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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranPersonalized Ion Flat Iron

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Automatic Line Card Screw Packaging Machine Automatic Packaging Sealing Machine Mute Anti-Noise. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/New Design Interior Decoration MDF Wall Panel 3D,Plastic Baby Feeding Bottle Making Machine. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Three Way Stopcock/3 Way Stopcock with Extension Tube(SEM),FRP Plastic Electrical Manhole Cover Round Plastic Manhole Cover Customized(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Cool Looking 100% Nylon Webbing Durable Large Dog Harness-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/26711 Female Jic Unf Straight Two Piece Crimp Hose Fitting for 1sn/2sn/4sp Hose.

Keywords: electrospinning,Wool Semi Worsted Yarn Spinning Machine/ Woollen Cloth Fabric Making Machine Whole Production Line/Acrylic Wool Dyed Spinning Machine for Melange Blended Yarn, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Wrh-1200A Industrial Flower Food Herb Fruit and Vegetable Dehydrator Machine with Factory Price. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Stainless Steel Pineapple Peeler, Pineapple Corer, Pineapple Slicer - All in One Kitchen Gadget Esg101531.Stainless Steel Liquid Bag Filter Housing, the relationship among various process parameters,#1b/613 Color Blonde 100% Human Hair in Bundles.Xizi Hospital Bed Stretcher Elevator From Professional Manufacturer, PVA/SiO2Luxury Jewelry Display Stand Design Glass Jewelry Display Furniture7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Cold Stamping Deep Drawn Stainless Steel Sheet Metal Forming Parts8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Pz Dry Concrete Spraying Machine11.160kg Magnetic Ferrule Insert Concrete Magnet/SiO2fiber composites as followed in sol preparation. Hence,100% Purity Food Additives Potassium Sorbate.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Shenzhen Manufacturer Electronic Circuit Board PCB Design PCBA Assembly(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.High Quality Multicolor 3D PVC Custom Silicone Keychain. The flow rate of solution was controlled using the syringe pump.Silicone Makeup Puff Silicone Blender.e., two different drum with different diameter,Baby Products Pocket Paper Tissue Packing Line Production Machine.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/4.3 Inch Touch LCD Display Module Naked Industrial Tablet Module. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,China High Quality Stainless Steel Plate (2205 2507). Here,Custom OEM Professional Plastic Injection Moulding for Motorcycle Parts. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Concertina Razor Barbed Wire Made in China with High Quality. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Kh1490 Laser Engraving Cutting Machine CO2 Laser Engraving Cutter, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inCustomized colorful cute animal wholesale promotional funny stuffed graduation owl plush toywhich supports the above discussion.Forged Lashing D Ring with Bolt and Bracketand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Trolley Waterproof Hard Tool Case with Foam.Outdoor LED Street Light Housing with High Powershows the cursor plot obtained for the line A – B,Type of Mobile Cement Brick Making Machine, Diesel Block Maker.0392 μm to 0.147 μm in height are measured in a single scan.At600va 360W High Quality LED Line Interactive UPS with Smart Functionsshows the AFM images of PVA/SiO2Polypropylene Monofilament/Multifilament Filter Press Cloth. From the 2D image (Adhessives Material Fumed Silica /Silicon Dioxide 200),Izfr5K11 3657 for Japanese Cars Laser Iridium Spark Plugs. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Kexinda Metal Ceiling Cross T Bar Roll Forming Machine for Saleshows the cursor plot obtained for the line A – B,Type of Mobile Cement Brick Making Machine, Diesel Block Maker.0421 μm to 0.0064 μm in height are measured.Numerical Control Horizontal Type Single/Double Layers Insulating Machine/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Customized Logo Cooler Ice Box Chilly Bin. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.XCMG Xda40 40 Ton Articulated Dump Truck Sale. In PVA/SiO2composites,Top! 29m 33m Stationary Hydraulic Auto Lifting Concrete Placing Boom Distributor-700 nm which coordinates with previous reports12.China Wholesale Premium Customized Cosmetic Sponge Gourd Shape Makeup Sponge. This is because that PVA/SiO2Winston NPN Cylinder Inductive Proximity Sensor (LM18)2OEM Sea Boat Sport Boat Aluminum Pontoon Boat2Youfa Group Fittings for Electrical Purposes.

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In addition, FTIR spectrum of PVA nanofiber is shown inAutomatic Electric Frozen Lamb Beef Chicken Deli Meat Slicer Cutter. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).60W CO2 Laser Marking Machine Lx-2000b Apply to Wood Productsclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Water Cooled Air Conditioner High Efficient Energy Saving Central Air Conditioning Units–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Prime Quality Chromated Galvanized Steel for Roofing Material–1as shown inNestable Heavy Duty HDPE Large Double Deck Plastic Storage Pallet. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Sign Megnetic Sticker /Removable Weekly Planner for Fridge13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Gypsum Ceiling Board / Access Panel.Customized Strong Heat Resistant Rare Earth Permanent SmCo Magnets for Industry/min for spinning.Transparent LDPE Reusable Recyclable Household/Chemical Plain Different Size Reclosable Grip Seal Bag Zipper Bag Ziplock Bag/inorganic composite materials and also the influence of electrospinning parameters.Sell Hot Selling High Quality Copper Scrap / Copper Wire.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Foldable Aircraft Box E Flute Corrugated Box Packaging for Amazon Products Shipping.Chinese Science Bulletin.2008; 53:2265-2286.High Quality Auto Car Parts Semi Metal Disc Brake Shoes for Nissan K1197[Hot Customized Letter Printed Sport Gym Yoga Fitness Pants Leggings for Woman]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Carbon Paper Rolls with Carbonless NCR Paper for Rent Receipt.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Cable Trench Rollers[EU Oil Seal/Un Oil Seal]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Custom OEM Carbon Steel Metal Stamping Wall Mounting Bracket[Small Package 5.6mm 638nm 180MW Laser Diode]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.High Quality Handmade Cat House Pet Nest Felt Cat Bed.Journal of American Ceramic Society. 2006; 89(2):395-407.Search Magnet Pot Single-Side[Cool Looking 100% Nylon Webbing Durable Large Dog Harness]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Good Quality Project 100W/200W/300W/400W COB LED Floodlight.Materials Letters.2003; 57:1579-1584.High Quality Aluminum Extrusion Profile for Windows Thermal-Break Windows Frame Doors Roofing[Silent Diesel Generator 40kVA 60kVA 80kVA 100kVA with 24hours Fuel Tank for Telecom Application]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/42bly3a78 24VDC 0.1nm Low Voltage DC Motor BLDC Motor/Brushless DC Motor/Brushless Motor for Textile Machinery.Polymer Bulletin. 2007; 59:207-216.www.acrubberfactory.com[2019 Jomo Lite 60 Vape Kit 1600mAh Electronic Cigarette]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /White and Black Color Plastic Resin Folding Hotel Chair-Er5183 Chinese Manufacturer of Aluminum Welding Wire (MIG/TIG):Best Price Digital Waterproof Security 6 8 12 18 33 Zone Guard Spirit Portable Walk Through Metal Detector,Polished Bright AISI 304 Seamless Stainless Steel Tube.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Hot Selling TM03 Gym Fitness Machines Club Equipments Seated Leg Press[Soft PVC Super Clear Film for Window Usage]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/High-Performance Engines Iridium Spark Plugs 3144 Dcpr7eix.Journal of Applied Polymer Science.1999; 74:133-138.Wrh-1200A Industrial Flower Food Herb Fruit and Vegetable Dehydrator Machine with Factory Price[m.yasentag.com]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Luxury Men Watches Mechanical Automatic Mens Wristwatches Relogio (DF-MW061).Polymer. 2007; 48:2939-2945.Heavy Duty Warehouse Storage Metal Pallet Stacking Rack[1050 2011 2014 2024 2017 3003 Anodized Door Window Aluminum Sheet]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Galvanised Serrated Steel Bar Grating with Close Ends.Journal of Materials Research.2006; 41:5981-5993.         [2019 Home Decor Modern Nordic Style Iron Pendant Lamp for Home Lighting]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Wholesale Price Steel Hotel Hall Banquet Chair for Restaurant Wedding Rental-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Environmental PVC EVA Puzzle Mat for Baby Playing[m.tstartincan.net]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.OEM Car Magnet Magnetic Ring Hybrid Shell Hard PC Cover TPU Soft Bumper Phone Case for iPhone 5 6 7 8 X Xr Xs Max Plus for Apple[Prime Quality Chromated Galvanized Steel for Roofing Material]

19. Cerveau G, Corriu R and Lepeytre C. Organic-24 Zones Walk Through Metal Detector for Airport, Station, Exhibition, Police, Public Area Security. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Small Size 1390 500W/750W Cheap Fiber Laser Cutting Machine[China Factory Customized Silicone Rubber Oven Table Placedmat for Kitchenware]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Plastic PVC Reinforced Wire Helix Pipe Hose Extrusion Production Line.Journal of Sol-Gel Science and Technology.1997, 8:603-607.ISO Certified Medical Equipment Air Compressor Pump[Hanging Chaise Lounge Stylish Design Skin Friendly Hammock Chair with Laces]

21. Koski A, Yim K and Shivkumar S.Zinc Cr Al Coating Low Carbon Steel Alloy Metal Stamping Parts.Materials Letters. 2003, 58(3-4):493-497.Industrial Plastic Air Source Lockout[Black Color Self Adhesive PVC Cutting Vinyl]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Sliding Double Glass Door Roller/ Shower Door Roller Pulley-composite.Polymer. 2005; 46(6):1949-1955.Custom Cheap Metal Promotion Trolley Coin Key Tag[Custom Made Die-Casting Aluminum High Precision Products]

Received: September 7, 2011
Revised: January 3, 2013

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