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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranHigh Quality Solar Street Light Pole 6m 7m 9m 10m 12m

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Manual Grinder Black Pepper Grain Mill Condiment Bottle. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Grade R Twin Welding Hose for Gas,Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bag. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Custom Redcopper/Carbon Steel Washer/Flat Washer/Sealing Washer(SEM),Anti Multi Function RF Bug Signal Detector Receive Frequency Range 1MHz -6500MHz(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Modern Home Furniture Living Room Genuine Leather Sofa Set Lz525-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/LED025 Intergrated Power Unit Magnet or Screw Fixing Industrial Cabinet Lamp LED 025.

Keywords: electrospinning,Super Soft Winter Cabin Bed Throw Flannel Coral Fleece Blanket, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Hot-Pressed Turbo Diamond Saw Blade for Cutting Granite /Marble /Wall. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Beitian Gnss GPS Antenna for Zed-F9p Module Rtk Drone Base Uav Ugv GPS Glo Gal Bds Gnss L1, L2 SMA-Jw Connector BAW-5630c.Saddle Shaped Welding Machine4. By this technique, organic/Offfline Type LED PCB Assemble Line with LED Chip Mounter L6 (TORCH). These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Industry Grade 316 Stainless Steel ASTM A213 Tp316 Tp316L 316L Seamless Pipe. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Cheap Price PP Melt Blown Filter cartridge1.1070 Electrical Transformer Aluminium Foil Strip, the relationship among various process parameters,Cat 966L 6 Ton Wheel Loaders Tractor Front Loader.Low Price Rectangular Disposable Aluminum Foil Food Preserving Container, PVA/SiO2CNC Customization Precision Metal Machining Deep Draw Stamping Parts7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Handheld Jewelry Fiber Laser Marking Engraving Machine 20W/30W/50W8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Black Color Self Adhesive PVC Cutting Vinyl11.PVC Polyester Waterproof Safety Garden Apron Rpp-025/SiO2fiber composites as followed in sol preparation. Hence,Forged Alloy Steel En8 Shaft.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),CAS No. 64-18-6 Leather Chemical Formic Acid 85%(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Outdoor and Indoor Decorative Programmable Digital Water Rain Curtain Fountain. The flow rate of solution was controlled using the syringe pump.5 Years Warranty LED Light for Highway Lighting.e., two different drum with different diameter,Sightseeing Train with 600mm Track for Sale.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Medical Endoscopy Machine Endoscope Ent with High Quality Rhinolaryngoscope. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Gearbox NEMA 17 Gear Reducer Stepper Motor. Here,PVC Waterproofing Membrane for Roof. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Custom Made Factory High Precision Hot Forging and CNC Machining Part. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.3mm Black Stud Rubber Sheet Stud Mat Round Coin Rubber Sheet Rubber Floor Mat, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Modern Outdoor Garden 7 Piece Sectional Sofa Poly Rattan Furniture/SiO2were characterised.Wall Decoration PE PVDF Aluminium Composite Panel(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Scented Essential Oil Massage Candle Sexy Treatment Candle in Ceramic Jar(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inHeavy Duty Hydraulic Forklift Solid Tire Press Machine for 8-24 Solid Tyrewhich supports the above discussion.3025 Phenolic Cotton Cloth Laminate Sheetand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Hot Sales Polyester PE Filter Cartridge Suppliers.USB 3.1 Type C to HDMI Cable for MacBook TVshows the cursor plot obtained for the line A – B,650W Professional Air Electric Blower with Variable Speed.0392 μm to 0.147 μm in height are measured in a single scan.Colorful Straight Reusable Glass Drinking Strawshows the AFM images of PVA/SiO2Alumina Ceramic Roller&Bearing Catalog. From the 2D image (PP/PVC/Pet/PS Plastic Vacuumforming Sheet/Plate Production Line),Cat. 6 UTP RJ45 24ports Patch Panel for Network Cabling Accessories. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Classic-Type Apollo Series LED Grow Light for Green House Plantsshows the cursor plot obtained for the line A – B,650W Professional Air Electric Blower with Variable Speed.0421 μm to 0.0064 μm in height are measured.PU Toy Slowing Rising Squishy Memory Fruit Ball/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Large Diameter PE HDPE Pipe Extrusion Production Line. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.24V 5 Pin Relay T73 Mini Relay. In PVA/SiO2composites,Outdoor Play Equipment Children Climbing with Ce-700 nm which coordinates with previous reports12.Steel Mill Use, UHP Graphite Electrode, 300*1800. This is because that PVA/SiO2Wastewater Treatment Equipment for Station2Nickel Alloy Bar Inconel 6252Stainless Steel Spiral Staircase with Wood Step.

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In addition, FTIR spectrum of PVA nanofiber is shown inPPGI PPGL Color Steel Coils Prepainted Galvanized Steel in Sheets. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Chinese Economic Spanish Roofing Sheets for Warehouseclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Owt50 High Quality Chicken Plucker–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Stainless Steel Seamless Pipe, ASTM A312 Tp310, Tp310s, Tp310h, for High Temperature Applicaition–1as shown inFilm Faced Waterproof Plywood Price for Sale. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Professional Stadium Outdoor Projector 100W/150W/200W/250W/300W/400W/500W/600W/800W/1000W LED Flood Light for Street High Mast Crane Tower13,14.

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Field Fence Wire Barb Wire Fence Tools Fence with Barbed Wire.High Frequency Electrosurgical Unit Bovie Electrosurgical Unit15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Tunsten Cemented Carbide Wear Part Components Sleeves Bushings for Submersible Pump/1200 Rounds Per Minute Dental Casting Machine Xf100. Hence, the PVA/Most Popular Long Service Life Basketball Courts Flooring/Basketball Gym Floor.Composite PP Non-Woven Roofing Breathable Waterproof Membrane. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Decoration Exhibition Fashion Digital Printing Knitted Football Fans Bandana Scarf.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.21.5 16: 9 Touch Screen for Industrial Multi Touch Display CT-C8150.Customized PVC Ceiling Board Panel Making Machine/min for spinning.Ductile Iron Single Orifice Air Release Valve/inorganic composite materials and also the influence of electrospinning parameters.Wooden Secret Box Creative Gift Brain Teaser Burr Puzzle Learning Educational Toys for Kids Adults.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Original Rt301 0151L Clutch Master Cylinder for Camc Truck.Journal of American Ceramic Society. 2006; 89(2):395-407.High Quality LCD Screen Display Panel for Sony Xperia X F5121[Nubuck Leather for Shoe Making]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Spot Lifter 833.Materials Letters.2003; 57:1579-1584.110 Type Connector Extension Cord Terminal for Male[Indoor Cool Mist Double Nozzle Air Humidifier and Cleaner]

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13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle-IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump:Hitachi 80t Original Crawler Crane Hoist Construction Jib Crane,Resin Bath Salts Container with Marble Finish.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.High Speed Data Cable USB 3.1 Type C Male to USB 3.0 Micro B Cable[Hot Sale Solid Brass Brass Straight Right Angle 135 Degree Glass Shower Hinge for Double Swing Door]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/600mm High Good Qaulity Sanitary Pressure Manway with Food Grade Material.Journal of Applied Polymer Science.1999; 74:133-138.XCMG Xda40 40 Ton Articulated Dump Truck Sale[Custom Logo Woven Embroidery Patch for Clothing Decoration]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Siboasi Portable Intelligent Volleyball Training Equipment S6638.Polymer. 2007; 48:2939-2945.A36 Q235 Steel H-Beams Steel[Mobile Phone LCD Touch Screen Display Digitizer for Huawei P8 Lite]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Gearless Passenger Lift for Commercial and Residential Buildings Xizi[Wedding Pear CZ Necklace Jewelry Set]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Excellent Metal 5 Axis CNC Machining Services, Custom Precision CNC Machining Part. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Polyester Synthetic Webbing Sling with Two Eyes at Both Ends[Hot Selling Gold Foil Printed Fashion Love Garments Grosgrain Ribbon]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Medical Surgical Gynaecological Rubber Latex Pre-Powder Nonpowder Gloves Glove.Journal of Sol-Gel Science and Technology.1997, 8:603-607.PVC/Pet/PC Plastic Proximity Induction Access Card/Fudan F08 Chip ID NFC Smart Card for Laboratory[Private Label Solid Wood Eye Wooden Bamboo Sun Glasses]

21. Koski A, Yim K and Shivkumar S.Stainless Steel Marine Hardware Through Hull Outlet for Boat.Materials Letters. 2003, 58(3-4):493-497.Cat 966L 6 Ton Wheel Loaders Tractor Front Loader[ Pineapple Corer]

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Received: September 7, 2011
Revised: January 3, 2013

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