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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. Rajendranwww.zberic.com

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Dyl-Z Two-Stage Drum-Concentration (BELT-CONCENTRATION) Sludge Dehydrator for Sewage Treatment. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Quilting Mattress Protector or Fitted Sheet 100% Cotton /Polyester,14K Gold Plated Stone Thin Ring Jewelry Factory Customize Turkish Rings. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/20cm Groove Laminated PVC Ceiling Panel PVC Wall Panel(SEM),4 Deck Sand Vibrating Sieve Machine for Sale(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Dry Shiitake Mushrooms with Fragrant Flavor-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Kraft Paper Packaging Bag Stand up Pouch Doy Pouch.

Keywords: electrospinning,Woodworking Electric Edge Trimming Machine with PVC Edge Trimmer Knife Set, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-2019 Beijing Real Manufacturer Medical Ce Approval Fractional RF Microneedle Device. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.30d*30d Polyester Spandex Stretch Fabric for Shell or Lining Fabric1.Shengrun 3 Axles Box Body Self Dump Semi Truck Trailer, the relationship among various process parameters,50000hrs Lifetime High Power 400W LED Flood Light Outdoor Waterproof.Outdoor Garden Landscape Lighting LED Solar Flame Torch Light, PVA/SiO2China Weichai Engine Portable Silent Type Genset Automatic Protection Systems Soundproof Power Generator Diesel Generator Set with Warranty7.

Under specific process conditions,Professional Factory for Hot Runner Connector Terminal/inorganic composite from PVA/SiO2solution.Baode Lights Design 40m High Mast Lighting.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Inorganic Pigment Iron Oxide Red 130 and Iron Oxide Green 5605 for Bricks8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Factory Supply Movable Ozone Air Purifier Industrial Use Ozone Generator11.High Rigidity and Toughness Fpp Underground Drainage HDPE Pipe/SiO2fiber composites as followed in sol preparation. Hence,Multilayer Printed Circuit Board Assembly.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Skid Steer Loader Track T320*86k Rubber Tracks(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.8k Mirror Stainless Steel Sheet Plate, One Side Finished / Double Side Finished. The flow rate of solution was controlled using the syringe pump.Promotion New Model! Wood Effect Sunglasses of PC Model in 2017.e., two different drum with different diameter,Metal Fittings for Pipe and Joint System (H-6A).

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/12V 24V 48V 120mm 12cmx12cm DC Fan 120X120X25mm Cooling Fan. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Speaker Stand Aluminum Material to Hang The Microphone. Here,Fashion Jewelry Lovers Wooden Watches with Your Logo. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Hot Dipped Galvanized Steel Pipe ERW Carbon Black Steel Pipe. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Mbs-F16 Digital Controller Smart Sensor Sliding Glass Door System, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Fashion Cotton Coppola Cap/IVY Cap/Hunting Cap (DH-LH7286)/SiO2were characterised.Auto Tool Ford/GM/Mitsubishi/Nissan Compression Test Kit(Innova, Veeco, USA). The presence of PVA and PVA/SiO23A Under Floor Heating Room Thermostat(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inWall Mounted SMC Backboard Basketball Hoop with Backboardwhich supports the above discussion.Q195 Fencing Mild Carbon Welded Hot DIP 1.5 Inch Steel Pipe Manufacturer for Greenhouseand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Stainless Steel Pneumatic Tank Bottom Ball Valve (JN-BLV2009).Custom L10-15 Hydraulic Rotary Actuator with Counterbalance Valveshows the cursor plot obtained for the line A – B,2019 Waxed Leather Women Wallets Ladies Tri-Fold Long Purses.0392 μm to 0.147 μm in height are measured in a single scan.Zinc Cr Al Coating Low Carbon Steel Alloy Metal Stamping Partsshows the AFM images of PVA/SiO242cm 3D Hologram Fan with WiFi Holographic LED Fan Display. From the 2D image (T-Rex Plush Dinosaur Stuffed Animal Plush Toy Gifts -15′′),Logistics Cargo Storage Heavy Duty Pallet Rack and Shelving Systems. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Low Price Rectangular Disposable Aluminum Foil Food Preserving Containershows the cursor plot obtained for the line A – B,2019 Waxed Leather Women Wallets Ladies Tri-Fold Long Purses.0421 μm to 0.0064 μm in height are measured.New Design High Display Glass Case and Exhibition Cabinet/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Best 26 Inch Speed Mountain Bike Bicycle From China Packing Tape for Sealing Carton. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.45mm Slide Telescopic Channel Self Closing Slides Drawer Slide Rail. In PVA/SiO2composites,Wall Cladding and Roof Sheet Used Roll Forming Machine with Decoiler and Winder-700 nm which coordinates with previous reports12.Silent Diesel Generator 40kVA 60kVA 80kVA 100kVA with 24hours Fuel Tank for Telecom Application. This is because that PVA/SiO2UPVC PVC PPR PE PSP Drainage Drain Water Supply Pipe Produce Extrusion Pipe Making Machine2Rexroth Z2S Series Pilot Operated Check Valves Types22017 New Design Cable Ties Stainless Steel.

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In addition, FTIR spectrum of PVA nanofiber is shown inChina Weichai Engine Portable Silent Type Genset Automatic Protection Systems Soundproof Power Generator Diesel Generator Set with Warranty. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).4 Deck Sand Vibrating Sieve Machine for Saleclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1China Melamine Powder 99.8% Used for Sponge Packing in 25kg/500kg Bags–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Xinyuan Aluminium/PVC Profile/Wooden/Window Door Shrink Wrapping Machine–1as shown in450V 12UF Cbb60 Wire Series Grey Shell Capacitor. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Straw Pulp Double Screw Press for Paper Machinery13,14.

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Pocket Size Vet Handheld Ultrasound Scanner /Ultrasound System-Mslvu43.Uns No6617 Nickel Alloy Inconel 617 Plate / Sheet Price15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.LCD Digital Signage Kiosk 32 Inch Advertising Billboard Printing Machines Eyebrow Threading Kiosk for Sale/Wholesale Premium 750ml Green Champagne Bottle. Hence, the PVA/Mini/Lorry/Lcv/Commercial/Van Type/Cargo Box Light Duty Gasoline Engine Truck (Euro5).Hot Sale 12 Inch Stage Battery Bluetooth Speaker with Superpower. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/High quality fungicide Tebuconazole 98% TC  250g/L EW,60g/L FS, 250g/L EC.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.High Density Polyester Stripe Satin Yarn Dyed Fabric for Down Jacket.3X6m Rectangle Folding Gazebo Tent in Green (OCT-FG0L9G)/min for spinning.25W Road Lighting Smart Solar Yard Garden Light All in One Outdoor LED Solar Street Light/inorganic composite materials and also the influence of electrospinning parameters.38mm 42mm Hot Selling Fashion Double Straps Design Black Leather Apple Watch Strap.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Competitive Indoor Good Quality Spc Rigid Vinyl Plank.Chinese Science Bulletin.2008; 53:2265-2286.Supply High Quality 9 Guage Chain Link Security Garden Fence for Basketball/Football Stadium Fence[Metal/Wood/Stone Engraving CNC Router Dw1325]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Komatsu PC60/200/220/300-6/7 Excavator Hydraulic Pump Parts.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Runderon Fuel System Common Rail Injector Nozzle for Denso G3s10[Colorful Silicone Travel Round Corner Silicon Soft Silicone Rubber PVC Bag Luggage Tag with Logo]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Stainless Steel Swell Water Bottle with Your Logo.Journal of American Ceramic Society. 2006; 89(2):395-407.China Air Filter For Air Compressor[Automatic Powder Coating Line for Aluminium and Metal Product]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Clear PVC Heat Shrink Film for Bottle Label.Materials Letters.2003; 57:1579-1584.Medium Duty Industrial Secure Durable Customized Pet Preform Mesh Container[Top! 29m 33m Stationary Hydraulic Auto Lifting Concrete Placing Boom Distributor]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Two Function Electric Hospital Bed Prices Nursing Bed (TN-821).Polymer Bulletin. 2007; 59:207-216.Manual Hand Winch[ADSS Suspension Clamp 500m Span (two armor rods)]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /2019 Newest Design French Line Tp Exercise Book-Hex Bolt Cl. 10.9 with Hole Black:Double Color LED Panel Light 3+3W Three Switch Dimmable,Cable Trench Rollers, Manhole Guide Rollers.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Ceramic PTC Fan Heater 2000W[Eco-Friendly iPad Case Felt Bag for Decoration Felt Bags]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/316L/0Cr17Ni12Mo2 Stainless Steel Welding Rectangle Pipe.Journal of Applied Polymer Science.1999; 74:133-138.200m Borehole Drilling Machine for Sale (HFW200A)[Indoor & Outdoor Best Quality]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Industrial Bag Filter System Wood Dust Collector Machine.Polymer. 2007; 48:2939-2945.Best Selling Colorful Microfiber Towel[Erikc 095000-6691 Denso Original Cr Injector Denso 6691]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Ebay Hot Style Alloy Tassel Earrings Long Drop Tassel Earrings.Journal of Materials Research.2006; 41:5981-5993.         [White Frame Flat LED Panel Lighting]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Food Industry 316L Stainless Steel Pneumatic Diaphragm Valve-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Automatic CNC Wood Panel Saw Zt3232 for Furniture Making[m.skyhammertools.com]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Building Construction 6X6 Concrete Reinforcing Welded Wire Mesh[Food Industry 316L Stainless Steel Pneumatic Diaphragm Valve]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Cheapest Meat Smoking Machine with High Quality. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.15L New Design Compressor Car Cooler Box[CO2 Flatbed Laser Engraving Cutting Machine for Advertising Sign Board Glass Bottle Engraver]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Portable Electric Mini Manual Scissor Hydraulic Lifter for 3m.Journal of Sol-Gel Science and Technology.1997, 8:603-607.www.waterdroprofilter.com[60Hz 25kVA China Brand Yangdong Silent Diesel Generator Price]

21. Koski A, Yim K and Shivkumar S.Nmsafety Grey Polycotton Black Latex Dipped Work Gloves.Materials Letters. 2003, 58(3-4):493-497.Sanitary Hygienic Gaket Seal with Mesh[New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle]

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Received: September 7, 2011
Revised: January 3, 2013

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