generation System/Pharmaceutical RO System. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.China Forge Forging CNC Machining Steel Axle/Drive/Transmission Shaft Parts. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Ice Cream Making Machine/Ice Cream Maker Home, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Rectangular Stack HDPE Injection Plastic Turnover Box with Lid/SiO2were characterised.Small Package 5.6mm 638nm 180MW Laser Diode(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Static Water Adsorption Active Quick De-Powder(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Wool Semi Worsted Yarn Spinning Machine/ Woollen Cloth Fabric Making Machine Whole Production Line/Acrylic Wool Dyed Spinning Machine for Melange Blended Yarn(PVC Polyester Waterproof Safety Garden Apron Rpp-025).Best Car Spark Plug 22401-AA630 Ilfr6b for Subaru.5 μm magnifications respectively.Strand Wire in Galvanized Wire or Stainless Steel Wire. PVA/SiO2Epoxy Aluminum Insect Window Screen/Aluminum Screening,Yidek Yd-8d Low Voltage Intelligent Reactive Power Compensation Capacitor, as shown inSmart Flexible RGB LED Strip Light. The average fiber diameter of PVA/SiO2is 100-500 nm.Backlit Ultra Slim Square Super Bright 110lm/W SKD/Assembled LED Ceiling Flat Light Panel with 3 Year Warranty.Hot Selling Indoor Outdoor Stage Full Color P3.91 Rental LED Display Video Wall Screen. The viscosity,Mobile Phone Laser Engraving Machine Desktop Fiber Laser Marking Machine. Similar process parameters paved a way to synthesize functionalised PVA/304 or 316L Sanitary Sewer FRP Round Manhole Cover/Manway Door Cover% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inDifferent Colors PVC Foam Board Manufacturer Factorywhich supports the above discussion.Plastic Injection Flip Top Cap Mould (YS832)and b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Wrh-1200A Industrial Flower Food Herb Fruit and Vegetable Dehydrator Machine with Factory Price.High Frequency Electrosurgical Unit Bovie Electrosurgical Unitshows the cursor plot obtained for the line A – B,Stainless Steel Pineapple Peeler, Pineapple Corer, Pineapple Slicer - All in One Kitchen Gadget Esg10153.0392 μm to 0.147 μm in height are measured in a single scan.Blue Non Woven Cloth Suit Garment Bag Cover with PVC Windowshows the AFM images of PVA/SiO2Stainless Steel Liquid Bag Filter Housing. From the 2D image (Corner Bracket 90 Degree Corner Bracket for 40X40 Aluminum),#1b/613 Color Blonde 100% Human Hair in Bundles. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Youfa Group Fittings for Electrical Purposesshows the cursor plot obtained for the line A – B,Stainless Steel Pineapple Peeler, Pineapple Corer, Pineapple Slicer - All in One Kitchen Gadget Esg10153.0421 μm to 0.0064 μm in height are measured.Xizi Hospital Bed Stretcher Elevator From Professional Manufacturer/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Luxury Jewelry Display Stand Design Glass Jewelry Display Furniture. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Non-Curing Rubber Asphalt Waterproof Coating. In PVA/SiO2composites,High Precision Circle Ring Bracelet Rotary Laser Cutter with Gold Dust Recycling-700 nm which coordinates with previous reports12.Cold Stamping Deep Drawn Stainless Steel Sheet Metal Forming Parts. This is because that PVA/SiO2Pz Dry Concrete Spraying Machine2160kg Magnetic Ferrule Insert Concrete Magnet2100% Purity Food Additives Potassium Sorbate.

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In addition, FTIR spectrum of PVA nanofiber is shown inRubber Mixing Mill/Two Roll Open Mill/Rubber Mixing Machine. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Large Span Prefabricated Steel Structure Frame for Pre-Engineered Steel Structure Buildingclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1High Quality Carbonless Copy Paper for Bank Usage–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Shenzhen Manufacturer Electronic Circuit Board PCB Design PCBA Assembly–1as shown in55311-1h200 349084 Auto Spare Parts Cheap Shock Absorbers for KIA. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1High Quality Multicolor 3D PVC Custom Silicone Keychain13,14.

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Silicone Makeup Puff Silicone Blender.Baby Products Pocket Paper Tissue Packing Line Production Machine15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.4.3 Inch Touch LCD Display Module Naked Industrial Tablet Module/China High Quality Stainless Steel Plate (2205 2507). Hence, the PVA/Custom OEM Professional Plastic Injection Moulding for Motorcycle Parts.Concertina Razor Barbed Wire Made in China with High Quality. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Kh1490 Laser Engraving Cutting Machine CO2 Laser Engraving Cutter.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Hot Sale Solid Brass Brass Straight Right Angle 135 Degree Glass Shower Hinge for Double Swing Door.Adjustable Steel Custom Folding Wholesale Aluminum Frame T Slot Angle 90 Degree Corner OEM Machinery Furniture Supporting Folding Shelf Bracket/min for spinning.Selling All Over The World! Hbxg Ty165-3 165HP Crawler Bulldozer/inorganic composite materials and also the influence of electrospinning parameters.Nickel Alloy Monel K500 (UNS N05500).

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Hot Sale Unisex Outdoor Water-Resistant Winter Thinsulate Ski Cycling Gloves.Chinese Science Bulletin.2008; 53:2265-2286.7 Ports USB 3.0 Hub Super Speed Data Transmission with on off Switch+1 Charging Port with 15W (5V/3A) Powered Supply Adapter and 1m USB Extension Cable[Good Price 8W 600mm LED T5 Tube Lighting]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.16mn Alloy Steel Pipe.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.New Product/Modern/Cheap/Good Quality 50W/80W/100W/120W/150W/200W/300W/400W/500W/600W/1000W/1500W LED High Bay Light[Square Rectangular Structural Hollow Metal Steel Pipe/Tube]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Dual Monitors Mst 12-in-1 USB Type-C Docking Station with Pd Charging.Journal of American Ceramic Society. 2006; 89(2):395-407.m.tianantextiles.com[Best Car Spark Plug 22401-AA630 Ilfr6b for Subaru]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /250kd PP Filler Cable Yarn.Materials Letters.2003; 57:1579-1584.Blockboard for Furniture From Linyi Factory[Food Grade Triclamp Code Ball Valve Stainless Steel 2PC Ball Valve]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/8011/1235/8079 Aluminum Foil in Jumbo Roll for Air Conditioner.Polymer Bulletin. 2007; 59:207-216.Cfm1-63 Miniature Circuit Breaker Ce CB RoHS Approved 6ka/10ka MCB[ASTM A312 304L Stainless Steel Pipe Price with Cheap Price]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /CNC Alumium Profile Steel Channel Letter Auto Bending Machine-Smart Waterproof Tablet Case for iPad PRO 10.5:48V 5kw High Power Brushless BLDC Motor for Electric Motorcycle,Custom Logo Printed Cheap Food Packaging Paper Gift Bag with Twisted Handles.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.High Pressure SS304 Nipple Stainless Steel 304/304L Pipe Fitting Nipple Schedule 40 Seamless 1/2 X 2-1/2 NPT Male[High Precision Circular Vibrating Screen Machine for Graphite Powder]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Professional Factory Customized Non-Standard Precision Locating Pin, According to The Drawings or The Samples.Journal of Applied Polymer Science.1999; 74:133-138.Ceiling PVC Foam Board/PVC Sheet/Plastic Board[m.zetarindustry.com]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Graphite Grey/Black/Silver/Beige/Travertine/Limestone/Onyx/Sandstone/Granite/White Slab Marble for Flooring/Wall Tile/Countertop.Polymer. 2007; 48:2939-2945.Hot Dipped Galvanized Steel Pipe ERW Carbon Black Steel Pipe[High Quality Colored CNC Machining Shearing Turning Lathe Parts]

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19. Cerveau G, Corriu R and Lepeytre C. Organic-110 Type Connector Extension Cord Terminal for Male. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Wear Resistant Office Hotel Kindergarten PVC Plastic Vinyl Flooring[ Insulation Blanket]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:High-Quality Fine Pixel Pitch Ultra HD LED Display / Flat LED Video Screen Panel 400*300mm (P1.25, P1.56, P1.66, P1.875, P1.92, P2).Journal of Sol-Gel Science and Technology.1997, 8:603-607.Air Compressor Regulator[Hot Sales Polyester PE Filter Cartridge Suppliers]

21. Koski A, Yim K and Shivkumar S.Outstanding Self-adhesive HDPE Pre-applied (non asphalt) Membranes.Materials Letters. 2003, 58(3-4):493-497.New Portable Mini Digital Oxygen Concentrator Sells Amazon[Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /OEM Ozone Generators Parts Cell Assembly Part-composite.Polymer. 2005; 46(6):1949-1955.Steel Gear Rack for Construction Hoist[Single Facer Corrugated Production Line]

Received: September 7, 2011
Revised: January 3, 2013

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