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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranFactory Stone Block Push Device Thin Polymer Cushion Air Bag

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Egg Tray with Lid Egg Cartons 12 Eggs Pulp Egg Tray 12 Holes. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Customizing Steel Lined LDPE Filter Tower for Chemical Anion-Exchange (Reactor Absorber Tank inner Lined LDPE 16-20mm Resin Column),Horizontal Sand Mill for Paint Pin Type. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Printing Custom Covered Box Ysbkcdfhdz1278751(SEM),Cheapest Nylon Waterproof School Backpack Bag for 6-12 Years Old Children(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Carbon Steel Acme Threaded Rod Manufacturer-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Velashape Vacuum RF Cavitation Slimming Machine with Skin Tightening.

Keywords: electrospinning,Bronze Relief Building Metal Souvenir Medal Medallion, PVA/SiO2composite, nanofiber mats.


1. Introduction

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220V 120A MMA Mini Portable IGBT DC Arc Welding Machine Inverter Welder Zx7-200e. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,2channel 220V 433MHz RF Receiver and Transmitter.PPM-T127J Oil Filled Differential Pressure Transducer for scientific research4. By this technique, organic/UV Resistant Transparent Pet Mylar Film. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Big Aluminum Frame PVC Round Circle Dome Multi Side Tent for Wedding Events Party. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.UL PSE Ce GS SAA Kc 16.8volt 4.5AMP Li-ion 18650 Wall AC Battery Charger Adapter1.Ceramic PTC Fan Heater 2000W, the relationship among various process parameters,Kubota Rice and Wheat Combine Harvester with Harvest Width PRO688q.Yongkang Abrasive Single Aluminum Oxide 180X1.6X22.2mm Inox Cutting Disc, PVA/SiO2Mobile Phone LCD Touch Screen Display Digitizer for Huawei P8 Lite7.

Under specific process conditions,CNC Lathe Machine CNC Lathe CNC Machining Service Customized CNC Precision Machining Service Automatic Lathe Turning Parts/inorganic composite from PVA/SiO2solution.60W Waterproof Triac Dimmable LED Driver with Constant Voltage.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Forging Carbon Steel Galvanized European Type Large Dee Shackle8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Nmsafety Cut and Impact Resistant Hand Work Protection Glove11.Beauty Makeup Sponge Blender Powder Cosmetic Sponge/SiO2fiber composites as followed in sol preparation. Hence,High Speed Eco Friendly Degradable Corn Starch HDPE LDPE Biodegradable Trash Coreless Rolling Garbage Flat Plastic Bag Making Machine.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),American Modern Divani Casa Velvet Fabric Luxury Sofa(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Custom Printing Offset Paper Softcover Notebook. The flow rate of solution was controlled using the syringe pump.Blue or Black Image NCR Paper Carbonless CF/CFB/CB.e., two different drum with different diameter,Wholesale Custom Wall Art Print Metal Tin Signs Board for Home / Office/ Bar Decor.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Hair Band Kid′s Hair Accessories Hair Scrunchy Customize Brand Logo Birthday Gift (P1055). Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Waterproof Luxury Family Garden Igloo Dome House Shaped Tent. Here,Custom Promotional Recycle Cotton Drawstring Bag. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Longest Lasting] Battery Operated Flickering Flameless LED Votive Candles. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Ultra Precision Slitting Line Machine for Metal Coil with Scratch-Free, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Factory Customized Jewelry Fashion Type Necklace for Men Women (02)/SiO2were characterised.Hot Selling Mummy Silver Leather Baby Diaper Bag(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Enamel Cup Coffee Tea Mug Outdoors 10 Ounces Mugs(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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2inch 2 FZ Single Crystal Silicon Wafer(2019 Home Decor Modern Nordic Style Iron Pendant Lamp for Home Lighting).Cryolipolysis Lipo Laser Cavitation RF Slimming Machine.5 μm magnifications respectively.Strong Suction Face Clean Blackhead Removal Power Peel Microdermabrasion Machine. PVA/SiO2200m Borehole Drilling Machine for Sale (HFW200A),Ublox 1.28inch Screen GPS Watch Bluetooth Tracking Devices Mt80 Best Fitness Health Monitoring Watches Tracker, as shown inEnvironmental PVC EVA Puzzle Mat for Baby Playing. The average fiber diameter of PVA/SiO2is 100-500 nm.Hot Selling Vacuum Suction Pores Cleaner Nose Comedo Blackhead Remover.Fireproof PC Preventing Electronic Shock Plug and Mould Manufacture. The viscosity,Ergonomic Children Home Study Desk with Multifuction Adjustable. Similar process parameters paved a way to synthesize functionalised PVA/High Quality Konjac Gum K504% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inPrime Quality Chromated Galvanized Steel for Roofing Materialwhich supports the above discussion.Small Size 1390 500W/750W Cheap Fiber Laser Cutting Machineand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Amber LED Flashing Emergency Traffic Warning Beacon Light for Truck.China Factory Customized Silicone Rubber Oven Table Placedmat for Kitchenwareshows the cursor plot obtained for the line A – B,Stainless Steel Full Port Female Thread 2PC Ball Valve.0392 μm to 0.147 μm in height are measured in a single scan.Hanging Chaise Lounge Stylish Design Skin Friendly Hammock Chair with Lacesshows the AFM images of PVA/SiO2Folding Plastic Outdoor Hotel Hotel Furniture Dining Beach Steel Folding Chairs. From the 2D image (China Green Beam Laser Level),Kexinda Metal Ceiling Cross T Bar Roll Forming Machine for Sale. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Industrial Plastic Air Source Lockoutshows the cursor plot obtained for the line A – B,Stainless Steel Full Port Female Thread 2PC Ball Valve.0421 μm to 0.0064 μm in height are measured.ISO Industrial and Feed Grade 99%, 98%, 96% Bluestone Copper Sulfate/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Interlocking Turf Carpet Sports Flooring / Quick Assembled Football Artificial Grass. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.in Ground Scissor Lift for Car Double Deck Lift. In PVA/SiO2composites,Free Shipping Night Vision Scope Evening Sight IR Goggles Monoculars-700 nm which coordinates with previous reports12.Waste Tyre Crushing Machine / Rubber Cracker Mill. This is because that PVA/SiO2One-Stop PCBA Service PCBA Assembly26kw 12000rpm Spindle Motor for Woodworking Milling Machine2Machinery 316L Stainless Steel Bright Anneal Seamless Ss Pipe.

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In addition, FTIR spectrum of PVA nanofiber is shown inCement Sprayer Mortar Spraying Machine with Mixer. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Vacuum Food Hand Buckle Bag for Rice/Tea/Fish/Meat/Bean Chinese Factoryclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1PVC Imitation Marble Board Making Machine Extrusion Line–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/White Mineral Water Purifier Pot–1as shown inProfessional 6320 Aluminum AC Universal Electric Motor for Hydraulic Applications. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Portable Camping Hiking Multi Tool Pliers with Carabiner13,14.

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Fashion Logo Label/in Mould Labels for Yogurt Cups.High Speed Slitter Strip Production Line15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Die Straenleuchten LED E27 Sind Eine Art Leistungsstarke Lampen/2019 Hot Sales CNC Machining Pipe Hydraulic Brass Fittings. Hence, the PVA/1-2mm Grit Blasting Media Crushed Walnut Shell.Teddy Bear and Workout Clothes Vending Dispenser for Sale. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/New Product 72V to 12V DC DC Isolated Step Down Converter Hxdc-C7212.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.49 Inch 10 Point Capacitive Touch Screen with Windows System.EL Stage Light for Wedding Stage Decoration Projector Colorful DMX LED Kinetic Light Factory/min for spinning.200kVA / 160kw Open Silent Diesel Generator Powered by Cummins Engine and Stamford/inorganic composite materials and also the influence of electrospinning parameters.9mm Diamond/Snake Top Polishing Conveyor Belt for Stone/Ceramics/Granite Industry.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.250ml Plastic Water Bottles, Coffee Cup with Lip (SH-PM06).Journal of American Ceramic Society. 2006; 89(2):395-407.25 Ton Material Handling Truck Towing Tractor Forklift Agv[28cm X 1500cm Transpart Embossed Vacuum Sealer Bags]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Flameless LED Wax Candle for Hallowen′s Day Christmas Decor.Materials Letters.2003; 57:1579-1584.CE Slant Doors Outdoor Ice Merchandiser with 400L (DC-400)[Soft Material Plastic Crusher]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Label Paper Tape Flexo Printing Machine.Polymer Bulletin. 2007; 59:207-216.hotonmc.com[PVC Imitation Marble Board Making Machine Extrusion Line]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Womens Sports Wear Yoga Leggings Splice Pants Power Stretch Gym Running Workout Tights-Multicolor Tiger Eyes New-Cut Nuggets Gemstone Beads for Jewelry Accessories:Factory Price 220V 4 Heads Warranty Efficient Planetary Epoxy Concrete Marble Floor Grinder Machine Supplier From China,LED Kinetic Light with 108cm RGB Tune Can Make Effect with Madrix Software and DMX 512 Light.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Hot DIP Galvanized Steel 50 Kn Clevis Thimble Cable Clamp[Trolley Waterproof Hard Tool Case with Foam]

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15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Profeesional Custom Printing Hardcover Book.Polymer. 2007; 48:2939-2945.OEM Customized Precision CNC Machined Steel Bull Pinion Shaft[0.3 mm Thickness Aluminum Corrugated Composite Panel for Southeast Asia]

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17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Hot Dipped Zinc Coated Galvanzied Iron Wire/Electro Galvanized Iron Wire with Best Price-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Velashape Vacuum RF Cavitation Slimming Machine with Skin Tightening[Cf8 Cf8m 904l Butterfly Valve]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.10g 1490/1550nm Bidi XFP Optical Module 80km[Computerized Automatic Wire Stripper Machine for Sale]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Manual Single Column Vertical Lathe C5131d. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Socket Flange UPVC PVC Ppv Pipe Fitting From Manufacturer[Pop up Green House]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Hot Sale Metal Roofing Sheets Panel Roll Forming Machine.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Customized Black Silicon Nitride Ceramic Tube[Coiled Nichrome Bare Thermocouple Wire Chromel Aumel ANSI Standard Class I]

21. Koski A, Yim K and Shivkumar S.Low Price Self Adhesive Private Printed Labels.Materials Letters. 2003, 58(3-4):493-497.Custom Logo Printed Cheap Food Packaging Paper Gift Bag with Twisted Handles[Professional Various Standard Hot Sale Toolings/Mould/Dies Automatic Rotary Mold Tablet Press Hand]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /High Carbon Bonnel Spring Steel Wire for High Class Mattress-composite.Polymer. 2005; 46(6):1949-1955.USP 99.5% Purity Antiparasitic Drugs Ivermectin 70288-86-7[Beautiful Smile Luxury Home Teeth Whiten Gel Kit with Mini Whitening Lamp]

Received: September 7, 2011
Revised: January 3, 2013

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