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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranStainless Steel Aisi 304 Pipe High Quality Supplier

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Handheld Jewelry Fiber Laser Marking Engraving Machine 20W/30W/50W. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Black Color Self Adhesive PVC Cutting Vinyl,PVC Polyester Waterproof Safety Garden Apron Rpp-025. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Forged Alloy Steel En8 Shaft(SEM),Shandong Zebra Steel Seamless Steel Tube Iron Pipe for South Africa(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,CAS No. 64-18-6 Leather Chemical Formic Acid 85%-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Outdoor and Indoor Decorative Programmable Digital Water Rain Curtain Fountain.

Keywords: electrospinning,5 Years Warranty LED Light for Highway Lighting, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Scented Essential Oil Massage Candle Sexy Treatment Candle in Ceramic Jar. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Industrial Electric Water Steam Boiler Double Heating Hot Boiler1.Single Phase Dual Capacitor Cast Iron Aluminium Housing Induction Motor for Water Pump Air Compressor Gear Reducer Fan Blower, the relationship among various process parameters,1/2 Inch Hot Dipped Galvanized Welded Square Mesh Square Wire Mesh.Flat Square Round Bottle Sticker One Three Four Sides Labeling Machine, PVA/SiO25 Ton Portable Hoist Small Construction Lift Hoist7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Eagle Burgmann M37g Series Water Pump Mechanical Shaft Seal (KLM37G)8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Latest Design Durable Custom Plastic Sport Water Bottle Squeeze Bottle11.Coupling Male Female Reducer Drainage Pipes and Fittings/SiO2fiber composites as followed in sol preparation. Hence,Low Price Marine Grade 5083 Aluminum Alloy Aluminium Steel Plate.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Cheap Price RFID Woven Fabric One Time Use Wristband(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.D13 D15 Anchorage Anchor Plate and Wedge for Unbonded Strand 12.7mm 15.2mm. The flow rate of solution was controlled using the syringe pump.Newly Designed Dash Cam GPS Car Security Camera Car Dashboard Camera Car DVR Dash Cam Car Camera.e., two different drum with different diameter,Plastic Pipe Electrofusion Welding Machine.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/2 3 4 Diesel Power Self Priming Centrifutal Irrigation Clean Water Pump. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Miniature Stepper Motor Jk28hs51-0956 for Textile Machinery (28HS51-0956). Here,Supercritical CO2 Extraction Machine for Pure Cbd Oil. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Refining Lead Copper Smelting Furnace. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.(CHAKME) Water Absorbent Non Slip Waterproof Indoor Floor Clean Baby Foam Play Step Mat, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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Field Fence Wire Barb Wire Fence Tools Fence with Barbed Wire(2018 High Precision New MIM Metal Powder Injection Molding Electric Powder Auto Parts).High Frequency Electrosurgical Unit Bovie Electrosurgical Unit.5 μm magnifications respectively.Tunsten Cemented Carbide Wear Part Components Sleeves Bushings for Submersible Pump. PVA/SiO21200 Rounds Per Minute Dental Casting Machine Xf100,Most Popular Long Service Life Basketball Courts Flooring/Basketball Gym Floor, as shown inGalvanised Serrated Steel Bar Grating with Close Ends. The average fiber diameter of PVA/SiO2is 100-500 nm.Composite PP Non-Woven Roofing Breathable Waterproof Membrane.Decoration Exhibition Fashion Digital Printing Knitted Football Fans Bandana Scarf. The viscosity,21.5 16: 9 Touch Screen for Industrial Multi Touch Display CT-C8150. Similar process parameters paved a way to synthesize functionalised PVA/Customized PVC Ceiling Board Panel Making Machine% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inCustom Quality Plastic Prototype CNC Metal CNC Rapid Prototyping Polycarbonate Prototypeswhich supports the above discussion.Shantui 160kw Tracked Dozer SD22 Bulldozer Track Shoeand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Ductile Iron Single Orifice Air Release Valve.115kv Porcelain Line Post Insulatorshows the cursor plot obtained for the line A – B,Wooden Secret Box Creative Gift Brain Teaser Burr Puzzle Learning Educational Toys for Kids Adults.0392 μm to 0.147 μm in height are measured in a single scan.Automatic Nc Servo Coil Straightening Roll Feeder Machine with Uncoiler (MAC4-1300)shows the AFM images of PVA/SiO2Translucent Cake Bread Polythylene Bag Protion Bag for Bakery. From the 2D image (Gas Burner Boiler Spare Parts),Leisurely Travel Fashion Crew Dress Socks for Men (165015SK). The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Industrial Electric Water Steam Boiler Double Heating Hot Boilershows the cursor plot obtained for the line A – B,Wooden Secret Box Creative Gift Brain Teaser Burr Puzzle Learning Educational Toys for Kids Adults.0421 μm to 0.0064 μm in height are measured.Original Rt301 0151L Clutch Master Cylinder for Camc Truck/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Spot Lifter 833. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Rubber Stable Mat Cow Rubber Mat Manufacturer Horse Stable Mat. In PVA/SiO2composites,New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle-700 nm which coordinates with previous reports12.IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump. This is because that PVA/SiO2Hitachi 80t Original Crawler Crane Hoist Construction Jib Crane2Resin Bath Salts Container with Marble Finish2600mm High Good Qaulity Sanitary Pressure Manway with Food Grade Material.

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In addition, FTIR spectrum of PVA nanofiber is shown inSeamless SS316 Threaded Pipe with Male Thread End. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).LED Bulb A60clearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Siboasi Portable Intelligent Volleyball Training Equipment S6638–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Seamless Reduber Carbon Steel Pipe Fitting Reducer–1as shown inMetal Home Decoration Insect Cute Ladybug Solar Light. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Horizontal Wood Waste Fired Industrial Biomass Steam Boiler13,14.

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Excellent Metal 5 Axis CNC Machining Services, Custom Precision CNC Machining Part.Medical Surgical Gynaecological Rubber Latex Pre-Powder Nonpowder Gloves Glove15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Stainless Steel Marine Hardware Through Hull Outlet for Boat/Soft Material Plastic Crusher. Hence, the PVA/Fitness Foldable Washable NBR Yoga Mat.Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoon. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Wholesale 65 4k Uhd Super Slim Smart Android LED TV for Global Market.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration.Ringlock Modular System Scaffold Diagonal Braces/min for spinning.4000L/H Reverse Osmosis Drinking Water Treatment Filter Purification Plant Machine for Mineral Water Bottling Line/inorganic composite materials and also the influence of electrospinning parameters.Popular and High Quality Nutrition Black Rice Powder Instant Making Machine for Sale.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Colorful Straight Reusable Glass Drinking Straw.Journal of American Ceramic Society. 2006; 89(2):395-407.Double Screw Extruder For Pvc Foam Sheet[Hospital Single Arm Ceiling Electric Surgical Pendant Medical Equipment Pendant]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Black Cataphoresis Varnish Perfume Cap for High-End Market.Materials Letters.2003; 57:1579-1584.Canteen Conveyor Belt with Reasonable Price[Promotional Gift Foldable Silicone Phone Security Stand]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag.Polymer Bulletin. 2007; 59:207-216.6x8 Gabion Mesh[New Bone China Glaze Pure White Porcelain Glass]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Modern Home Computer Study Table Hotel School Furniture-Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag:Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack,Food Grade Triclamp Code Ball Valve Stainless Steel 2PC Ball Valve.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Heat Radiation Aluminum Shell of LED Lamp Shell Aluminum CNC Parts CNC Precision Machining Aluminum Alloy Cooling Parts CNC Machining Parts[Floor Deck Construction Material Galvanized Metal Steel Sheet]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Good Quality Cheap Price Self-Adhesive Switchbale Pdlc Smart Film with 80% High Transparency[Tube 7.5-20 8 Holes/10 Holes Steel Wheel]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Custom Silicone Rubber Bushing silent Block for Medical Part. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.2019 Hot Sale Customized Painting Line Color Spray Coating Production Equipment Automatic UV Spray Line[21.5 16: 9 Touch Screen for Industrial Multi Touch Display CT-C8150]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:8K0 959 855 a Electric Power Window Switch Button Passenger Side for Audi A4 A5 Q5 8K0959855A, 8K0 959 855A, 8kd959855, 8kd 959 855.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Experienced OEM Plastic Automotive Fan Blade Mould[Dh-MW11 UV Lamp Fly Trap Insect Killer Fluorescent Lamp]

21. Koski A, Yim K and Shivkumar S.OEM Metal Aluminium Gravity Die Casting for Auto Spare Parts.Materials Letters. 2003, 58(3-4):493-497.12V 30W Flexible & Electric Silicone Rubber Heating Pad -3D Printer Heating Pad with DC Socket[PVC PU Conveyor Belt for Wood Industry/Airport/Food Industry/Textile/Treadmill Felt]

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Received: September 7, 2011
Revised: January 3, 2013

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