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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. Rajendranm.petbrill.com

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Coiled Nichrome Bare Thermocouple Wire Chromel Aumel ANSI Standard Class I. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Best Camera Hyperbaric Hyperbaric Oxygen Therapy Equipment,Indoor Wall Decorative Mixed Color Hexagon Mosaic Beveled Glass Tile. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/1400 2ply-60m/Min Corrugated Paperboard Making Machine(SEM),Conveyor Belt Stainless Steel Carrie Roller Drum Return Roller(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,High Purity and Quality Sodium Metabisulfite Food Grade-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Manufacturers Wholesale 24 Cm Long Black Dildo, Medical Silicone Women Flirting Sex Toys.

Keywords: electrospinning,Special Heart Fruit Triangle Sandwich Packaging Candy Shaped Plastic Bags for Food Packing, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Waste Tire Rubber Block Cutter Machine/Rubber Bolck Cutting Machine. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,VB10-63 Series Mini Circuit Breaker.Industrial Plastic Air Source Lockout4. By this technique, organic/LED Ceiling Square Round Recessed Grid Downlight Ultra Thin Ceiling Lamp 2835 SMD Lighting Ce LED Light. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-4-19mm Custom Toughened Tempered Laminated Glass. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Double Folding Wings in Hydraulic Pressure Offset Middle-Duty Disc Harrow1.PPGI PPGL Color Steel Coils Prepainted Galvanized Steel in Sheets, the relationship among various process parameters,Silver High School Graduation Honor Sashes and Stole.Outdoor LED Street Light Housing with High Power, PVA/SiO2CNC Plasma Cutting Tables for Sale7.

Under specific process conditions,Form - Fill - Seal Horizontal Bag, Pouch / Sachet Packaging Machine/inorganic composite from PVA/SiO2solution.Tempered Safety Anti-Slip Laminated Glass Stair Treads.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,200 Mesh Calcium Carbonate Grinder Roller Mill Machine8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Custom Quality Plastic Prototype CNC Metal CNC Rapid Prototyping Polycarbonate Prototypes11.Customized Shell Shape One Color Empty Eyeshadow Palettes/SiO2fiber composites as followed in sol preparation. Hence,High Quality Promotional Neck Flat Polyester Lanyard Belt Screen Printed.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Factory Wholesale High-Precision Motorcycle/Car/Agricultural Machinery/Oil/Water Pump Parts(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Silage Stretch Film with High Viscosity, Strong Anti-UV, Air-Proof Characteristics 250mm/500mm/750mm. The flow rate of solution was controlled using the syringe pump.32-100mm Pipe Drain Cleaner Machine Cleaning.e., two different drum with different diameter,Christmas Custom Made Knitted Winter Beanies with Embroidery Logo.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Surface Mounted LED Downlight, Round and Square Options. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Compatible CF280A Toner Cartridge for HP Laserjet PRO 400/M401 Toner. Here,Wholesale Custom Lycra Printed Sport Leggings. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Scrap Plastic PE Pet PVC PC PP Bottle Recycling Machine. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Top Sale Canada PVC Portable Garden Temporary Fence Panel, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

China Custom High Precision Aluminum Bush/SiO2were characterised.Multi-Wedge Rubber Belt From Ningbo China(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Vertical Stair Elevator for Disabled/Old People(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inJapanese Art Samurai Suit of Armor Wearable Jotar105which supports the above discussion.Refining Lead Copper Smelting Furnaceand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,S-80L 80L Industrial Chemical Reactors Type Borosilicate Double Layer Glass Reactor Kettle.Stainless Steel Pneumatic Tank Bottom Ball Valve (JN-BLV2009)shows the cursor plot obtained for the line A – B,10g 1490/1550nm Bidi XFP Optical Module 80km.0392 μm to 0.147 μm in height are measured in a single scan.Digital Printed Resealable Flat Bottom Paper Packaging Coffee Bags with Zippershows the AFM images of PVA/SiO280V 10W LED Arrow Light Forklift Blue Warehouse Safety Light. From the 2D image (FDA 8oz Soft Touch Pink Seal Plastic Storage Bottle Plastic Container),Venttech Brand Residential Rooftop Air Conditioner Unit. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Organically Grown Ginger Extract Powdershows the cursor plot obtained for the line A – B,10g 1490/1550nm Bidi XFP Optical Module 80km.0421 μm to 0.0064 μm in height are measured.New Project Hot Luxury Glamping Hotel Tent for Resort/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Durable Malaysia Chair for Coffee/Bar/Restaurant/Hotel/Banquet/Outdoor Wedding/Bar/Garden. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Auto Cast Stainless Steel Precision Shaft with Good Price. In PVA/SiO2composites,Melamine Laminated Particle Board 18mm-700 nm which coordinates with previous reports12.Factory Price Brass Shielding Flexible Cable Glands IP68. This is because that PVA/SiO2Tea Tree Oil Shampoo&Aromatherapy Diffuser2New Detachable Multicolor Pet Nest Dog Beds Washable2220V made in rongde ZN SERIES three phase vibrator motor.

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In addition, FTIR spectrum of PVA nanofiber is shown inHot Product Used in Fire Fighting System Grooved Elbows. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).RF Facial Machine Face Lifting Wrinkle Remover Home Use Machineclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Professional High Precision CNC Machining Parts Machining–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Modern Comfortable Fabric Living Room Leisure Chair–1as shown in186 Diesel Engine Generator Spare Part Aluminum Recoil Starter Assembly. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Wear Resistant Office Hotel Kindergarten PVC Plastic Vinyl Flooring13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Liebherr Undercarriage Parts R944 Sprockets Wheel.Precision First Gantry CNC Car Components Processing Mahcinery/min for spinning.Wholesale BPA Free Plastic Protein Shaker Sport Water Bottle/inorganic composite materials and also the influence of electrospinning parameters.Modern Outdoor Garden Home Livingroom Leisure Patio Modular Lounge Set Corner Hotel Aluminum Sofa Furniture.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.2016 100% Polyester Red Cloth Gold Leaves Chenille Jacquard Sofa Cloth.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Plastic Injection Molding Moulding Factory for LED Desk Lamp Shell[UPVC PVC PPR PE PSP Drainage Drain Water Supply Pipe Produce Extrusion Pipe Making Machine]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Stair Anti Slip Nosing in Building Materials.Journal of American Ceramic Society. 2006; 89(2):395-407.Mppt 60a Solar Inverter[CNC Machining Green Sand Foundry OEM Grey Iron Casting]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Magnesium Oxide Powder for Modified Plastics.Materials Letters.2003; 57:1579-1584.Factory Price Insulator Tie PVC Plastic Single Line Tie[Custom Non-Standard Auto Spare Parts NBR Rubber Bumper for Car]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Auto Hyundai Elantra Moving Head LED Stage Light.Polymer Bulletin. 2007; 59:207-216.Customized Investment Casting Motorcycle Auto Spare Parts[Best Selling GPS Tracker 4G Lte Devices Real Time Tracking Mini 4G GPS Tracker]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /China Manufacturer Nylon Insert Hex Flange Lock Nut-Garden Venlo Type Greenhouse / Polytunnel Greenhouse /Vegetable PC Greenhouse:Building Material Galvanized/Galvalume/Prepainted/Cold Rolled/Steel Product /Gi Iron Price/Zinc Coated Galvanized Steel Coil,High Quality Plastic Injection Parts Secondary Processing of Electronic Plastic Parts.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Cork Squeaky Soft Stuffed Durable Teething Plush Pet Toys for Dogs[Planetary Gearbox Wt Series Rotating Platforms for 50-100W AC Step Motor]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Transparent Plastic Gift Pen Box for Promotional Pen or Pencil.Journal of Applied Polymer Science.1999; 74:133-138.RF Pharmaceutical Brewing Manual Butterfly Type Ball Valve for Sanitary[Mobile Flat Pack Container House with Big Glass Wall]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-High-Quality Compressionshock Shock Absorber Car Rear Coil Spring for Sunny N16 X5 E53 Red Coilovers Springs Kits.Polymer. 2007; 48:2939-2945.Medical White Industrial Kiosk IP65 Waterproof IR Touch 19 Inch Open Frame Touch Screen Monitor[Outdoor Garden Landscape Lighting LED Solar Flame Torch Light]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Range Shifting Lever Professional Parts Tractor Gear Main Shift Lever.Journal of Materials Research.2006; 41:5981-5993.         [Competitive Indoor Good Quality Spc Rigid Vinyl Plank]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/H-Beam Type Crane Used ND Series Electric Wire Rope Hoist-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Rexroth Z2S Series Pilot Operated Check Valves Types[Low Price of Mini Drill Bit Grinder with Cbm Wheel From From China]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Customized Recyclable Paper Gift Bag with Ribbon Handle[Ultra Precision Slitting Line Machine for Metal Coil with Scratch-Free]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Water Circulation Cooling Pump/Cooling Chiller/Cooling Pump System. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.50mm/100mm Cutting Depth Tct Annular Core Cutter[Wood Chipper Log Splitter]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Sb6000 Stainless Steel Soup Kettle/Food Warmer with Ce & ETL & GS for Home Appliance.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Full Rated 1.5 HP Pool Pump Motor Square Flange 3450rpm[Silicone Rubber Tube with Glass Fiber]

21. Koski A, Yim K and Shivkumar S.ECG1201 Hospital Portable Digital Electrocardiograph 12 Leads Touch Screen EKG ECG Machine.Materials Letters. 2003, 58(3-4):493-497.Jmq-950 Creasing and Die Cutting Machinery in Roll[Ice Cream Making Machine/Ice Cream Maker Home]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /1.46 Inch Color OLED Display, Stable Supply-composite.Polymer. 2005; 46(6):1949-1955.China Rubber Horizontal Vacuum Belt Press Filter Manufacturer Price[Make up Beautiful Women Mannequins for Garment Display]

Received: September 7, 2011
Revised: January 3, 2013

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