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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranAuto Parts

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Leisurely Travel Fashion Crew Dress Socks for Men (165015SK). As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Original Rt301 0151L Clutch Master Cylinder for Camc Truck,Spot Lifter 833. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Rubber Stable Mat Cow Rubber Mat Manufacturer Horse Stable Mat(SEM),New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Hitachi 80t Original Crawler Crane Hoist Construction Jib Crane.

Keywords: electrospinning,Resin Bath Salts Container with Marble Finish, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Fitness Foldable Washable NBR Yoga Mat. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoon1.Wholesale 65 4k Uhd Super Slim Smart Android LED TV for Global Market, the relationship among various process parameters,High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration.Ringlock Modular System Scaffold Diagonal Braces, PVA/SiO24000L/H Reverse Osmosis Drinking Water Treatment Filter Purification Plant Machine for Mineral Water Bottling Line7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Hot Selling Car Engine Front Hood Support Gas Struts for Triton 20158,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Colorful Straight Reusable Glass Drinking Straw11.Black Cataphoresis Varnish Perfume Cap for High-End Market/SiO2fiber composites as followed in sol preparation. Hence,Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack. The flow rate of solution was controlled using the syringe pump.Food Grade Triclamp Code Ball Valve Stainless Steel 2PC Ball Valve.e., two different drum with different diameter,Sodium Hydroxid/Caustic Soda Flakes/Pearls for Industrial Uses.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Sandblasting Abrasives Media Glass Beads for Surface Preparation. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Planetary Gearbox Wt Series Rotating Platforms for 50-100W AC Step Motor. Here,Low Porosity Fireclay Bricks Lpfb01. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Custom Silicone Rubber Bushing silent Block for Medical Part. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.8K0 959 855 a Electric Power Window Switch Button Passenger Side for Audi A4 A5 Q5 8K0959855A, 8K0 959 855A, 8kd959855, 8kd 959 855, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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In addition, FTIR spectrum of PVA nanofiber is shown inClassic Brown PU Leather Key Holder Only Online Phone Personalized Phone Stand. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).China Wholesale Premium Customized Cosmetic Sponge Gourd Shape Makeup Spongeclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Powder Coated Spiral Wound Gasket Green or Yellow–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Stainless Steel DIN933 Hex Bolt with Nut and Washer–1as shown inPC50hm Series Spare Parts for Excavator Pump. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Hot Sell Reddot Awarding School Student Plastic Chair13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Wall Mounted SMC Backboard Basketball Hoop with Backboard.Jmq-950 Creasing and Die Cutting Machinery in Roll/min for spinning.Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard/inorganic composite materials and also the influence of electrospinning parameters.450V 12UF Cbb60 Wire Series Grey Shell Capacitor.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.New Arrival I8 Plus 2.4GHz with Wireless Hand Held Keyboard Mini Air Mouse for Android TV Box.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Titan 40 Tons Cement Bulk Carriers for Sale[Makute Electric Power Drill Hand Mini Drilling Tools with 450W]

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10. David YL, Michael A, Richard JA, Vohden Junior D, Chen and David CM. Tailored nanofiber morphologies using modulated electrospinning for biomedical applications.Material Research Society Symposium Proceedings. 2003. 736:D3.8.1-D3.8.6.         [Label Paper Tape Flexo Printing Machine]

11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Rapid Kit Dry Immunofluorescence Quantitative Analyzer Mslif01c, Hba1c.Materials Letters.2003; 57:1579-1584.OEM Manufacturer 12V 24V Small DC Planetary Gear Motor[42cm 3D Hologram Fan with WiFi Holographic LED Fan Display]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Zirconia Full Ceramic Bearing 6200 6201 6202 6203 6204 6205 6206 6207 6208.Polymer Bulletin. 2007; 59:207-216.Prp Mesotherapy Injection Gun[Professional Travel Amenities Sets]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Good Quality Bg415 Flexible Shaft Assembly-China Manufacturer Black Vinyl Electric Sweeper Seat:White Leather Oxford Dress Shoes,Screwed Joint Stainless Steel Bellows Metal Flexible Hose (304 316L).Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Metal Fittings for Pipe and Joint System (H-6A)[Stable and High Precision CNC Milling Machinery Tool]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/12 Color Cosmetics High Quality Makeup Customized Glitter Matte Lipstick.Journal of Applied Polymer Science.1999; 74:133-138.Multi-Wedge Rubber Belt From Ningbo China[Mine Carboxymethylcellulose Sodium Salt Supplier & Factory]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Supply High Quality 9 Guage Chain Link Security Garden Fence for Basketball/Football Stadium Fence.Polymer. 2007; 48:2939-2945.Medical Automatic Volumetric Infusion Syringe Pump; IP737[Qt4-20 Brick Molding Machine Pavers Block Brick Making Machine]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Cute Customed Logo Metal Keychain Gift (YB-HD-180).Journal of Materials Research.2006; 41:5981-5993.         [Hot Selling Wall PIR Motion Sensor for Home Security]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Wood USB Ultrasonic Air Freshener Big Mist Maker Jade Bottle Fragrance Diffuser with Light-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Most Popular Long Service Life Basketball Courts Flooring/Basketball Gym Floor[300t /24h Wheat Flour Milling Machine]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Automatic Sf6 Gas Hexafluoride Density Relay Calibrator[9mm Diamond/Snake Top Polishing Conveyor Belt for Stone/Ceramics/Granite Industry]

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20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Parts of Motorcycle Cdi/Regulator/Stator Coil Spare Parts for Um Motorrycles and Scooters.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Cheap Pipe Laser Cutter with Automatic Feeding Patent Design[Stackable Brown Color Beech Wood Cross Back Chair for Garden]

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22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Custom OEM Carbon Steel Metal Stamping Wall Mounting Bracket-composite.Polymer. 2005; 46(6):1949-1955.Outdoor LED Street Light Housing with High Power[Eco Square Bottom Biodegradable Food Pouch Factory China]

Received: September 7, 2011
Revised: January 3, 2013

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