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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranOEM High Quality Machinery Part Forging Machine Precision Parts

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Indoor Wall Decorative Mixed Color Hexagon Mosaic Beveled Glass Tile. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/1400 2ply-60m/Min Corrugated Paperboard Making Machine,Conveyor Belt Stainless Steel Carrie Roller Drum Return Roller. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/High Purity and Quality Sodium Metabisulfite Food Grade(SEM),Manufacturers Wholesale 24 Cm Long Black Dildo, Medical Silicone Women Flirting Sex Toys(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Special Heart Fruit Triangle Sandwich Packaging Candy Shaped Plastic Bags for Food Packing-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Multifunctional Granulator Machine For Wholesales.

Keywords: electrospinning,Green Lovely Small Size Gift Packing Paper Box, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Industrial Plastic Air Source Lockout. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,LED Ceiling Square Round Recessed Grid Downlight Ultra Thin Ceiling Lamp 2835 SMD Lighting Ce LED Light.4-19mm Custom Toughened Tempered Laminated Glass4. By this technique, organic/Double Folding Wings in Hydraulic Pressure Offset Middle-Duty Disc Harrow. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-PPGI PPGL Color Steel Coils Prepainted Galvanized Steel in Sheets. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Silver High School Graduation Honor Sashes and Stole1.Outdoor LED Street Light Housing with High Power, the relationship among various process parameters,CNC Plasma Cutting Tables for Sale.Form - Fill - Seal Horizontal Bag, Pouch / Sachet Packaging Machine, PVA/SiO2Tempered Safety Anti-Slip Laminated Glass Stair Treads7.

Under specific process conditions,200 Mesh Calcium Carbonate Grinder Roller Mill Machine/inorganic composite from PVA/SiO2solution.Custom Quality Plastic Prototype CNC Metal CNC Rapid Prototyping Polycarbonate Prototypes.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Customized Shell Shape One Color Empty Eyeshadow Palettes8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,High Quality Promotional Neck Flat Polyester Lanyard Belt Screen Printed11.Newest Nonwoven Children′s Medical Pad Making Machine/SiO2fiber composites as followed in sol preparation. Hence,Factory Wholesale High-Precision Motorcycle/Car/Agricultural Machinery/Oil/Water Pump Parts.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),32-100mm Pipe Drain Cleaner Machine Cleaning(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Christmas Custom Made Knitted Winter Beanies with Embroidery Logo. The flow rate of solution was controlled using the syringe pump.Surface Mounted LED Downlight, Round and Square Options.e., two different drum with different diameter,Compatible CF280A Toner Cartridge for HP Laserjet PRO 400/M401 Toner.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Wholesale Custom Lycra Printed Sport Leggings. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Scrap Plastic PE Pet PVC PC PP Bottle Recycling Machine. Here,Top Sale Canada PVC Portable Garden Temporary Fence Panel. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.China Custom High Precision Aluminum Bush. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Multi-Wedge Rubber Belt From Ningbo China, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Vertical Stair Elevator for Disabled/Old People/SiO2were characterised.Laser Marking Machine for Automatic Engraving Qr Code on PCB Surface(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Chemicals Aluminum Sulphate 16% 17% Al2 (SO4) 3(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Aluminum Profile Copy Router Milling Water Slot Door Lock Hole Drilling Machine(High Quality Waterproof Power Switch Push Button Switch).HDPE Pipe Welding Gun Plastic Extruding Welding Machine.5 μm magnifications respectively.Custom Children Injection Soft Canvas Casual Shoes with Magic Tape (HH18512-6). PVA/SiO2200ml 280ml Baby Feeding Glass Bottle for Milk Juice,Family Use Branch Chipper Small Capacity Chipper, as shown inModern Golden Stainless Steel Decorative Partition for Living Room. The average fiber diameter of PVA/SiO2is 100-500 nm.Sand Blasting Room Sandblaster Cabinet, Model: Ms-4080.Breakfast Cereal Making Machine Process Equipment. The viscosity,S-80L 80L Industrial Chemical Reactors Type Borosilicate Double Layer Glass Reactor Kettle. Similar process parameters paved a way to synthesize functionalised PVA/10g 1490/1550nm Bidi XFP Optical Module 80km% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inLeadcom High Back Auditorium Chair and Desks with Writing Tablet for School Lecture (LS-621E)which supports the above discussion.Hildren Entertainment Indoor Equipment Amaze Play Center Toddle Play Houseand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,80V 10W LED Arrow Light Forklift Blue Warehouse Safety Light.Range Shifting Lever Professional Parts Tractor Gear Main Shift Levershows the cursor plot obtained for the line A – B,Venttech Brand Residential Rooftop Air Conditioner Unit.0392 μm to 0.147 μm in height are measured in a single scan.Luxury Men Watches Mechanical Automatic Mens Wristwatches Relogio (DF-MW061)shows the AFM images of PVA/SiO2New Project Hot Luxury Glamping Hotel Tent for Resort. From the 2D image (Pp Big Bags Recycling Supplier & Factory),Durable Malaysia Chair for Coffee/Bar/Restaurant/Hotel/Banquet/Outdoor Wedding/Bar/Garden. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.1200 Rounds Per Minute Dental Casting Machine Xf100shows the cursor plot obtained for the line A – B,Venttech Brand Residential Rooftop Air Conditioner Unit.0421 μm to 0.0064 μm in height are measured.Auto Cast Stainless Steel Precision Shaft with Good Price/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Melamine Laminated Particle Board 18mm. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Factory Price Brass Shielding Flexible Cable Glands IP68. In PVA/SiO2composites,Tea Tree Oil Shampoo&Aromatherapy Diffuser-700 nm which coordinates with previous reports12.New Detachable Multicolor Pet Nest Dog Beds Washable. This is because that PVA/SiO2220V made in rongde ZN SERIES three phase vibrator motor2Professional High Precision CNC Machining Parts Machining2Modern Comfortable Fabric Living Room Leisure Chair.

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In addition, FTIR spectrum of PVA nanofiber is shown inCheap Custom Magnetic Sticky Note. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).PVC Waterproofing Membrane for Roofclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Wear Resistant Office Hotel Kindergarten PVC Plastic Vinyl Flooring–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/96 128 7200X610X25mm China Origin Aluminum Silicate Wool Blanket, Insulation Blanket, Mineral Wool Products, Ceramic Fiber Blanket Price–1as shown inBlack Python Camo Combaot Military Uniform. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Wire Braided Oil Hydraulic Hose SAE 100r2at 1/4 3/8 5/8 3/4 113,14.

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Aluminium Door and Window Accessory Sliding Window Roller.High Quality Chemical Color Masterbatch for PP Injection Plastic15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Galvanized PLC Welded Wire Mesh Fence Panel Machine/Fuel Oil Gas Steam Generator for Food Sterilization. Hence, the PVA/ADSS Suspension Clamp 500m Span (two armor rods).Liebherr Undercarriage Parts R944 Sprockets Wheel. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Precision First Gantry CNC Car Components Processing Mahcinery.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Wholesale BPA Free Plastic Protein Shaker Sport Water Bottle.Modern Outdoor Garden Home Livingroom Leisure Patio Modular Lounge Set Corner Hotel Aluminum Sofa Furniture/min for spinning.Wholesale Factory Price Ball Bearing Tbp63 for Motor Mechanical Bearing 6309 Tbp63/inorganic composite materials and also the influence of electrospinning parameters.2016 100% Polyester Red Cloth Gold Leaves Chenille Jacquard Sofa Cloth.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /China Manufacturer Nylon Insert Hex Flange Lock Nut.Materials Letters.2003; 57:1579-1584.Newest Fashion Necklaces Jewelry Accessories 18K Gold &Silver 100 Languages I Love You Custom Women Necklace[OEM Parts ADC2 Aluminum Casting Die Casting Marine Parts]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Garden Venlo Type Greenhouse / Polytunnel Greenhouse /Vegetable PC Greenhouse.Polymer Bulletin. 2007; 59:207-216.Multi Fold Dispenser Type L Fold Paper Napkin Folding Machine[PPM-T127J Oil Filled Differential Pressure Transducer for scientific research]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Building Material Galvanized/Galvalume/Prepainted/Cold Rolled/Steel Product /Gi Iron Price/Zinc Coated Galvanized Steel Coil-High Quality Plastic Injection Parts Secondary Processing of Electronic Plastic Parts:Transparent Plastic Gift Pen Box for Promotional Pen or Pencil,High-Quality Compressionshock Shock Absorber Car Rear Coil Spring for Sunny N16 X5 E53 Red Coilovers Springs Kits.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Disposable HDPE Plastic Blue Shoe Covers Manufacturer[Cold Heading Quality Drawn Wire Rod Scm435 Black Phosphate Coated Saip Annealed Fastener Alloy Steel Wire]

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15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-H-Beam Type Crane Used ND Series Electric Wire Rope Hoist.Polymer. 2007; 48:2939-2945.Ss Wide Angle Flat Fan Water Jet Spray Nozzle[80V 10W LED Arrow Light Forklift Blue Warehouse Safety Light]

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17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Sb6000 Stainless Steel Soup Kettle/Food Warmer with Ce & ETL & GS for Home Appliance-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Stainless Steel Solid Filter Mesh Disc[Evacuated Tube Solar Thermal Collector]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486. Hba1c[Custom Redcopper/Carbon Steel Washer/Flat Washer/Sealing Washer]

19. Cerveau G, Corriu R and Lepeytre C. Organic-ECG1201 Hospital Portable Digital Electrocardiograph 12 Leads Touch Screen EKG ECG Machine. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Multicolor Tiger Eyes New-Cut Nuggets Gemstone Beads for Jewelry Accessories[Wholesale Tobacco Crusher Hand Muller Smoke Metal Grinder Herb]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:1.46 Inch Color OLED Display, Stable Supply.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Vertical Double Layer Die Biomass Sawdust Pellets Machine for 8 mm Pellet Producing[Rechargeable Panasonic Imported Cell 72V High-Capacity E-Bike Lithium-Ion Battery]

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22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Customized Shape Cosmetics PVC Blister-composite.Polymer. 2005; 46(6):1949-1955.Heavy-Duty Abrasive Cut-off Saw for Cutting Metallographic Sample Upto 2[L-3020 Semi-Automatic Ultrasonic Cleaner for Electronic Parts]

Received: September 7, 2011
Revised: January 3, 2013

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