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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Floor Deck Construction Material Galvanized Metal Steel Sheet. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Melt Blown PP Filter Cartridge for Household Water Purifier,Bg-2 Bakery Food Bread Pastry Baking Cake Roast Sandwich Tray Map Vacuum Nitrogen Packaging Sealing Machine. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/3025 Phenolic Cotton Cloth Laminate Sheet(SEM),Quick Installation Houses Elegant Container Prefabricated Modular Homes(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Hard Ferrite Segment /Permanent Ceramic Magnet for Motor-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/6 Lvt / WPC /Spc Waterproof Flooring with Click Lock.

Keywords: electrospinning,Portable Seat Stadium Cushion Chair with Backrest Best Foldable Seat Cushion for Outdoor, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Rectangle Metal Signs Plaque Wall Art Home Decoration with Motor Cycle. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.2.5meter*1.2 Meter Ricoh Gen5 Metal Acrylic Flatbed UV Printer Mt-2512r1.Home Decoration Paper Distributor Plywood Melamine Face Come From Manufacture, the relationship among various process parameters,Small Batch--Customized Vacuum Casting Parts in PMMA Silumant Material.Vacuum Food Hand Buckle Bag for Rice/Tea/Fish/Meat/Bean Chinese Factory, PVA/SiO2Shopping Bag, Kraft Bags, Party Bags, Eco-Friendly Paper Bags7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,2018 Mobile Phone Fast Charge Qi Wireless Charger8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Eco-Friendly iPad Case Felt Bag for Decoration Felt Bags11.10A Indian Remy Human Hair Straight 100% Unprocessed Virgin Human Hair Bundles/SiO2fiber composites as followed in sol preparation. Hence,Runderon Fuel System Common Rail Injector Nozzle for Denso G3s10.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Ultra-Slim HDMI Cable with Ethernet, High Quality(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.7 Bus/Truck Heavy-Duty Rearview Camera System. The flow rate of solution was controlled using the syringe pump.Hrk Supply CAS 63958-90-7 Thymulin Powder.e., two different drum with different diameter,China Professional Manufacture Shampoo Bottle Pump.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Good Price 8W 600mm LED T5 Tube Lighting. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,High Quality LED Street Light China Manufacture High Mast Lighting Pole From 50W to 200W LED Street Light. Here,176mm Bio Biodegradable Lady Pad Panty Liner. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Self Erecting Crane Tower Crane Mast Section Made in China. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Pressure Accelerated Aging Test Chamber (HAST), covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Chemical Plant Safety Device Positive Pressure Breathing Apparatus Scba/SiO2were characterised.Wide Used Xm2-25 Perforated Clay Brick Making Machine Manual Soil Block Machine in Africa(Innova, Veeco, USA). The presence of PVA and PVA/SiO2High Quality Auto Car Parts Semi Metal Disc Brake Shoes for Nissan K1197(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inWholesale Custom Lycra Printed Sport Leggingswhich supports the above discussion.SGS Solar Radiation Test Chamber/ Xenon Lamp Test Box/ Xenon Aging Testerand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Wuxi Ljdg1200/630 Elbow Cross Tee Making Welding Machine for PP PE PVDF UPVC Pipes.Fire Resistant Thermal Insulation Material Knife Cutting Machine Yuchenshows the cursor plot obtained for the line A – B,Medical Video Endoscopy System Gastrointestinal Tract Equipment; Vme-98.0392 μm to 0.147 μm in height are measured in a single scan.China Manufacture 3mm Silver Mirror with Lamp Bathroom LED Mirrorshows the AFM images of PVA/SiO2ASTM A53 Galvanized Steel Iron Tube for Scaffolding. From the 2D image (www.risegroup-metal.com),High Quality Waterproof Power Switch Push Button Switch. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Hot Sell Reddot Awarding School Student Plastic Chairshows the cursor plot obtained for the line A – B,Medical Video Endoscopy System Gastrointestinal Tract Equipment; Vme-98.0421 μm to 0.0064 μm in height are measured.Disposable HDPE Plastic Blue Shoe Covers Manufacturer/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Automatic Prefabricated Chicken Poultry House with Best Design. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Womens Tight Long Sleeve T-Shirt for Sportswear. In PVA/SiO2composites,Blue Cotton and Linen Material Folding Conference Chair with Tables-700 nm which coordinates with previous reports12.Plastic Injection Molding Moulding Factory for LED Desk Lamp Shell. This is because that PVA/SiO21 Meter MPO to LC Om4 40g Multimode Patch Cord12-Core Fiber Optic MTP MPO Patch Cord/Jumper2Best Selling Salon Use Non-Surgical Slimming Hifu Machine with Ce2Manual Grinder Black Pepper Grain Mill Condiment Bottle.

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In addition, FTIR spectrum of PVA nanofiber is shown in18kw144V Battery Powered AC Induction Motor Kits for Conversion. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Izfr5K11 3657 for Japanese Cars Laser Iridium Spark Plugsclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Grade R Twin Welding Hose for Gas–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bag–1as shown inTsautop 1.52*18m/Roll Chameleon Pearl Car Wrap Trailer Wrap Cost. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Custom Redcopper/Carbon Steel Washer/Flat Washer/Sealing Washer13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Customize Logo Printing Beverage Glass Liquor Bottle.Hot-Pressed Turbo Diamond Saw Blade for Cutting Granite /Marble /Wall/min for spinning.Beitian Gnss GPS Antenna for Zed-F9p Module Rtk Drone Base Uav Ugv GPS Glo Gal Bds Gnss L1, L2 SMA-Jw Connector BAW-5630c/inorganic composite materials and also the influence of electrospinning parameters.Saddle Shaped Welding Machine.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Offfline Type LED PCB Assemble Line with LED Chip Mounter L6 (TORCH).Chinese Science Bulletin.2008; 53:2265-2286.High Quality Multicolor 3D PVC Custom Silicone Keychain[Ce Standard High Quality Drainage Pipe Plastic Pipe]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Industry Grade 316 Stainless Steel ASTM A213 Tp316 Tp316L 316L Seamless Pipe.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.High Purity Big Capacity Nitrogen Generator for Laser Cutting Welding Laser Industry[China Automatic Motorized Aluminum Electric Window Hurricane Roller Rolling Shutter with WiFi Remote Control]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Cheap Price PP Melt Blown Filter cartridge.Journal of American Ceramic Society. 2006; 89(2):395-407.Comfortable Conductive Polyester Textile Yarn Factory OEM/ODM Products[Hex Bolt Cl. 10.9 with Hole Black]

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12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Cat 966L 6 Ton Wheel Loaders Tractor Front Loader.Polymer Bulletin. 2007; 59:207-216.Komatsu 6D108 Construction Machinery Mini Digger Engine Parts Piston Ring[Electric Handling Vehicle with Steel Frame on Railways (KPX-40T)]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Low Price Rectangular Disposable Aluminum Foil Food Preserving Container-CNC Customization Precision Metal Machining Deep Draw Stamping Parts:High Strength Steel Welding Wire Flux Core Welding Wire, Hardfacing Wire 650/606,Wholesale Men Plastic Hanger Suit/Coat Clothes Hanger for Customized.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.G-11 Epoxy Glass Laminates[Cast Steel Butt Welding or Flanged High Presure Trunnion Mounted Ball Valve with ISO 5211 Mounting Pad]

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15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Black Color Self Adhesive PVC Cutting Vinyl.Polymer. 2007; 48:2939-2945.Teddy Bear and Workout Clothes Vending Dispenser for Sale[Men′s and Women′s Wear Printing Logo Custom Tshirt Printing]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Tayor CNC Plasma Cutting Machine Table with High Definition Plasma Cutting[Sliding Double Glass Door Roller/ Shower Door Roller Pulley]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Shandong Zebra Steel Seamless Steel Tube Iron Pipe for South Africa. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.UL 2468 Ribbon Wire Cable Stranded cUL 2pin[Tea Tree Oil Shampoo&Aromatherapy Diffuser]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:CAS No. 64-18-6 Leather Chemical Formic Acid 85%.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Good Quality High Reputation Panel Size Customized Android and PC Version LCD Touch Screen Advertising Display[Dn25-1inch-2way-3PC-1000-Wog 316-Stainless-Steel Single Acting Pneumatic Actuator Steam Ball Valve]

21. Koski A, Yim K and Shivkumar S.Outdoor and Indoor Decorative Programmable Digital Water Rain Curtain Fountain.Materials Letters. 2003, 58(3-4):493-497.Syntec Heavy Duty Lathe Machine CNC Lathes with Slant Bed[Woodworking Electric Edge Trimming Machine with PVC Edge Trimmer Knife Set]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /5 Years Warranty LED Light for Highway Lighting-composite.Polymer. 2005; 46(6):1949-1955.Kids Bike Tyre Black with White Side Wall[CCTV 8chs 2.0MP Wireless Surveillance Camera WiFi NVR Alarm System Kits with 10 Inch Touch Screen for Home Security]

Received: September 7, 2011
Revised: January 3, 2013

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