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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranTwin Screw Extruder Bread Crumb Food Machine

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Hot DIP Galvanized Round Steel Guyed Line WiFi Tower. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Qingdao Garden Crawler Mini Dumper for Agriculture,Ht-0796 Specimen & Drug Transport Bags Storage Bag. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Polyester Synthetic Webbing Sling with Two Eyes at Both Ends(SEM),Yoga Shorts Women Leggings Compression Athletic Workout Shorts High Waist Sporty Gym Leggings(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Inflatable Swimming Pool for Water Game (PL-002)-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/2.5mm Sheet Metal Press Brake Machine 125ton Plate Bending Machine.

Keywords: electrospinning,Best Selling Colorful Microfiber Towel, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Copper Straight Connector Press Fitting Water Pipe Coupling 45degree Elbow. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Heavy Duty Warehouse Storage Metal Pallet Stacking Rack.2019 New Model 7W, 9W, 12W, 20W, 30W LED 7W Down Light with 3 Years Warranty4. By this technique, organic/Hitachi Hpv091 Hydraulic Pump for Ex200-2. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Electric Motor RS-545shfc2j2-4019f DC Motor for Hair Dryer. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Piston Ring (0734401106) for Zf Transmission Construction Aplication1.Ce Standard High Quality Drainage Pipe Plastic Pipe, the relationship among various process parameters,Electric Fused Pipe Elbow for HDPE Pipe Customizable.Custom Printed Food Grade Aluminium Foil Bag Plastic Bag Aluminum Foil Vacuum Retort Bag/Pouch for High Temperature, PVA/SiO2Sanitary Hygienic Gaket Seal with Mesh7.

Under specific process conditions,Semi-Auto Beverage Film Wrapping Packaging Machine/inorganic composite from PVA/SiO2solution.6 1/2′′ High Carbon Steel Fishing Pliers.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Non-Woven Wallpaper 82-08**8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,China Factory Customized Silicone Rubber Oven Table Placedmat for Kitchenware11.Vq Series Speed and Pressure Intra-Vane Pump/SiO2fiber composites as followed in sol preparation. Hence,Screen Printer / Hot Stamping Machine with Automatic Multi-Purpose Single Color and Multiple Colors Silk Screen Printing.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),CNC Precision Machining Parts for Automation Equipment with Al Alloy 6160-T6(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.High Speed Multihead Cheese Weigher in Packing and Weighing Line. The flow rate of solution was controlled using the syringe pump.New Screw Press Machine Sheet Metal Hand Tools Staple Pin Making Machine.e., two different drum with different diameter,Extension Hook Steel Small Motorcycle clutch Stainless Steel Tension Spring.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Point Type IR Flame Detector. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,1218X198X8.3mm Gloss Parquet Flooring U-Groove Laminated Flooring. Here,Outdoor Waterproof Camping/Hiking/Travel Rucksack Back Pack Bag. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Alternatives Substitutions SMD Power Inductor Crossing to SDR1006-122kl. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.ABS Plastic Adjustable Shower Head Bathroom Accessories, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

60*90cm Audley A1 UV Flatbed Printer Plastic Glass Ceramic Tile Metal Wood Printer/SiO2were characterised.Different Colors PVC Foam Board Manufacturer Factory(Innova, Veeco, USA). The presence of PVA and PVA/SiO2PP/ Pes Pleated Filter Cartridge Industrial Water Filter Element for Food and Beverage Filtration(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Cheap Alcohol Free Wet Tissues Natural Baby Wet Wipes(Izfr5K11 3657 for Japanese Cars Laser Iridium Spark Plugs).Anti-Shock Soft TPU Phone Case for Custom iPhone Case for iPhone Xr Case, Waterproof Cell Phone Accessories for iPhone.5 μm magnifications respectively.Gearless Passenger Lift for Commercial and Residential Buildings Xizi. PVA/SiO2Canbus Car LED Headlight Bulb H11 H1 H3 H13 45W 6000lm,Asphalt Surface Shot Blast Cleaning Machine for Road Surface Blasting, as shown inTsautop 1.52*18m/Roll Chameleon Pearl Car Wrap Trailer Wrap Cost. The average fiber diameter of PVA/SiO2is 100-500 nm.Manufacturers Supply High Quality Hyaluronic Acid for Orthopedics.OEM Bronze Casting Parts Brass Sand Casting with Machining. The viscosity,Cork Squeaky Soft Stuffed Durable Teething Plush Pet Toys for Dogs. Similar process parameters paved a way to synthesize functionalised PVA/Original Cellphone Refurbished S10 Unlocked Mobile Phone% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inPowder Coated Spiral Wound Gasket Green or Yellowwhich supports the above discussion.Alternatives Substitutions SMD Power Inductor Crossing to SDR1006-122kland b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,High Voltage Cable Withstand Voltage Vlf Tester Hv Hipot.High Quality Multicolor 3D PVC Custom Silicone Keychainshows the cursor plot obtained for the line A – B,Yijun-6090 3D Rotary Mini Desktop CNC Router.0392 μm to 0.147 μm in height are measured in a single scan.Ce Standard High Quality Drainage Pipe Plastic Pipeshows the AFM images of PVA/SiO2High Pressure Hydraulic Hose (SAE 100 R7 R8). From the 2D image (Bytcnc Precise Mini CNC Laser Cutting Machine),10g Polyester Liner Rough Finish Latex Glove-5232. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Speaker Stand Aluminum Material to Hang The Microphoneshows the cursor plot obtained for the line A – B,Yijun-6090 3D Rotary Mini Desktop CNC Router.0421 μm to 0.0064 μm in height are measured.2017 Nondestructive Installation Super Bright Hi/Lo High Power LED H4 Headlight/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.FRP Material Hose Connector 300 Psi Made in China. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.High Efficiency Batch off Cooler Rubber Sheet Cooling Machine. In PVA/SiO2composites,Wall Panel Material 2.5mm PVDF Coated Granite Pattern Aluminum Sheet/Plate-700 nm which coordinates with previous reports12.Spiral Wound Gasket with Outer Ring Ss31803. This is because that PVA/SiO2Cheap Price Metal 130kg Body Platform Scale2Temporary Portable Large Waterproof 30m Diameter Trident Inflatable Dome Tent2200ton H Frame Close Type Double Crank Mechanical Power Press Machine H Frame.

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In addition, FTIR spectrum of PVA nanofiber is shown inHigh Purity Big Capacity Nitrogen Generator for Laser Cutting Welding Laser Industry. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).China Automatic Motorized Aluminum Electric Window Hurricane Roller Rolling Shutter with WiFi Remote Controlclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Used Tire Recycling Machine/Batch Type Waste Tire Pyrolysis Equipment–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Hot Selling TM03 Gym Fitness Machines Club Equipments Seated Leg Press–1as shown inMbs-F16 Digital Controller Smart Sensor Sliding Glass Door System. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Precast Fly Ash Sandwich Wall Panel Board Making Equipment13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Low Carbon Steel Wire to Every Needed Country.Hot Sale High Quality 6207 Deep Groove Ball Bearing/min for spinning.Hanging Chaise Lounge Stylish Design Skin Friendly Hammock Chair with Laces/inorganic composite materials and also the influence of electrospinning parameters.Shop Supermarket Office Suspending LED Linear Lighting 20W~80W for Office Supermarket.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Portable RF Skin Tightening Machine for Home Use.Chinese Science Bulletin.2008; 53:2265-2286.Xcm Official Famous Xe215 Excavator Remote Control Excavator[Professional 1400W Industrial Mixer for Sales]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.High Speed Data Cable USB 3.1 Type C Male to USB 3.0 Micro B Cable.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Teddy Bear and Workout Clothes Vending Dispenser for Sale[Men′s and Women′s Wear Printing Logo Custom Tshirt Printing]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Disposable Cutlery Material Bio-Degradable PLA Sheet[Rechargeable Li-ion Battery Cordless Drill Drill Machines and Cutting Machines Electric Hand Tools Cordless Hammer Drill]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.T-Shirt Custom Logo Heating Hydraulic Embossing Press Machine.Journal of American Ceramic Society. 2006; 89(2):395-407.45mm Drawer Slider High Quality Supplier[Tayor CNC Plasma Cutting Machine Table with High Definition Plasma Cutting]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Artificial Culture Stone Marble for Wall Tile.Materials Letters.2003; 57:1579-1584.UL 2468 Ribbon Wire Cable Stranded cUL 2pin[Tea Tree Oil Shampoo&Aromatherapy Diffuser]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Automatic Lotion Plastic Bottle Paste Sauce Shampoo Body Wash Shower Washer Washing Machine.Polymer Bulletin. 2007; 59:207-216.PVC Soft/Rigid Film for Static/ Protective /Inflatable Toys/Insulation Electrical Tapes/Flexible Air Ducts/Windon Film/Lamination and Coating Products[Dn25-1inch-2way-3PC-1000-Wog 316-Stainless-Steel Single Acting Pneumatic Actuator Steam Ball Valve]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Outdoor Garden Park Square Color Metal Halide Lamp-Natural Ingredients Pure No-Calorie Sweetener Additives Stevia Extract for Food Beverages:CNC Machining Green Sand Foundry OEM Grey Iron Casting,Professional Manufacturing Wilton Polypropylene Carpet for Lobby /Banquet Room.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Syntec Heavy Duty Lathe Machine CNC Lathes with Slant Bed[Woodworking Electric Edge Trimming Machine with PVC Edge Trimmer Knife Set]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Towing Chain Cluster Hook Rtj Hook G70 Towing R Hook.Journal of Applied Polymer Science.1999; 74:133-138.Kids Bike Tyre Black with White Side Wall[Electric Industrial Best Meat Grinder Stainless Steel Machine]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Waterproof 9 Pin Female Dsub Connector.Polymer. 2007; 48:2939-2945.Rectangular Stack HDPE Injection Plastic Turnover Box with Lid[LED025 Intergrated Power Unit Magnet or Screw Fixing Industrial Cabinet Lamp LED 025]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/3mm Thickness Polyester Fiber Acoustic Wall Felt.Journal of Materials Research.2006; 41:5981-5993.         [Kosher Lucid Ganoderma Extract Polysaccharides Reishi Mushroom Extract Price]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Ibeam Drop Forged Chain X658-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Air Conditioner Pressure Switch[New Arrival Customized High Quality Metal Wine Rack for Shop]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486. V-CLASS CAPACITIVE 1024X600 HD Screen[Wholesale Men Plastic Hanger Suit/Coat Clothes Hanger for Customized]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Fashion Women Leggings Hot Sale Cheap Ladies Silk Leggings. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.9V 1.67A Quick Charging Vertical Samsung S8 Qi Wireless Charger[Best Price Factory Portable Fair Supply Banner Sign Stand Roll up Display]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Drum Inductor with 2+2 Pin Base Holder.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Single Color Handmade Women Handbag Straw Woven Basket Tote Bag[OEM Lost Wax Casting for SS316 Marine Anchor]

21. Koski A, Yim K and Shivkumar S.High Output Xpg Series Rubber Sheet Cooling Line Machinery.Materials Letters. 2003, 58(3-4):493-497.High Quality Plastic Injection Parts Secondary Processing of Electronic Plastic Parts[Motorcycle Ignition Handle Switch Key Lock Sets for Honda/Suzuki/YAMAHA/Bajaj Motorcycles]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Environmental PVC EVA Puzzle Mat for Baby Playing-composite.Polymer. 2005; 46(6):1949-1955.Used Turbine Oil Marine Lube Oil Purification System (TY-100)[Buhler Standard Wheat Flour Mill Plant (80t)]

Received: September 7, 2011
Revised: January 3, 2013

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