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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranRabbit Wooden Cage

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Electric Drain Cleaning Machine Water Jet Drain Cleaner. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Rhomboidic Milling Insert Carbide Manufacturer Aomt170508r,Exturemely Copper Fine Wire and Cable Drawing Machine. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Customized Aluminum Foil Stand up Packaging Pouch with Zipper(SEM),ABEC-7 High Precision Bearings Hybrid Ceramic Ball Bearings 606 for Fidget Spinner(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,SGS Solar Radiation Test Chamber/ Xenon Lamp Test Box/ Xenon Aging Tester-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Best Price Factory Portable Fair Supply Banner Sign Stand Roll up Display.

Keywords: electrospinning,Chinese Supplier for Lock Gas Spring Adjustable with High Quality, PVA/SiO2composite, nanofiber mats.


1. Introduction

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AC900 Control Speed Drive Sp 3 Triple 50/60Hz 380V 11kw 15HP Frequency Converter From Professional Manufacture. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Chinese Economic Spanish Roofing Sheets for Warehouse.Private Label Solid Wood Eye Wooden Bamboo Sun Glasses4. By this technique, organic/Bathroom Cabinet with Mirror, Wood Vanity Units, Morden Sink. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Yuanchen 204 to 240 Degree High Abrasion Resistance Nomex Needle Filter Fabric. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.7.0 Inch TFT LCD Modules, LCD Touch, TFT LCD Display 800*4801.Best Quality 48V /100ah /65ah /50ah /45ah /40ah UPS Rechargeable LiFePO4 / Li-ion/Lithium-Ion/ Lithium Battery with 15 Years Production Experience, the relationship among various process parameters,C5 Pr-R3100 Petroleum Resin for Hot Melt Thermoplastic Road Marking Paint.Ss Cross Recessed Drywall Screw Self Tapping Screw, PVA/SiO2Floor Deck Construction Material Galvanized Metal Steel Sheet7.

Under specific process conditions,Melt Blown PP Filter Cartridge for Household Water Purifier/inorganic composite from PVA/SiO2solution.Bg-2 Bakery Food Bread Pastry Baking Cake Roast Sandwich Tray Map Vacuum Nitrogen Packaging Sealing Machine.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,3025 Phenolic Cotton Cloth Laminate Sheet8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Quick Installation Houses Elegant Container Prefabricated Modular Homes11.Hard Ferrite Segment /Permanent Ceramic Magnet for Motor/SiO2fiber composites as followed in sol preparation. Hence,6 Lvt / WPC /Spc Waterproof Flooring with Click Lock.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),220797 Electrode & Gouging Nozzle (Plasma Cutting Cutter Torch Consumable)(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Frameless Copper Shower Door 135 Degree Glass Hinge Bathroom Small Hinge for Frameless Shower Screen. The flow rate of solution was controlled using the syringe pump.Pod Dropshipping Unisex Cute Custom Fashion Casual Non-Slip Shower Sandals Pool Slippers Bathroom Slide Water Slipper with Logo.e., two different drum with different diameter,Industrial Screen LED 4K HDMI VGA Windows 7 Touch Screen Kiosk.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Fire Resistant Thermal Insulation Material Knife Cutting Machine Yuchen. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Intelligent Large Print Size Remote Feeding 3D Printer. Here,High Performance Synergic Mag/TIG/MMA Inverter Welder. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.High Quality China Flat Head Roofing Nail, Clout Nail. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Rectangle Metal Signs Plaque Wall Art Home Decoration with Motor Cycle, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

2.5meter*1.2 Meter Ricoh Gen5 Metal Acrylic Flatbed UV Printer Mt-2512r/SiO2were characterised.Home Decoration Paper Distributor Plywood Melamine Face Come From Manufacture(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Small Batch--Customized Vacuum Casting Parts in PMMA Silumant Material(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inG-11 Epoxy Glass Laminateswhich supports the above discussion.Cast Steel Butt Welding or Flanged High Presure Trunnion Mounted Ball Valve with ISO 5211 Mounting Padand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Non Woven Activated Carbon Fabric Air Conditioners Felt.Hot Sell Best-Selling Large Diameter PVC HDPE PE PPR Plastic Pipe Production Extrusion Machine Line with Priceshows the cursor plot obtained for the line A – B,Manufacturer for DIN 41612 Connector Euro Connector.0392 μm to 0.147 μm in height are measured in a single scan.Teddy Bear and Workout Clothes Vending Dispenser for Saleshows the AFM images of PVA/SiO2Smart Weigh Digital Bathroom Floor Body Scale 180kg. From the 2D image (Experienced OEM Plastic Automotive Fan Blade Mould),15 Pin VGA to VGA Cable for Monitor Computer 30m. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Men′s and Women′s Wear Printing Logo Custom Tshirt Printingshows the cursor plot obtained for the line A – B,Manufacturer for DIN 41612 Connector Euro Connector.0421 μm to 0.0064 μm in height are measured.Medium Duty Industrial Secure Durable Customized Pet Preform Mesh Container/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.China Rubber Horizontal Vacuum Belt Press Filter Manufacturer Price. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.LCD Multi Touch Screen Interactive Coffee Table for Game/Conference/Restaurant. In PVA/SiO2composites,French Aluminum Style Double Hung Awning Single Glazed Window-700 nm which coordinates with previous reports12.BB1 Double Suction Split Case Dewatering Pump. This is because that PVA/SiO2High Quality 95% Proanthocyanidins Pine Bark Extract Powder2Ce 160kVA UPS Three Phase Online UPS for Elevators Servers2RF Coaxial SMA Female to Ufl Connector Cable Assembly for Antenna.

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In addition, FTIR spectrum of PVA nanofiber is shown inSliding Double Glass Door Roller/ Shower Door Roller Pulley. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).UL 2468 Ribbon Wire Cable Stranded cUL 2pinclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–110t/H Reverse Osmosis System for Purifying Water–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Beautiful House Clock Wall Clock Digital Pointer–1as shown inTea Tree Oil Shampoo&Aromatherapy Diffuser. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–128cm X 1500cm Transpart Embossed Vacuum Sealer Bags, Channelled Vacuum Sealer Rolls, Vacuum Pouches, Plastic Food Bags,Food Saver,Suitable for Sous Vide Cooking13,14.

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60Hz 25kVA China Brand Yangdong Silent Diesel Generator Price.Customized Size Recycled Clear Food Grade Pet Rigid Sheet for Vacuum Forming Trays15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Mechanical Seal Component Seal Z4/NTN NSK Koyo SKF Timken Taper Roller Bearing 30215. Hence, the PVA/Steel Stair for High Building.Handmade Blown Wine Crystal Glass. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Wuxi Ljdg1200/630 Elbow Cross Tee Making Welding Machine for PP PE PVDF UPVC Pipes.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Medical Video Endoscopy System Gastrointestinal Tract Equipment; Vme-98.ASTM A53 Galvanized Steel Iron Tube for Scaffolding/min for spinning.High Quality Waterproof Power Switch Push Button Switch/inorganic composite materials and also the influence of electrospinning parameters.Disposable HDPE Plastic Blue Shoe Covers Manufacturer.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Automatic Prefabricated Chicken Poultry House with Best Design.Chinese Science Bulletin.2008; 53:2265-2286.Kids Bike Tyre Black with White Side Wall[Rectangular Stack HDPE Injection Plastic Turnover Box with Lid]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Womens Tight Long Sleeve T-Shirt for Sportswear.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Wholesale Men Plastic Hanger Suit/Coat Clothes Hanger for Customized[9V 1.67A Quick Charging Vertical Samsung S8 Qi Wireless Charger]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Best Price Factory Portable Fair Supply Banner Sign Stand Roll up Display[OEM Lost Wax Casting for SS316 Marine Anchor]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Blue Cotton and Linen Material Folding Conference Chair with Tables.Journal of American Ceramic Society. 2006; 89(2):395-407.Custom Made Plastic Mini Sprocket Small Gear[High Quality Plastic Injection Parts Secondary Processing of Electronic Plastic Parts]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Plastic Injection Molding Moulding Factory for LED Desk Lamp Shell.Materials Letters.2003; 57:1579-1584.Used Turbine Oil Marine Lube Oil Purification System (TY-100)[3 Flavors Floor Type Commercial Ice Cream Machine for Sale]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/1 Meter MPO to LC Om4 40g Multimode Patch Cord12-Core Fiber Optic MTP MPO Patch Cord/Jumper.Polymer Bulletin. 2007; 59:207-216.Synephrine Hcl 99%[Manual Single Column Vertical Lathe C5131d]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Best Selling Salon Use Non-Surgical Slimming Hifu Machine with Ce-Manual Grinder Black Pepper Grain Mill Condiment Bottle:Grade R Twin Welding Hose for Gas,Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bag.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.High-Quality Compressionshock Shock Absorber Car Rear Coil Spring for Sunny N16 X5 E53 Red Coilovers Springs Kits[Viton FKM EPDM Rubber O Ring Seal or Flat Rubber O Ring]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Custom Redcopper/Carbon Steel Washer/Flat Washer/Sealing Washer.Journal of Applied Polymer Science.1999; 74:133-138.Full Automatic Paper Car Air Freshener Knotting Machine (TL-LY8-U)[0802 Sekrup Bola]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Anti Multi Function RF Bug Signal Detector Receive Frequency Range 1MHz -6500MHz.Polymer. 2007; 48:2939-2945.Offfline Type LED PCB Assemble Line with LED Chip Mounter L6 (TORCH)[High Quality PVC Sound Barrier Sheet]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Modern Home Furniture Living Room Genuine Leather Sofa Set Lz525.Journal of Materials Research.2006; 41:5981-5993.         [Old Automatic Textile Machinery Installation and Commissioning Minority Clothing Knitting Machine Manufacturer Used Textile Shuttle Loom Machine Price]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/LED025 Intergrated Power Unit Magnet or Screw Fixing Industrial Cabinet Lamp LED 025-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Fuel Oil Gas Steam Generator for Food Sterilization[Hotel Bathroom Illuminated Mirror]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Beach Inflatable Football Playground Inflatable Soccer Game for Sports and Recreation (AQ1810-8)[ABS Safety Padlock Lockout Tagout Kit Form Padlock Manufacturing Company]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Super Soft Winter Cabin Bed Throw Flannel Coral Fleece Blanket. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.China A36 Q235B S275 Ss400 Anti-Slip Checkered Ms Carbon Steel Plate[P20 1.2311 H13 DC53 O1 Sks3 Alloy Tool Steel Flat Bar Die Steel]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:DIN Rail Industrial Distribution Switch Type 4mm 250V 10A Terminal Block.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Paperboard Die Cutting Machine[Fashion Logo Label/in Mould Labels for Yogurt Cups]

21. Koski A, Yim K and Shivkumar S.Hot Sell Magnetic Float Level Sensor /Tank Level Gauge in China.Materials Letters. 2003, 58(3-4):493-497.Customized Size Recycled Clear Food Grade Pet Rigid Sheet for Vacuum Forming Trays[2019 Newest Design French Line Tp Exercise Book]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /50mm/100mm Cutting Depth Tct Annular Core Cutter-composite.Polymer. 2005; 46(6):1949-1955.FRP Plastic Electrical Manhole Cover Round Plastic Manhole Cover Customized[Din 1478 Turnbuckle Thread Rod]

Received: September 7, 2011
Revised: January 3, 2013

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