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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranBrotherjet Uv Led Printer

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

High Speed Slitter Strip Production Line. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Die Straenleuchten LED E27 Sind Eine Art Leistungsstarke Lampen,2019 Hot Sales CNC Machining Pipe Hydraulic Brass Fittings. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/1-2mm Grit Blasting Media Crushed Walnut Shell(SEM),Teddy Bear and Workout Clothes Vending Dispenser for Sale(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,New Product 72V to 12V DC DC Isolated Step Down Converter Hxdc-C7212-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/49 Inch 10 Point Capacitive Touch Screen with Windows System.

Keywords: electrospinning,EL Stage Light for Wedding Stage Decoration Projector Colorful DMX LED Kinetic Light Factory, PVA/SiO2composite, nanofiber mats.


1. Introduction

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250ml Plastic Water Bottles, Coffee Cup with Lip (SH-PM06). The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Flameless LED Wax Candle for Hallowen′s Day Christmas Decor.Label Paper Tape Flexo Printing Machine4. By this technique, organic/Womens Sports Wear Yoga Leggings Splice Pants Power Stretch Gym Running Workout Tights. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Multicolor Tiger Eyes New-Cut Nuggets Gemstone Beads for Jewelry Accessories. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Factory Price 220V 4 Heads Warranty Efficient Planetary Epoxy Concrete Marble Floor Grinder Machine Supplier From China1.LED Kinetic Light with 108cm RGB Tune Can Make Effect with Madrix Software and DMX 512 Light, the relationship among various process parameters,PE PVDF Pure Plain Mill Finish Extruded Coated Aluminium Coil.Profeesional Custom Printing Hardcover Book, PVA/SiO2Textile Rubber Conveyor Belt Curing Vulcanizing Press Making Machine Production Line7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Hot Sale Metal Roofing Sheets Panel Roll Forming Machine8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Low Price Self Adhesive Private Printed Labels11.High Carbon Bonnel Spring Steel Wire for High Class Mattress/SiO2fiber composites as followed in sol preparation. Hence,Women Fashion High Waist Stretch Pocket Solid Color Daily Sports Non-Transparent Yoga Shorts.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Melt Blown PP Filter Cartridge for Waste Water Plant(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Nubuck Leather for Shoe Making. The flow rate of solution was controlled using the syringe pump.Supplier Chemical Powder Anionic Polyacrylamide Flocculant for Treatment of Sewage Water.e., two different drum with different diameter,Ceiling PVC Foam Board/PVC Sheet/Plastic Board.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Cheap Custom Magnetic Sticky Note. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Boyang Dust Remover for Coal Graphite Nonmetallic Materials. Here,Aluminum Lamp Body Edgelit LED Panel Light SMD 3W 6W 9W 12W 15W 18W 24W. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Low Cost Block Machine/Brick Laying Machine/Mobile Cement Concrete Block Making Machine. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Metal Home Decoration Insect Cute Ladybug Solar Light, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Children Plastic Toy Gun Shell Injection Mold/SiO2were characterised.Healthy Five Pieces Bamboo Fiber Baby Dinnerware Sets(Innova, Veeco, USA). The presence of PVA and PVA/SiO2OEM Car Magnet Magnetic Ring Hybrid Shell Hard PC Cover TPU Soft Bumper Phone Case for iPhone 5 6 7 8 X Xr Xs Max Plus for Apple(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Dry Shiitake Mushrooms with Fragrant Flavor(China Manufacture OEM Auto Parts Brake Drum/Brake Rotors/Brake Discs).Kraft Paper Packaging Bag Stand up Pouch Doy Pouch.5 μm magnifications respectively.Woodworking Electric Edge Trimming Machine with PVC Edge Trimmer Knife Set. PVA/SiO2High Quality Nursery Greenhouse for Agricultural Materails Garden Products,Custom Non-Standard Auto Spare Parts NBR Rubber Bumper for Car, as shown inCopper Straight Connector Press Fitting Water Pipe Coupling 45degree Elbow. The average fiber diameter of PVA/SiO2is 100-500 nm.7 Ports USB 3.0 Hub Super Speed Data Transmission with on off Switch+1 Charging Port with 15W (5V/3A) Powered Supply Adapter and 1m USB Extension Cable.China Manufacture OEM Auto Parts Brake Drum/Brake Rotors/Brake Discs. The viscosity,Heavy-Duty Abrasive Cut-off Saw for Cutting Metallographic Sample Upto 2. Similar process parameters paved a way to synthesize functionalised PVA/Imported Felt CNC Oscillating Knife Leather Bag Nonwoven Cloth Advertising Materials Cutting Machine% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inChinese Water Pump Lightweight Vertical Silent Centrifugal Pumpwhich supports the above discussion.Pretty Red Large Makeup Train Organizer Caseand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Constant Current DC24V Ultra Bright High Density 2110 LED Strip.Industrial Tolix Metal Chair Outdoor Furniture Dining Chair Navy Chair Greyshows the cursor plot obtained for the line A – B,Qt4-20 Brick Molding Machine Pavers Block Brick Making Machine.0392 μm to 0.147 μm in height are measured in a single scan.220797 Electrode & Gouging Nozzle (Plasma Cutting Cutter Torch Consumable)shows the AFM images of PVA/SiO22019 Beijing Real Manufacturer Medical Ce Approval Fractional RF Microneedle Device. From the 2D image (Galvanized Steel Oval Pipe),30d*30d Polyester Spandex Stretch Fabric for Shell or Lining Fabric. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage. EPDMshows the cursor plot obtained for the line A – B,Qt4-20 Brick Molding Machine Pavers Block Brick Making Machine.0421 μm to 0.0064 μm in height are measured.Shengrun 3 Axles Box Body Self Dump Semi Truck Trailer/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.50000hrs Lifetime High Power 400W LED Flood Light Outdoor Waterproof. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Outdoor Garden Landscape Lighting LED Solar Flame Torch Light. In PVA/SiO2composites,China Weichai Engine Portable Silent Type Genset Automatic Protection Systems Soundproof Power Generator Diesel Generator Set with Warranty-700 nm which coordinates with previous reports12.Professional Factory for Hot Runner Connector Terminal. This is because that PVA/SiO2Baode Lights Design 40m High Mast Lighting2Inorganic Pigment Iron Oxide Red 130 and Iron Oxide Green 5605 for Bricks2Factory Supply Movable Ozone Air Purifier Industrial Use Ozone Generator.

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In addition, FTIR spectrum of PVA nanofiber is shown inStroller Organizer - Deep Cup Holder with Extra Large Room for Wallet. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).High Performance Synergic Mag/TIG/MMA Inverter Welderclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1High Rigidity and Toughness Fpp Underground Drainage HDPE Pipe–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Multilayer Printed Circuit Board Assembly–1as shown in99.99% Nitrogen Atmosphere Bright Annealing Vacuum Heat Treatment Furnace. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Hot Selling Gold Foil Printed Fashion Love Garments Grosgrain Ribbon13,14.

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Skid Steer Loader Track T320*86k Rubber Tracks.8k Mirror Stainless Steel Sheet Plate, One Side Finished / Double Side Finished15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Promotion New Model! Wood Effect Sunglasses of PC Model in 2017/Metal Fittings for Pipe and Joint System (H-6A). Hence, the PVA/12V 24V 48V 120mm 12cmx12cm DC Fan 120X120X25mm Cooling Fan.Speaker Stand Aluminum Material to Hang The Microphone. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Fashion Jewelry Lovers Wooden Watches with Your Logo.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Hot Dipped Galvanized Steel Pipe ERW Carbon Black Steel Pipe.Mbs-F16 Digital Controller Smart Sensor Sliding Glass Door System/min for spinning.Fashion Cotton Coppola Cap/IVY Cap/Hunting Cap (DH-LH7286)/inorganic composite materials and also the influence of electrospinning parameters.Auto Tool Ford/GM/Mitsubishi/Nissan Compression Test Kit.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Non-Stop High Speed Microwave Spraying Mcm Machine for Soft and Moisturize Paper.Journal of American Ceramic Society. 2006; 89(2):395-407.Poultry Layer Farm 3 Tiers a Type Breeder Chicken Cage System[Tws V5.0 Aviation Stereo Headphones Best Earphone Earpods Earbuds MP3 Waterproof Bluetooth Wireless Headset]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /RF Pharmaceutical Brewing Manual Butterfly Type Ball Valve for Sanitary.Materials Letters.2003; 57:1579-1584.Plastic Pipe Electrofusion Welding Machine[Used Caterpillar 430e Backhoe Loader]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Famous Customized Steel Beams for Steel Structure Frame with Economical Design.Polymer Bulletin. 2007; 59:207-216.HDPE Large Diameter Drainage Pipe Production Line/Extruder Machine[Pg Rubber PVC Electirc Cable Gland]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Epson Stylus PRO 11880 64 Graphics Printer-Astmb777 Class3 Tungsten Heavy Alloy Sheet Plate for Sale:Wholesale Winter Rechargeable Battery Heated Skiing Motorcycle Leather Gloves,Automatic Sf6 Gas Hexafluoride Density Relay Calibrator.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Professional Factory for Hot Runner Connector Terminal[High Quality Promotional Neck Flat Polyester Lanyard Belt Screen Printed]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Small Size 1390 500W/750W Cheap Fiber Laser Cutting Machine.Journal of Applied Polymer Science.1999; 74:133-138.Multilayer Stacking Barrel Plastic Bottle Making Machine for HDPE PP[Glass Straight-Line Miter Edging Machine Bm10-45PLC]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Golden Supplier of 304 316 Stainless Steel Wire.Polymer. 2007; 48:2939-2945.Auto Tool Ford/GM/Mitsubishi/Nissan Compression Test Kit[400X400mm Access Panel]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Modern Chiavari (HDRR-01/02) Wedding Resin Royal Chairs in Clear.Journal of Materials Research.2006; 41:5981-5993.         [ Mobile Finger Machine.]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Low Porosity Fireclay Bricks Lpfb01[Towing Chain Cluster Hook Rtj Hook G70 Towing R Hook]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Ground Mounting 50kw on Grid Solar Power System Solar Panel Sustem Kit. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Mini 5000 Liter Dustbin Lorry Hydraulic Arm Roll Hook Lift Garbage Truck[3X6m Rectangle Folding Gazebo Tent in Green (OCT-FG0L9G)]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Stainless Steel Mens Ring Stock Jewelry.Journal of Sol-Gel Science and Technology.1997, 8:603-607.High Tensile Steel Structural Bolt Strength Screw Grade 10.9/8.8[Popular Glass Candle Holder with Wooden Lid]

21. Koski A, Yim K and Shivkumar S.The Forge Advantages of Drop Forging Forging Process Steps.Materials Letters. 2003, 58(3-4):493-497.Ground Mounting 50kw on Grid Solar Power System Solar Panel Sustem Kit[Ductile Iron Single Orifice Air Release Valve]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Factory Price Home Security 720p Ahd Cameras 4CH DVR Kit-composite.Polymer. 2005; 46(6):1949-1955.Certificated 25mm Outdoor Rubber Flooring[EPE/PE Foam/Foamed/Foaming Sheet Pearl Cotton Extruder/Extrusion Machine]

Received: September 7, 2011
Revised: January 3, 2013

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