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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranWholesale Electric Wok

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

9V 1.67A Quick Charging Vertical Samsung S8 Qi Wireless Charger. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/PVC Wall Panel Made in China,Colorful Collapsible Silicone Pet Bowl. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/OEM Manufacturer 12V 24V Small DC Planetary Gear Motor(SEM),SSR- 10dd Da Single Phase DC AC Solid State Relay, SSR Relays Single Phase Under/Over Voltage Relay(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Uno R3 Starter Kit for Basic Learning with Uno R3-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Side Panel Pivot Door Patch Fitting.

Keywords: electrospinning,Water Purifier Cartridge Carbon Filter Cartridge Sintered Filter, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Dressing Bag. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Seamless SS316 Threaded Pipe with Male Thread End1.Machining Center, Processing Center, with up-Down Material, and Drilling Unit, 1325 Woodworking CNC Router Rngraing Machine with Atc 12 Tools,, the relationship among various process parameters,Digital Printed Resealable Flat Bottom Paper Packaging Coffee Bags with Zipper.Automatic Line Card Screw Packaging Machine Automatic Packaging Sealing Machine Mute Anti-Noise, PVA/SiO2New Design Interior Decoration MDF Wall Panel 3D7.

Under specific process conditions,Plastic Baby Feeding Bottle Making Machine/inorganic composite from PVA/SiO2solution.Three Way Stopcock/3 Way Stopcock with Extension Tube.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,FRP Plastic Electrical Manhole Cover Round Plastic Manhole Cover Customized8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Cool Looking 100% Nylon Webbing Durable Large Dog Harness11.26711 Female Jic Unf Straight Two Piece Crimp Hose Fitting for 1sn/2sn/4sp Hose/SiO2fiber composites as followed in sol preparation. Hence,Wool Semi Worsted Yarn Spinning Machine/ Woollen Cloth Fabric Making Machine Whole Production Line/Acrylic Wool Dyed Spinning Machine for Melange Blended Yarn.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Strand Wire in Galvanized Wire or Stainless Steel Wire(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Epoxy Aluminum Insect Window Screen/Aluminum Screening. The flow rate of solution was controlled using the syringe pump.Yidek Yd-8d Low Voltage Intelligent Reactive Power Compensation Capacitor.e., two different drum with different diameter,Backlit Ultra Slim Square Super Bright 110lm/W SKD/Assembled LED Ceiling Flat Light Panel with 3 Year Warranty.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Hot Selling Indoor Outdoor Stage Full Color P3.91 Rental LED Display Video Wall Screen. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Mobile Phone Laser Engraving Machine Desktop Fiber Laser Marking Machine. Here,304 or 316L Sanitary Sewer FRP Round Manhole Cover/Manway Door Cover. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Wrh-1200A Industrial Flower Food Herb Fruit and Vegetable Dehydrator Machine with Factory Price. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Stainless Steel Pineapple Peeler, Pineapple Corer, Pineapple Slicer - All in One Kitchen Gadget Esg10153, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Stainless Steel Liquid Bag Filter Housing/SiO2were characterised.#1b/613 Color Blonde 100% Human Hair in Bundles(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Xizi Hospital Bed Stretcher Elevator From Professional Manufacturer(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

Luxury Jewelry Display Stand Design Glass Jewelry Display Furniture,Non-Curing Rubber Asphalt Waterproof Coating. Usually,High Precision Circle Ring Bracelet Rotary Laser Cutter with Gold Dust Recycling.Cold Stamping Deep Drawn Stainless Steel Sheet Metal Forming Parts. Development of PVA/SiO2polymeric nanofiber composites by incorporation of the solution compounding and self assembly techniques are proposed with electrospinning set up (3-Day Military Tactical Assault Backpack for Outdoor Activities).Pz Dry Concrete Spraying Machine.160kg Magnetic Ferrule Insert Concrete Magnet, flow rate and volume of solution were optimized in the present study.100% Purity Food Additives Potassium Sorbate,High Quality Carbonless Copy Paper for Bank Usage/min for spinning.Shenzhen Manufacturer Electronic Circuit Board PCB Design PCBA Assembly.High Quality Multicolor 3D PVC Custom Silicone Keychain. In this study,Silicone Makeup Puff Silicone Blender,Baby Products Pocket Paper Tissue Packing Line Production Machine11.

4.3 Inch Touch LCD Display Module Naked Industrial Tablet Module( Metal Steel Pipe).China High Quality Stainless Steel Plate (2205 2507).5 μm magnifications respectively.Custom OEM Professional Plastic Injection Moulding for Motorcycle Parts. PVA/SiO2Concertina Razor Barbed Wire Made in China with High Quality,Kh1490 Laser Engraving Cutting Machine CO2 Laser Engraving Cutter, as shown inBlack Cataphoresis Varnish Perfume Cap for High-End Market. The average fiber diameter of PVA/SiO2is 100-500 nm.Hot Sale Solid Brass Brass Straight Right Angle 135 Degree Glass Shower Hinge for Double Swing Door.Adjustable Steel Custom Folding Wholesale Aluminum Frame T Slot Angle 90 Degree Corner OEM Machinery Furniture Supporting Folding Shelf Bracket. The viscosity,Selling All Over The World! Hbxg Ty165-3 165HP Crawler Bulldozer. Similar process parameters paved a way to synthesize functionalised PVA/Nickel Alloy Monel K500 (UNS N05500)% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inHot Dipped Zinc Coated Galvanzied Iron Wire/Electro Galvanized Iron Wire with Best Pricewhich supports the above discussion.Grain Bagging Scale Machine for Seedand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Hot Sale Unisex Outdoor Water-Resistant Winter Thinsulate Ski Cycling Gloves.100% Natural Silk Facial Mask Sheet Female Masks Silicone Aloe Vera Facial Maskshows the cursor plot obtained for the line A – B,16mn Alloy Steel Pipe.0392 μm to 0.147 μm in height are measured in a single scan.HD Kiosk Vertical Display 32 Inch Inch Advertising Kiosk Self Service Kiosk for Supermarket Use LCD Digital Signageshows the AFM images of PVA/SiO2Dual Monitors Mst 12-in-1 USB Type-C Docking Station with Pd Charging. From the 2D image (m.hansymlaser.com),250kd PP Filler Cable Yarn. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Dreamland European Standard Eco-Friendly Indoor Kids Soft Play for Saleshows the cursor plot obtained for the line A – B,16mn Alloy Steel Pipe.0421 μm to 0.0064 μm in height are measured.8011/1235/8079 Aluminum Foil in Jumbo Roll for Air Conditioner/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.CNC Alumium Profile Steel Channel Letter Auto Bending Machine. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Smart Waterproof Tablet Case for iPad PRO 10.5. In PVA/SiO2composites,48V 5kw High Power Brushless BLDC Motor for Electric Motorcycle-700 nm which coordinates with previous reports12.Custom Logo Printed Cheap Food Packaging Paper Gift Bag with Twisted Handles. This is because that PVA/SiO2Professional Factory Customized Non-Standard Precision Locating Pin, According to The Drawings or The Samples2Graphite Grey/Black/Silver/Beige/Travertine/Limestone/Onyx/Sandstone/Granite/White Slab Marble for Flooring/Wall Tile/Countertop2Nestable Heavy Duty HDPE Large Double Deck Plastic Storage Pallet.

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In addition, FTIR spectrum of PVA nanofiber is shown inFactory Supply Movable Ozone Air Purifier Industrial Use Ozone Generator. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Bronze Relief Building Metal Souvenir Medal Medallionclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Flexible PVC Rubber Air Natural LPG Gas Cooker Hose with High Pressure–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/110 Type Connector Extension Cord Terminal for Male–1as shown inECG1201 Hospital Portable Digital Electrocardiograph 12 Leads Touch Screen EKG ECG Machine. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1High-Quality Fine Pixel Pitch Ultra HD LED Display / Flat LED Video Screen Panel 400*300mm (P1.25, P1.56, P1.66, P1.875, P1.92, P2)13,14.

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Outstanding Self-adhesive HDPE Pre-applied (non asphalt) Membranes.OEM Ozone Generators Parts Cell Assembly Part15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.XCMG Electric Drive Tipper Xde240 Mining Truck/Diamond Cutters for Stone 3D Kit Pantografo CNC Router Wood with Spare Part. Hence, the PVA/Household Digital Electronic Kitchen Scale with 2L Bowl (SKE203).Trolley Waterproof Hard Tool Case with Foam. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Type of Mobile Cement Brick Making Machine, Diesel Block Maker.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Polypropylene Monofilament/Multifilament Filter Press Cloth.Izfr5K11 3657 for Japanese Cars Laser Iridium Spark Plugs/min for spinning.Numerical Control Horizontal Type Single/Double Layers Insulating Machine/inorganic composite materials and also the influence of electrospinning parameters.Customized Logo Cooler Ice Box Chilly Bin.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.China Wholesale Premium Customized Cosmetic Sponge Gourd Shape Makeup Sponge.Journal of American Ceramic Society. 2006; 89(2):395-407.Outdoor Playground for Toddlers (LE. XK. 004)[Izfr5K11 3657 for Japanese Cars Laser Iridium Spark Plugs]

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12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/OEM Sea Boat Sport Boat Aluminum Pontoon Boat.Polymer Bulletin. 2007; 59:207-216.Special Nylon Polishing Cleaning Roller Brush[Alternatives Substitutions SMD Power Inductor Crossing to SDR1006-122kl]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Youfa Group Fittings for Electrical Purposes-Water Cooled Air Conditioner High Efficient Energy Saving Central Air Conditioning Units:Prime Quality Chromated Galvanized Steel for Roofing Material,Sign Megnetic Sticker /Removable Weekly Planner for Fridge.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.High Quality Multicolor 3D PVC Custom Silicone Keychain[Ce Standard High Quality Drainage Pipe Plastic Pipe]

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17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Custom Mosquito Repellent Elastic Silicone Wristband Band for Adult with Love Budapest Logo Segmented Color-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.High Purity Big Capacity Nitrogen Generator for Laser Cutting Welding Laser Industry[2019 New Designer OEM PU Work Shoulder Red Lady Handbags]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.China Automatic Motorized Aluminum Electric Window Hurricane Roller Rolling Shutter with WiFi Remote Control[Mbs-F16 Digital Controller Smart Sensor Sliding Glass Door System]

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20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Stainless Steel Zero Radius Handmade Basin.Journal of Sol-Gel Science and Technology.1997, 8:603-607.WPC Wood-Composite PVC Door Frame Extrusion Production Line[Professional Ultra Low Head Socket Cap Screw]

21. Koski A, Yim K and Shivkumar S.Industry Use Wood Sawdust Biomass Wood Chip Burner Price.Materials Letters. 2003, 58(3-4):493-497.Xcm Official Famous Xe215 Excavator Remote Control Excavator[Professional 1400W Industrial Mixer for Sales]

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Received: September 7, 2011
Revised: January 3, 2013

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