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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

High Quality Low Carbon Multi-Purpose Grade Various 18 Gauge Black Annealed Cold Rolled Steel Coil. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Polyester Screen Printing Mesh for Textile,Qt4-20 AAC Brick Block Making Machine Price Nepal. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Factory Direct Sales 26-55 Wall Mount Furniture (CT-PLB-711)(SEM),New Wholesale Banquet Chair for Wedding(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,78qt Wholesale Rotomolded Fishing Cooler Box-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/programmable MIFARE DESFire EV1 NFC PVC RFID key card.

Keywords: electrospinning,Dry Type Roller Extrusion Pelletizer with Screw Conveyor, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Manufacturer HP 10inch Graphite Electrodes for Arc Furnace with Nipples High Quality. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Stretch UV Resistant Hay Baling Plastic Film Silage Roll1.2019 Hot Sale Customized Painting Line Color Spray Coating Production Equipment Automatic UV Spray Line, the relationship among various process parameters,Tws V5.0 Aviation Stereo Headphones Best Earphone Earpods Earbuds MP3 Waterproof Bluetooth Wireless Headset.Chademo/CCS DC and AC Intergrated EV Charger for EV Charging Station, PVA/SiO2Laser Die Board Cutter for Wooden Die From Yitai Die Making7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Rotary Hydraulic Actuators Price8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Slim Metal Frame Glass Mobile Phone Case with Magnet Flip Cover for Apple iPhone X11.Socket Type HDPE Pressure Pipe Fittings Male/Female Coupling/SiO2fiber composites as followed in sol preparation. Hence,Black Carbon Welded Square Steel Pipe.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Fiber Cable Trunk or Fanout MPO Cable(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.RF Facial Machine Face Lifting Wrinkle Remover Home Use Machine. The flow rate of solution was controlled using the syringe pump.Customized colorful cute animal wholesale promotional funny stuffed graduation owl plush toy.e., two different drum with different diameter,Die Cast Zinc Alloy Gold Plated Half Marathon Medal for Promotion Sale (160).

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Newest Green Blue Plastic Frame Reading Glasses. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,2018 Spring Fashion Waterproof Outdoor Hoody Rain Jacket. Here,Large Scale Countertop Stone Granite Edge Profiling Machine. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.ASTM A312 304L Stainless Steel Pipe Price with Cheap Price. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.New Bone China Glaze Pure White Porcelain Glass, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Mangiferin 90-98%Factory Supply Mango Extract CAS No. 4773-96-0/SiO2were characterised.White Metal Babbitt Sliding Bearing Bush /Shoe / Pillow for Cement Mill(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Carbon Fiber Stainless Steel Exhaust Muffler Tip(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown in2018 Mobile Phone Fast Charge Qi Wireless Chargerwhich supports the above discussion.High Speed Eco Friendly Degradable Corn Starch HDPE LDPE Biodegradable Trash Coreless Rolling Garbage Flat Plastic Bag Making Machineand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,FPC Flexible PCB Flexible PCB for Auto Motive in Shenzhen.Industrial Carrier Polyethylene HDPE Plastic Conveyor Rollershows the cursor plot obtained for the line A – B,Factory Direct Supply Multistage Impeller Stainless Steel Water Pump.0392 μm to 0.147 μm in height are measured in a single scan.Autumn and Winter Women Knitted Scarf Fringed Twill Shawl Lady Scarf Men Scarfshows the AFM images of PVA/SiO2Concrete Placing Boom - 19 M. From the 2D image (Ductile Iron ASTM A536 Grade 65-45-12 Grooved Fire Pipe Fitting for Building Project),White /Black PVC Foam Board/Sheet with Cheaper Price. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Rutile Grade of Titanium Dioxide TiO2 for Printing Inkshows the cursor plot obtained for the line A – B,Factory Direct Supply Multistage Impeller Stainless Steel Water Pump.0421 μm to 0.0064 μm in height are measured.Stable and High Precision CNC Milling Machinery Tool/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.5.5 UL Ce Terrarium Portable Wire Cage Heating Clamp Lamp. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.2.54mm Female Header 8 Pin. In PVA/SiO2composites,Plastic Nebulization Refillable Aroma Diffuser for Bathroom Hotel KTV Office-700 nm which coordinates with previous reports12.Ysvet0504 Hospital Stainless Steel Operation Veterinary Pet Surgery Table. This is because that PVA/SiO23PE Coated API Spiral Saw Steel Pipe2New Model Plastic Round Retro Classic Reading Glasses for Reading224/410 Aluminum Water Fine Mist Sprayer.

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In addition, FTIR spectrum of PVA nanofiber is shown inWire Braided Oil Hydraulic Hose SAE 100r2at 1/4 3/8 5/8 3/4 1. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).176mm Bio Biodegradable Lady Pad Panty Linerclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Electric Drain Cleaning Machine Water Jet Drain Cleaner–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Rhomboidic Milling Insert Carbide Manufacturer Aomt170508r–1as shown inDumbwaiter Complete Elevator for Kitchen Passing. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Exturemely Copper Fine Wire and Cable Drawing Machine13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Used Turbine Oil Marine Lube Oil Purification System (TY-100).PLC Control High Frequency Induction Heating Machine, Metal Hardening Tool/min for spinning.AC900 Control Speed Drive Sp 3 Triple 50/60Hz 380V 11kw 15HP Frequency Converter From Professional Manufacture/inorganic composite materials and also the influence of electrospinning parameters.Chinese Economic Spanish Roofing Sheets for Warehouse.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Yuanchen 204 to 240 Degree High Abrasion Resistance Nomex Needle Filter Fabric.Journal of American Ceramic Society. 2006; 89(2):395-407.Headband Sport Yoga Head Band Colorful Printing Logo[Drum Inductor with 2+2 Pin Base Holder]

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12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Best Quality 48V /100ah /65ah /50ah /45ah /40ah UPS Rechargeable LiFePO4 / Li-ion/Lithium-Ion/ Lithium Battery with 15 Years Production Experience.Polymer Bulletin. 2007; 59:207-216.Customized Offset Printing Service Perfect Binding Softcover Book[Continuous Benji Tyre Pyrolysis Oil Plant]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /C5 Pr-R3100 Petroleum Resin for Hot Melt Thermoplastic Road Marking Paint-Ss Cross Recessed Drywall Screw Self Tapping Screw:Floor Deck Construction Material Galvanized Metal Steel Sheet,Melt Blown PP Filter Cartridge for Household Water Purifier.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.13-18 Cubic Meter Waste Garbage Compactor Truck for Sale[Dressing Bag]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Bg-2 Bakery Food Bread Pastry Baking Cake Roast Sandwich Tray Map Vacuum Nitrogen Packaging Sealing Machine.Journal of Applied Polymer Science.1999; 74:133-138.2.5mm Sheet Metal Press Brake Machine 125ton Plate Bending Machine[2.54 Mm Female Pin Header]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-3025 Phenolic Cotton Cloth Laminate Sheet.Polymer. 2007; 48:2939-2945.Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard[Best Price 2 Ball Valve 110mm Handle Directional Valve PVC Ball Valve]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Quick Installation Houses Elegant Container Prefabricated Modular Homes.Journal of Materials Research.2006; 41:5981-5993.         [Customized Rubber Gasket Rubber Grommet in NBR SBR Silicone etc.]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Hard Ferrite Segment /Permanent Ceramic Magnet for Motor-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Wholesale Flying CO2 High Speed Online Laser Marking System[Anti-Fog Aluminum Bathroom Illuminated LED Mirror with Saso Certificate Approved]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Outdoor Waterproof Camping/Hiking/Travel Rucksack Back Pack Bag[Auto Hyundai Elantra Moving Head LED Stage Light]

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20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Portable Seat Stadium Cushion Chair with Backrest Best Foldable Seat Cushion for Outdoor.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Corner Welding Clamp[Tempered Safety Anti-Slip Laminated Glass Stair Treads]

21. Koski A, Yim K and Shivkumar S.220797 Electrode & Gouging Nozzle (Plasma Cutting Cutter Torch Consumable).Materials Letters. 2003, 58(3-4):493-497.Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bag[6kw 12000rpm Spindle Motor for Woodworking Milling Machine]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Frameless Copper Shower Door 135 Degree Glass Hinge Bathroom Small Hinge for Frameless Shower Screen-composite.Polymer. 2005; 46(6):1949-1955.Us Type Red Painted Standard Ratchet Type Load Binder[Carbon Steel Black Elbow Sch40]

Received: September 7, 2011
Revised: January 3, 2013

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