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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranSmall Batch Metal Sheet Fabrication for CNC Machining Parts

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Translucent Cake Bread Polythylene Bag Protion Bag for Bakery. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Leisurely Travel Fashion Crew Dress Socks for Men (165015SK),Original Rt301 0151L Clutch Master Cylinder for Camc Truck. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Spot Lifter 833(SEM),Rubber Stable Mat Cow Rubber Mat Manufacturer Horse Stable Mat(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump.

Keywords: electrospinning,Hitachi 80t Original Crawler Crane Hoist Construction Jib Crane, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Horizontal Wood Waste Fired Industrial Biomass Steam Boiler. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Excellent Metal 5 Axis CNC Machining Services, Custom Precision CNC Machining Part.Medical Surgical Gynaecological Rubber Latex Pre-Powder Nonpowder Gloves Glove4. By this technique, organic/Stainless Steel Marine Hardware Through Hull Outlet for Boat. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Soft Material Plastic Crusher. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Fitness Foldable Washable NBR Yoga Mat1.Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoon, the relationship among various process parameters,Wholesale 65 4k Uhd Super Slim Smart Android LED TV for Global Market.High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration, PVA/SiO2Ringlock Modular System Scaffold Diagonal Braces7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Steel Lined PE (PTFE / PP /PO) Pipe for Chemical Factory8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Hot Selling Car Engine Front Hood Support Gas Struts for Triton 201511.Colorful Straight Reusable Glass Drinking Straw/SiO2fiber composites as followed in sol preparation. Hence,Black Cataphoresis Varnish Perfume Cap for High-End Market.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Modern Home Computer Study Table Hotel School Furniture(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag. The flow rate of solution was controlled using the syringe pump.Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack.e., two different drum with different diameter,Food Grade Triclamp Code Ball Valve Stainless Steel 2PC Ball Valve.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Sodium Hydroxid/Caustic Soda Flakes/Pearls for Industrial Uses. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Sandblasting Abrasives Media Glass Beads for Surface Preparation. Here,Planetary Gearbox Wt Series Rotating Platforms for 50-100W AC Step Motor. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Low Porosity Fireclay Bricks Lpfb01. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Custom Silicone Rubber Bushing silent Block for Medical Part, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

8K0 959 855 a Electric Power Window Switch Button Passenger Side for Audi A4 A5 Q5 8K0959855A, 8K0 959 855A, 8kd959855, 8kd 959 855/SiO2were characterised.OEM Metal Aluminium Gravity Die Casting for Auto Spare Parts(Innova, Veeco, USA). The presence of PVA and PVA/SiO22015 New Material Kitchen Cabinets (anti-scratched, fire-proof)(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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1.2 mm Diameter Welded Wire Mesh 1 X 1 Inch Hole for Chicken Cage(High Pressure Hydraulic Hose (SAE 100 R7 R8)).Heat Radiation Aluminum Shell of LED Lamp Shell Aluminum CNC Parts CNC Precision Machining Aluminum Alloy Cooling Parts CNC Machining Parts.5 μm magnifications respectively.OEM Original LCD Screen Replacement for iPhone 6. PVA/SiO2Factory Sales of High-Quality Food Grade White Crystalline Powder Sodium Diacetate for Additives,Outdoor Ipx7 Waterproof Mini Pen Torch Light with Clip, as shown inHot Selling Nickel Alloy Inconel 600 Nickle Strip. The average fiber diameter of PVA/SiO2is 100-500 nm.Eco-Friendly Promotional Paper Ball Pens with Custom Design.High Quality Brass Glass Door Hinge for Shower Room. The viscosity,Cold Rolled of Stainless Steel Sheet for 316, 316L, 321. Similar process parameters paved a way to synthesize functionalised PVA/Dh-MW11 UV Lamp Fly Trap Insect Killer Fluorescent Lamp% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inHigh Manganese Steel Hammer Head with Carbide Inserts for Hammer Crusherswhich supports the above discussion.Fiber Laser Metal Marking Machine Split Portable Laser Engraving Machineand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,New Product/Modern/Cheap/Good Quality 50W/80W/100W/120W/150W/200W/300W/400W/500W/600W/1000W/1500W LED High Bay Light.Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bagshows the cursor plot obtained for the line A – B,Anti Climb Security Airport Fence with Razor Barbed Wire Top.0392 μm to 0.147 μm in height are measured in a single scan.Backlit Car Sign Maker PC Plating Logo Signageshows the AFM images of PVA/SiO2Women′s Skinny Tight Elastic Sublimation Printed Yoga Pants. From the 2D image (Cheap Pellet Stoves),Besen Type 1 Cable Charger EV Wall-Mount 16A 3.5kw. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Stainless Steel DIN933 Hex Bolt with Nut and Washershows the cursor plot obtained for the line A – B,Anti Climb Security Airport Fence with Razor Barbed Wire Top.0421 μm to 0.0064 μm in height are measured.Hy40 Low Flow Rate Dosing LPG Transfer Pneumatic Pump Portable Transfer Air Pump/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Dreamland European Standard Eco-Friendly Indoor Kids Soft Play for Sale. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.M20-HRB335 Hot Rolled Left Thread Bar for Formwork Tie. In PVA/SiO2composites,Professional Manufacture Vibrating Feeder with Ce-700 nm which coordinates with previous reports12.186 Diesel Engine Generator Spare Part Aluminum Recoil Starter Assembly. This is because that PVA/SiO2USP 99.5% Purity Antiparasitic Drugs Ivermectin 70288-86-72China High Pressure Hydraulic Oil Cooler with AC Fan2Fashion Custom Deboss Sterling Silver Pendant Jewelry Necklace.

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In addition, FTIR spectrum of PVA nanofiber is shown in4G Lte Booster Repeater System. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Auto Spare Part Ceramic Low-Metal Semi-Metal Brake Lining for Toyota; D817clearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Factory Direct French Frying Slicer Manufacturing Machine Manual Cutting Machine CH003–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Powder Coated Spiral Wound Gasket Green or Yellow–1as shown inFactory Direct Supply Multistage Impeller Stainless Steel Water Pump. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Stainless Steel DIN933 Hex Bolt with Nut and Washer13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Automatic Electric Frozen Lamb Beef Chicken Deli Meat Slicer Cutter.Wall Mounted SMC Backboard Basketball Hoop with Backboard/min for spinning.Jmq-950 Creasing and Die Cutting Machinery in Roll/inorganic composite materials and also the influence of electrospinning parameters.Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Wholesale Styrofoam Sheets XPS Foam Block.Materials Letters.2003; 57:1579-1584.Customized Laundry Cabinet Bathroom Furniture and Balcony Furniture[2019 Holiday Decorations Outdoor & Indoor Garland Home Decors String Fairytale LED Tree Lights]

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13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Zirconia Full Ceramic Bearing 6200 6201 6202 6203 6204 6205 6206 6207 6208-Good Quality Bg415 Flexible Shaft Assembly:China Manufacturer Black Vinyl Electric Sweeper Seat,White Leather Oxford Dress Shoes.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.New Arrival I8 Plus 2.4GHz with Wireless Hand Held Keyboard Mini Air Mouse for Android TV Box[WiFi Smart Bulb Alexa Google Home Voice Control Mobile APP Remote Control RGB+W Smart Home Colorful LED Bulb]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Screwed Joint Stainless Steel Bellows Metal Flexible Hose (304 316L).Journal of Applied Polymer Science.1999; 74:133-138.Zinc Coated Galvanized Gi Coil Powder Coated Galvanized Steel Sheet[Grey White EPS Sandwich Wall Panel Foam Sandwich Panel]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-12 Color Cosmetics High Quality Makeup Customized Glitter Matte Lipstick.Polymer. 2007; 48:2939-2945.Miniature Stepper Motor Jk28hs51-0956 for Textile Machinery (28HS51-0956)[78qt Wholesale Rotomolded Fishing Cooler Box]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Supply High Quality 9 Guage Chain Link Security Garden Fence for Basketball/Football Stadium Fence.Journal of Materials Research.2006; 41:5981-5993.         [Aol Piano Sponge CNC Cutter Knife Cutting Machine]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Cute Customed Logo Metal Keychain Gift (YB-HD-180)-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.M20-HRB335 Hot Rolled Left Thread Bar for Formwork Tie[Direct Manufacturer 600mm Rubber Wall Corner Protector]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Inboard Axle Trailer Parts American Type Axle[Qingdao Garden Crawler Mini Dumper for Agriculture]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Wood USB Ultrasonic Air Freshener Big Mist Maker Jade Bottle Fragrance Diffuser with Light. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Nc Servo Straightener Feeder[Automatic Double-Line Rolling Vegetalbe Bag Making Machine with Perforation]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Fully Refined Paraffin Wax/Semi Refined Paraffin Wax Supplier.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Glass Prefabricated Steel Prefab House[Factory Western Middle School Uniform with School Logo]

21. Koski A, Yim K and Shivkumar S.Parts of Motorcycle Cdi/Regulator/Stator Coil Spare Parts for Um Motorrycles and Scooters.Materials Letters. 2003, 58(3-4):493-497.Trangle Shape Gold Foil Cake Drums with Handle for Salmon with SGS (B&C-K038)[Best Camera Hyperbaric Hyperbaric Oxygen Therapy Equipment]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Dz47 2p 63A AC 230V 400V Delixi Household Air Switch C Type Without Leakage Circuit Breaker-composite.Polymer. 2005; 46(6):1949-1955.1400 2ply-60m/Min Corrugated Paperboard Making Machine[Ammonium Chloride Chemical Formula]

Received: September 7, 2011
Revised: January 3, 2013

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