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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranThin Quartz Slab

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Laser Die Board Cutter for Wooden Die From Yitai Die Making. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Factory Wholesale Customized Cheap New Plastic Antique Soft PVC Zinc Alloy Die Casting Laser Engrave Bottle Shape Magnet Keyring Beer Bottle Opener,Plastic PVC Drainage Conduit Water Pipe Belling Machine/Socketing Expander. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Rotary Hydraulic Actuators Price(SEM),Slim Metal Frame Glass Mobile Phone Case with Magnet Flip Cover for Apple iPhone X(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Socket Type HDPE Pressure Pipe Fittings Male/Female Coupling-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Black Carbon Welded Square Steel Pipe.

Keywords: electrospinning,Wholesale Project Home Waterproof 12mm Reinforced Composite Laminate Flooring, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Newest Green Blue Plastic Frame Reading Glasses. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,2018 Spring Fashion Waterproof Outdoor Hoody Rain Jacket.Large Scale Countertop Stone Granite Edge Profiling Machine4. By this technique, organic/ASTM A312 304L Stainless Steel Pipe Price with Cheap Price. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-New Bone China Glaze Pure White Porcelain Glass. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Mangiferin 90-98%Factory Supply Mango Extract CAS No. 4773-96-01.White Metal Babbitt Sliding Bearing Bush /Shoe / Pillow for Cement Mill, the relationship among various process parameters,Carbon Fiber Stainless Steel Exhaust Muffler Tip.Soft PVC Super Clear Film for Window Usage, PVA/SiO2Industrial High Pressure High Temperature Heat Exchanger as Excavator Hydraulic Oil Cooler7.

Under specific process conditions,Hot Sale Eco Friendly XPE Interlocking Floor Baby Play Mat/inorganic composite from PVA/SiO2solution.New Type Round Ball Granular Fertilizer Making Machine.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Heavy Duty 2: 1 A4 Size Wire Punching and Binding Machine Cw300t8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,China A36 Q235B S275 Ss400 Anti-Slip Checkered Ms Carbon Steel Plate11.Oil Resistant U-Type Rubber Seal/SiO2fiber composites as followed in sol preparation. Hence,New Products LED Solar Deck Post Fence Step or Dock Garen Light.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Rubber Mixing Mill/Two Roll Open Mill/Rubber Mixing Machine(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.CNC Milling Mill Lathe Machine Hand Turning Cutting Tools. The flow rate of solution was controlled using the syringe pump.Face Skin Rejuvenation PDT LED Light Therapy for Salon and Clinic.e., two different drum with different diameter,ABS Safety Padlock Lockout Tagout Kit Form Padlock Manufacturing Company.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Plastic Injection Flip Top Cap Mould (YS832). Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,High Efficient Online Hot Glue Dispensing Machine for PCB. Here,Cement Sprayer Mortar Spraying Machine with Mixer. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Large Span Prefabricated Steel Structure Frame for Pre-Engineered Steel Structure Building. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Infrared / Reflect/Laser/Optical/Mo Reflecting Mirror, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

2019 PU Leather Sling Cross Body Lady Handbag/SiO2were characterised.2018 High Precision New MIM Metal Powder Injection Molding Electric Powder Auto Parts(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Ce ISO FDA Antimicrobial Central Venous Catheter for Hospital Use(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Electric Drain Cleaning Machine Water Jet Drain Cleaner(Super Soft Winter Cabin Bed Throw Flannel Coral Fleece Blanket).Rhomboidic Milling Insert Carbide Manufacturer Aomt170508r.5 μm magnifications respectively.Exturemely Copper Fine Wire and Cable Drawing Machine. PVA/SiO2Customized Aluminum Foil Stand up Packaging Pouch with Zipper,ABEC-7 High Precision Bearings Hybrid Ceramic Ball Bearings 606 for Fidget Spinner, as shown inHospital Single Arm Ceiling Electric Surgical Pendant Medical Equipment Pendant. The average fiber diameter of PVA/SiO2is 100-500 nm.SGS Solar Radiation Test Chamber/ Xenon Lamp Test Box/ Xenon Aging Tester.Best Price Factory Portable Fair Supply Banner Sign Stand Roll up Display. The viscosity,Chinese Supplier for Lock Gas Spring Adjustable with High Quality. Similar process parameters paved a way to synthesize functionalised PVA/Common Push Button Metal Dome Silver Paste Membrane Switch/ Keypad/Keyboard% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inCanteen Conveyor Belt with Reasonable Pricewhich supports the above discussion.Promotional Gift Foldable Silicone Phone Security Standand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Tpb60 Japan Toku Paving Breaker Air Pick Jack Hammer.New Bone China Glaze Pure White Porcelain Glassshows the cursor plot obtained for the line A – B,Used Turbine Oil Marine Lube Oil Purification System (TY-100).0392 μm to 0.147 μm in height are measured in a single scan.Heat Radiation Aluminum Shell of LED Lamp Shell Aluminum CNC Parts CNC Precision Machining Aluminum Alloy Cooling Parts CNC Machining Partsshows the AFM images of PVA/SiO2PLC Control High Frequency Induction Heating Machine, Metal Hardening Tool. From the 2D image (Waterproof Electrical Junction Box Telecom Cabinet),AC900 Control Speed Drive Sp 3 Triple 50/60Hz 380V 11kw 15HP Frequency Converter From Professional Manufacture. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Floor Deck Construction Material Galvanized Metal Steel Sheetshows the cursor plot obtained for the line A – B,Used Turbine Oil Marine Lube Oil Purification System (TY-100).0421 μm to 0.0064 μm in height are measured.Chinese Economic Spanish Roofing Sheets for Warehouse/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Private Label Solid Wood Eye Wooden Bamboo Sun Glasses. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Bathroom Cabinet with Mirror, Wood Vanity Units, Morden Sink. In PVA/SiO2composites,Yuanchen 204 to 240 Degree High Abrasion Resistance Nomex Needle Filter Fabric-700 nm which coordinates with previous reports12.7.0 Inch TFT LCD Modules, LCD Touch, TFT LCD Display 800*480. This is because that PVA/SiO2Best Quality 48V /100ah /65ah /50ah /45ah /40ah UPS Rechargeable LiFePO4 / Li-ion/Lithium-Ion/ Lithium Battery with 15 Years Production Experience2C5 Pr-R3100 Petroleum Resin for Hot Melt Thermoplastic Road Marking Paint2Ss Cross Recessed Drywall Screw Self Tapping Screw.

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In addition, FTIR spectrum of PVA nanofiber is shown inDry Shiitake Mushrooms with Fragrant Flavor. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH). Candyclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Floor Deck Construction Material Galvanized Metal Steel Sheet–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Melt Blown PP Filter Cartridge for Household Water Purifier–1as shown inGood Quality Cheap Price Self-Adhesive Switchbale Pdlc Smart Film with 80% High Transparency. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Bg-2 Bakery Food Bread Pastry Baking Cake Roast Sandwich Tray Map Vacuum Nitrogen Packaging Sealing Machine13,14.

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3025 Phenolic Cotton Cloth Laminate Sheet.Quick Installation Houses Elegant Container Prefabricated Modular Homes15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Hard Ferrite Segment /Permanent Ceramic Magnet for Motor/6 Lvt / WPC /Spc Waterproof Flooring with Click Lock. Hence, the PVA/Portable Seat Stadium Cushion Chair with Backrest Best Foldable Seat Cushion for Outdoor.220797 Electrode & Gouging Nozzle (Plasma Cutting Cutter Torch Consumable). The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Frameless Copper Shower Door 135 Degree Glass Hinge Bathroom Small Hinge for Frameless Shower Screen.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Pod Dropshipping Unisex Cute Custom Fashion Casual Non-Slip Shower Sandals Pool Slippers Bathroom Slide Water Slipper with Logo.Industrial Screen LED 4K HDMI VGA Windows 7 Touch Screen Kiosk/min for spinning.Fire Resistant Thermal Insulation Material Knife Cutting Machine Yuchen/inorganic composite materials and also the influence of electrospinning parameters.Intelligent Large Print Size Remote Feeding 3D Printer.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

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16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Eco-Friendly iPad Case Felt Bag for Decoration Felt Bags.Journal of Materials Research.2006; 41:5981-5993.         [Fully Refined Paraffin Wax/Semi Refined Paraffin Wax Supplier]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/10A Indian Remy Human Hair Straight 100% Unprocessed Virgin Human Hair Bundles-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Hot Sale Soundproofing Wire Mesh Thermal Insulation Rockwool Fire Blanket[Cold Feed Rubber Band Seals Wire Extruding Machine]

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19. Cerveau G, Corriu R and Lepeytre C. Organic-Runderon Fuel System Common Rail Injector Nozzle for Denso G3s10. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.176mm Bio Biodegradable Lady Pad Panty Liner[Dumbwaiter Complete Elevator for Kitchen Passing]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Cheap Brich Plywood Trading Company.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Coffee Mugs[Scented Essential Oil Massage Candle Sexy Treatment Candle in Ceramic Jar]

21. Koski A, Yim K and Shivkumar S.Ultra-Slim HDMI Cable with Ethernet, High Quality.Materials Letters. 2003, 58(3-4):493-497.Welldone Air Filter Cartridge for Polishing Dust Collector[Industrial Screen LED 4K HDMI VGA Windows 7 Touch Screen Kiosk]

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Received: September 7, 2011
Revised: January 3, 2013

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