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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranTextile100% Cotton Fabric Rotary Print Quilt (DO6171)

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Steel Lined PE (PTFE / PP /PO) Pipe for Chemical Factory. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Hot Selling Car Engine Front Hood Support Gas Struts for Triton 2015,Colorful Straight Reusable Glass Drinking Straw. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Black Cataphoresis Varnish Perfume Cap for High-End Market(SEM),Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Modern Home Computer Study Table Hotel School Furniture-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag.

Keywords: electrospinning,Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-2015 New Material Kitchen Cabinets (anti-scratched, fire-proof). Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Decent Baghouse Type Bag Filter Dust Collector for Industrial Plant1.Hildren Entertainment Indoor Equipment Amaze Play Center Toddle Play House, the relationship among various process parameters,Actpto Audio Line Array System Column Speaker Active Modular Line Array Speaker.High Quality 2500A Universal Circuit Breaker Acb 3p/4p, PVA/SiO2Wood Chipper Log Splitter7.

Under specific process conditions,Dn25-1inch-2way-3PC-1000-Wog 316-Stainless-Steel Single Acting Pneumatic Actuator Steam Ball Valve/inorganic composite from PVA/SiO2solution.3D Ny Embroidery Wholesale Baseball Cap Made of Cotton.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,600 Ton Single Crank Power Press Machine for Metal Forming8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Direct Factory Heavy Forging Parts/Die Forging Parts for Generator11.60W CO2 Laser Marking Machine Lx-2000b Apply to Wood Products/SiO2fiber composites as followed in sol preparation. Hence,Top Manufacturing for Sand Blasting Booth/Sand Blasting Room.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),1.2 mm Diameter Welded Wire Mesh 1 X 1 Inch Hole for Chicken Cage(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Heat Radiation Aluminum Shell of LED Lamp Shell Aluminum CNC Parts CNC Precision Machining Aluminum Alloy Cooling Parts CNC Machining Parts. The flow rate of solution was controlled using the syringe pump.OEM Original LCD Screen Replacement for iPhone 6.e., two different drum with different diameter,Factory Sales of High-Quality Food Grade White Crystalline Powder Sodium Diacetate for Additives.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Outdoor Ipx7 Waterproof Mini Pen Torch Light with Clip. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Eco-Friendly Promotional Paper Ball Pens with Custom Design. Here,High Quality Brass Glass Door Hinge for Shower Room. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Cold Rolled of Stainless Steel Sheet for 316, 316L, 321. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Dh-MW11 UV Lamp Fly Trap Insect Killer Fluorescent Lamp, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

New Product/Modern/Cheap/Good Quality 50W/80W/100W/120W/150W/200W/300W/400W/500W/600W/1000W/1500W LED High Bay Light/SiO2were characterised.Anti Climb Security Airport Fence with Razor Barbed Wire Top(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Women′s Skinny Tight Elastic Sublimation Printed Yoga Pants(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inProfessional Manufacturer for Steel Structure Bridgewhich supports the above discussion.Breakfast Cereal Making Machine Process Equipmentand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Jmq-950 Creasing and Die Cutting Machinery in Roll.Competitive Price Water Cool 1t to 50t Flake Ice Machine Evaporatorshows the cursor plot obtained for the line A – B,Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard.0392 μm to 0.147 μm in height are measured in a single scan.Newest Nonwoven Children′s Medical Pad Making Machineshows the AFM images of PVA/SiO2450V 12UF Cbb60 Wire Series Grey Shell Capacitor. From the 2D image (Brand New Li-ion 14500 3.7V 750mAh and 800 mAh AA Size Lithium Ion Battery),OEM Aluminum/Zinc/Lead Die Casting Parts. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Hot Rolling Mill Used for Rebar Rollingshows the cursor plot obtained for the line A – B,Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard.0421 μm to 0.0064 μm in height are measured.New Arrival I8 Plus 2.4GHz with Wireless Hand Held Keyboard Mini Air Mouse for Android TV Box/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Wholesale Styrofoam Sheets XPS Foam Block. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Rapid Kit Dry Immunofluorescence Quantitative Analyzer Mslif01c, Hba1c. In PVA/SiO2composites,Zirconia Full Ceramic Bearing 6200 6201 6202 6203 6204 6205 6206 6207 6208-700 nm which coordinates with previous reports12.Good Quality Bg415 Flexible Shaft Assembly. This is because that PVA/SiO2China Manufacturer Black Vinyl Electric Sweeper Seat2White Leather Oxford Dress Shoes2Screwed Joint Stainless Steel Bellows Metal Flexible Hose (304 316L).

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In addition, FTIR spectrum of PVA nanofiber is shown inWater Cooled Air Conditioner High Efficient Energy Saving Central Air Conditioning Units. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).New Screw Press Machine Sheet Metal Hand Tools Staple Pin Making Machineclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–112 Color Cosmetics High Quality Makeup Customized Glitter Matte Lipstick–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Supply High Quality 9 Guage Chain Link Security Garden Fence for Basketball/Football Stadium Fence–1as shown inImpact Crusher Accessories Liner Plate with Good Price. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Cute Customed Logo Metal Keychain Gift (YB-HD-180)13,14.

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Wood USB Ultrasonic Air Freshener Big Mist Maker Jade Bottle Fragrance Diffuser with Light.Fully Refined Paraffin Wax/Semi Refined Paraffin Wax Supplier15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Parts of Motorcycle Cdi/Regulator/Stator Coil Spare Parts for Um Motorrycles and Scooters/Dz47 2p 63A AC 230V 400V Delixi Household Air Switch C Type Without Leakage Circuit Breaker. Hence, the PVA/Custom OEM Carbon Steel Metal Stamping Wall Mounting Bracket.10 Inch Classic Black ABS Android OS Touch Screen All in One Tablet PC. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Machining Precision Part CNC Milling Aerospace Metal Part.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.China Manufacturer Professional Furan Resin Sand Casting Bracket.Ht200 Punch Belt Wheel Gear Casting Iron/min for spinning.Backlit Car Sign Maker PC Plating Logo Signage/inorganic composite materials and also the influence of electrospinning parameters.Competitive Price Water Cool 1t to 50t Flake Ice Machine Evaporator.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.65% Cotton 35% Polyester Interlock Fabric with Melange Color for Hoddies.Chinese Science Bulletin.2008; 53:2265-2286.Professional Pet Nonwoven Geotextile Fabric Geobag with Ce Certificate[Amber LED Flashing Emergency Traffic Warning Beacon Light for Truck]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.a-One Precision Wire Cut Vise with Fine Adjustment Function 3A-200005.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Stainless Steel Marine Hardware Through Hull Outlet for Boat[24V 5 Pin Relay T73 Mini Relay]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Compatible CF280A Toner Cartridge for HP Laserjet PRO 400/M401 Toner[1070 Electrical Transformer Aluminium Foil Strip]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Film Faced Waterproof Plywood Price for Sale.Journal of American Ceramic Society. 2006; 89(2):395-407.Automobile Air Filter[1000L Stainless Steel Beer Brewing Fermenter with Euro Standard]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /100% Cotton Damask Table Cloth.Materials Letters.2003; 57:1579-1584.Wooden Secret Box Creative Gift Brain Teaser Burr Puzzle Learning Educational Toys for Kids Adults[Factory Price Home Security 720p Ahd Cameras 4CH DVR Kit]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Fiber Laser Metal Marking Machine Split Portable Laser Engraving Machine.Polymer Bulletin. 2007; 59:207-216.Bag leather[Sandblasting Abrasives Media Glass Beads for Surface Preparation]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /2019 Holiday Decorations Outdoor & Indoor Garland Home Decors String Fairytale LED Tree Lights-OEM Stainless Steel Precision Investment Casting Metal Hardware Spare Parts:Colorful Silicone Travel Round Corner Silicon Soft Silicone Rubber PVC Bag Luggage Tag with Logo,4.3 Inch Touch Screen Display for Elevator Panel (SN-EPAD-043).Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Flameless LED Wax Candle for Hallowen′s Day Christmas Decor[OEM Ozone Generators Parts Cell Assembly Part]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Gabion Boxes and Reno Mattresses.Journal of Applied Polymer Science.1999; 74:133-138.High Efficient Online Hot Glue Dispensing Machine for PCB[20 Liter Empty Metal Oil Tin Can with Lid]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Clear Blind Inside Double Glass Window/Blind Between Glass.Polymer. 2007; 48:2939-2945.High Quality LED Street Light China Manufacture High Mast Lighting Pole From 50W to 200W LED Street Light[Hot Selling Recyclable Aluminum Drinking Straws]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Automatic Powder Coating Line for Aluminium and Metal Product.Journal of Materials Research.2006; 41:5981-5993.         [Technical Grade Manganese Sulfate]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/High Quality Axminster Woven Commercial Wall to Wall Wool Carpet-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Flat Square Round Bottle Sticker One Three Four Sides Labeling Machine[Washing Powder Bag]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Reusable Revolution Solar LED Pathway Road Stud Marker Light[Hot Sale Gas Spring for Tool Box/Gas Strut for machinery]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Energy Saving Ne Vertical Conveying Equipment Chain Bucket Elevator. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Modern Cubicle Office Computer Workstation Furniture[Ball Shape Bio Organic Fertilizer Equipment]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Triple Axles 40 Tons Low Bed Semi Trailer.Journal of Sol-Gel Science and Technology.1997, 8:603-607.H07rn-F Electric Wire Copper Welding Cable[Low Price Marine Grade 5083 Aluminum Alloy Aluminium Steel Plate]

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22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /High Quality Electric Hydraulic Lift with Ce Certification, Good Price for Sc200 /200construction Lift-composite.Polymer. 2005; 46(6):1949-1955.2019 PU Leather Sling Cross Body Lady Handbag[Modern Nail Salon Reception Desk]

Received: September 7, 2011
Revised: January 3, 2013

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