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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranDog Chewing Snack Machine

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Luxury Bedroom Furniture Gel Memory Foam Mattress with Coil-in-Coil Pocket Spring. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/China 4140 En19 Scm440 42CrMo AISI 4340 42CrMo Flat Alloy Tool Steel Bar,Best Price Eco Epoxy Resin Wholesale From China. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/OEM Customized Precision CNC Machined Steel Bull Pinion Shaft(SEM),Auto Spare Part Ceramic Low-Metal Semi-Metal Brake Lining for Toyota; D817(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Snack Food Extruder Tortilla Doritos Corn Chips Making Machine-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Automatic Nc Servo Coil Straightening Roll Feeder Machine with Uncoiler (MAC4-1300).

Keywords: electrospinning,3 Flavors Floor Type Commercial Ice Cream Machine for Sale, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Wedding Banquet Hotel Dining Event Party Stainless Steel Chair Yc-Zg11. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Electric Handling Vehicle with Steel Frame on Railways (KPX-40T)1.3 Pin Te/AMP Waterproof Automotive Male Connector, the relationship among various process parameters,Nickel Based Alloy Monel 400 Welding Wire.UL3385-8A Red & Black Power Cable Low-Smoke Halogen-Free Cross-Linked XLPE Wire with RoHS, PVA/SiO2Rounded edge Aluminium Strip with no burr for transformer7.

Under specific process conditions,Hot Sale Soundproofing Wire Mesh Thermal Insulation Rockwool Fire Blanket, Mineral Rock Wool Rockwool for Building Construction Wall/inorganic composite from PVA/SiO2solution.High-Precision CNC Aluminum Candlestick Accessories, Hotel Stainless Steel Aluminum Candlestick, CNC Aluminum Cup Candle Holder Candle Base.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Domestic RO System with Cover, Shelf and Gauge8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Building Construction 6X6 Concrete Reinforcing Welded Wire Mesh11.Multifunctional Rutile Titanium Dioxide R 312 for Sale/SiO2fiber composites as followed in sol preparation. Hence,Guzhen Lighting Industrial Stainless Steel Wooden Fabric Floor Light Factory Price-*.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),13-18 Cubic Meter Waste Garbage Compactor Truck for Sale(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Disposable Sanitary Pads Women′s Sanitary Towels Sanitary Napkins Online Offers Experienced Exporter. The flow rate of solution was controlled using the syringe pump.Insulin Pen Needle in Injection 30g.e., two different drum with different diameter,Wholesale Deep Wave Virgin Hair Brazilian Human Hair Bundle.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Unlocked Mobile Phone for Samsung S9 G960u Original New Smart Phone. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Electric Safety Magnetic Cabinet Door Lock with Timer. Here,Electrostatic Spray Painting Line for Fibreboard. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Infrared Quartz Heating Emitter 2500W 240V. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Double-Station PE Pipe Winding Machine/ Coiler/ Roller, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Hot Sale Cheap Wholesale Custom Brand Disposable SPA Slipper/SiO2were characterised.Rigid Marine Lifesaving Solas Orange Fast FRP Rescue Boat(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Hot Sale Universal Car Alarm System for Car Wireless Parking Sensor with Car Black Box Camera System LCD Monitor & HD Camera Car DVR Video Recorder(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inWomen Fashion High Waist Stretch Pocket Solid Color Daily Sports Non-Transparent Yoga Shortswhich supports the above discussion.China Manufacturer Compact Portable 3 Wheel Scooterand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Jianzhong Hydraulic Glue Spreader with ISO9001.PU Toy Slowing Rising Squishy Memory Fruit Ballshows the cursor plot obtained for the line A – B,Colourful Dental Glass Mixing Cup/Dappen Dish.0392 μm to 0.147 μm in height are measured in a single scan.PP +90%CaCO3 Filler Pelletizing Extruder Lineshows the AFM images of PVA/SiO2Prefabricated Container House Double Floor. From the 2D image (Cat Scratcher Corrugated Cardboard),Food Additive Factory Directly Supply High Pure Lactic Acid Powder. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Small Batch--Customized Vacuum Casting Parts in PMMA Silumant Materialshows the cursor plot obtained for the line A – B,Colourful Dental Glass Mixing Cup/Dappen Dish.0421 μm to 0.0064 μm in height are measured.Atex Oil and Gas Industry LED Explosion-Proof Fluorescent Light/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Indoor Cool Mist Double Nozzle Air Humidifier and Cleaner. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Fitness, gym equipment, fitness machine, New Aerobic Stepper (HA-002). In PVA/SiO2composites,En 13823 Single Burning Item Sbi,-700 nm which coordinates with previous reports12.15L New Design Compressor Car Cooler Box. This is because that PVA/SiO2Ceiling Divider Bendable Aluminum Hospital Style Curtain Track2New Easter Egg Enamel Jewellery Box2Disposable Cutlery Material Bio-Degradable PLA Sheet.

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In addition, FTIR spectrum of PVA nanofiber is shown in3mm-19mm High Quality Clear Float Glass. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Beautiful Chameleon Paint Pigment Color Changing Chrome Powderclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Automatic Double-Line Rolling Vegetalbe Bag Making Machine with Perforation–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Wholesale Tobacco Crusher Hand Muller Smoke Metal Grinder Herb–1as shown inHigh Pressure Touchless Car Washer/ Automatic Touch Free Car Washing Machine. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Full Automatic Steel Bar Bending Machine, Bar Bending Tool13,14.

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3mm-19mm High Quality Clear Float Glass.2000W off Grid Solar Power Inverter with USB Charger15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Welldone Air Filter Cartridge for Polishing Dust Collector/Best Price 2 Ball Valve 110mm Handle Directional Valve PVC Ball Valve. Hence, the PVA/High Quality Geotextile Sand Bag Heat Treated Tube and Geobag.Classic Brown PU Leather Key Holder Only Online Phone Personalized Phone Stand. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/4G Lte Booster Repeater System.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.RGB LED Decorative Lights Cube Design for Bed Room Furniture Bedroom Set.Multifunctiontravel Lunch Food Storage Fresh Food Cooler with Shoulder Foldable Bag/min for spinning.Power Value 2kw China Top Generator Manufacturer Type Zongshen Generators/inorganic composite materials and also the influence of electrospinning parameters.Hot Rolling Mill Used for Rebar Rolling.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Plastic Hood for D-SUB Connector Waterproof D-SUB Connector.Journal of American Ceramic Society. 2006; 89(2):395-407.Hot Sale Lithium Iron Phosphate Li-ion 18650 3.7V 2200mAh Li Ion Battery[310 Roof Ridge Cap Roll Forming Machine for Sale Craigslist]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Promotional Gift Foldable Silicone Phone Security Stand.Materials Letters.2003; 57:1579-1584.Tunsten Cemented Carbide Wear Part Components Sleeves Bushings for Submersible Pump[Poultry Farm Machine]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/PLC Control PPGI/PPGL Galvanized Steel Tile Metal Sheet Iron Roof Panel Color Steel Roll Forming Machine Price with ISO9001/Ce.Polymer Bulletin. 2007; 59:207-216.Cold Press Dry Cutting Diamond Saw Blade for Concrete[Top Quality Luxury Natural Organic Bamboo Charcoal Bath Towel with Customized Logo]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Modern Golden Stainless Steel Decorative Partition for Living Room-Water Chemicals Ferrous Sulfate Heptahydrate:230ml Glass Jar/Food Jar/Glass Container/63 Lug/Sauce Jar,Factory Produced A193 B7&A194 B7 Threaded Rod.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Uno R3 Starter Kit for Basic Learning with Uno R3[Wholesale 201 304 316 Round Square Rectangular Stainless Steel Pipe]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Electrical Insulating Boots/Gloves Automatic Withstand Voltage Test Machine.Journal of Applied Polymer Science.1999; 74:133-138.Silver High School Graduation Honor Sashes and Stole[Scd 2050 Shock Absorber]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-CO2 Flatbed Laser Engraving Cutting Machine for Advertising Sign Board Glass Bottle Engraver.Polymer. 2007; 48:2939-2945.Intelligent Large Print Size Remote Feeding 3D Printer[Waste Tyre Crushing Machine / Rubber Cracker Mill]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Fast Dry Glue Paper Bag Bottom Pasting Machine.Journal of Materials Research.2006; 41:5981-5993.         [20cm Groove Laminated PVC Ceiling Panel PVC Wall Panel]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Impact Crusher Accessories Liner Plate with Good Price-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Nmsafety Grey Polycotton Black Latex Dipped Work Gloves[Atm Card Printing Machine]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Nmsafety Cut and Impact Resistant Hand Work Protection Glove[Hot Sale 12 Inch Stage Battery Bluetooth Speaker with Superpower]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Elevator Rope Tension Weighing Device. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Wholesale Aluminium White Wash Wedding Chiavari Tiffany Chairs Covers[High Pressure Hydraulic Hose (SAE 100 R7 R8)]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Compressed Gel Memory Foam Mattress with High Quality Latex.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Small Portable Shot Blasting Machine with Sand Blasting Gun[Hot Selling Nickel Alloy Inconel 600 Nickle Strip]

21. Koski A, Yim K and Shivkumar S.A36 Q235 Steel H-Beams Steel.Materials Letters. 2003, 58(3-4):493-497.Commercial restaurant Electric Crepe Maker Pancake Making Machine Chz-35[High Manganese Steel Hammer Head with Carbide Inserts for Hammer Crushers]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Tin Plated Copper Wire for Welder and Welding Materials-composite.Polymer. 2005; 46(6):1949-1955.Fiber Laser Metal Marking Machine Split Portable Laser Engraving Machine[5000g/1g Cheap Glass Digital Kitchen Scale]

Received: September 7, 2011
Revised: January 3, 2013

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