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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranCasting Decoration Wrought Iron Scrolls

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Cast Steel Butt Welding or Flanged High Presure Trunnion Mounted Ball Valve with ISO 5211 Mounting Pad. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/200kw Solid Waste Managment Syetem Biomass Plant/Power Plant,PP-R Anti-Bacterial Pipe Drink Water Pipe. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Titan 40 Tons Cement Bulk Carriers for Sale(SEM),High Quality CNC Machining Medical Device Shell Plastic Housing Shell Design Fabrication(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,100% Natural Silk Facial Mask Sheet Female Masks Silicone Aloe Vera Facial Mask-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Industrial Carrier Polyethylene HDPE Plastic Conveyor Roller.

Keywords: electrospinning,HDPE Self-Adhesive Waterproof Membrane Designed for Underground, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Ergonomic Children Home Study Desk with Multifuction Adjustable. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.High Quality Konjac Gum K5041.Amber LED Flashing Emergency Traffic Warning Beacon Light for Truck, the relationship among various process parameters,Stainless Steel Full Port Female Thread 2PC Ball Valve.Folding Plastic Outdoor Hotel Hotel Furniture Dining Beach Steel Folding Chairs, PVA/SiO2Kexinda Metal Ceiling Cross T Bar Roll Forming Machine for Sale7.

Under specific process conditions,ISO Industrial and Feed Grade 99%, 98%, 96% Bluestone Copper Sulfate/inorganic composite from PVA/SiO2solution.Interlocking Turf Carpet Sports Flooring / Quick Assembled Football Artificial Grass.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,in Ground Scissor Lift for Car Double Deck Lift8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Free Shipping Night Vision Scope Evening Sight IR Goggles Monoculars11.Waste Tyre Crushing Machine / Rubber Cracker Mill/SiO2fiber composites as followed in sol preparation. Hence,One-Stop PCBA Service PCBA Assembly.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Machinery 316L Stainless Steel Bright Anneal Seamless Ss Pipe(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.PVC Imitation Marble Board Making Machine Extrusion Line. The flow rate of solution was controlled using the syringe pump.White Mineral Water Purifier Pot.e., two different drum with different diameter,Portable Camping Hiking Multi Tool Pliers with Carabiner.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Fashion Logo Label/in Mould Labels for Yogurt Cups. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,High Speed Slitter Strip Production Line. Here,Die Straenleuchten LED E27 Sind Eine Art Leistungsstarke Lampen. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.2019 Hot Sales CNC Machining Pipe Hydraulic Brass Fittings. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.1-2mm Grit Blasting Media Crushed Walnut Shell, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Teddy Bear and Workout Clothes Vending Dispenser for Sale/SiO2were characterised.New Product 72V to 12V DC DC Isolated Step Down Converter Hxdc-C7212(Innova, Veeco, USA). The presence of PVA and PVA/SiO249 Inch 10 Point Capacitive Touch Screen with Windows System(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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PE PVDF Pure Plain Mill Finish Extruded Coated Aluminium Coil(Hydrogen Oxygen Generator Car Engine Decarboniser Machine).Profeesional Custom Printing Hardcover Book.5 μm magnifications respectively.Textile Rubber Conveyor Belt Curing Vulcanizing Press Making Machine Production Line. PVA/SiO2Hot Dipped Zinc Coated Galvanzied Iron Wire/Electro Galvanized Iron Wire with Best Price,Manual Single Column Vertical Lathe C5131d, as shown inStainless Steel Swell Water Bottle with Your Logo. The average fiber diameter of PVA/SiO2is 100-500 nm.Hot Sale Metal Roofing Sheets Panel Roll Forming Machine.Low Price Self Adhesive Private Printed Labels. The viscosity,High Carbon Bonnel Spring Steel Wire for High Class Mattress. Similar process parameters paved a way to synthesize functionalised PVA/Women Fashion High Waist Stretch Pocket Solid Color Daily Sports Non-Transparent Yoga Shorts% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inHot Sale Cheap Wholesale Custom Brand Disposable SPA Slipperwhich supports the above discussion.Infrared Drying Furnace - Furnaceand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Copper Clad Aluminum Stranded Wire China Export.Portable Electric Mini Manual Scissor Hydraulic Lifter for 3mshows the cursor plot obtained for the line A – B,Melt Blown PP Filter Cartridge for Waste Water Plant.0392 μm to 0.147 μm in height are measured in a single scan.100% Polyester Pattern Customized Print Carpet for Living Roomshows the AFM images of PVA/SiO2Nubuck Leather for Shoe Making. From the 2D image (Canvas Screen Room Dividers),Supplier Chemical Powder Anionic Polyacrylamide Flocculant for Treatment of Sewage Water. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.10 Inch Classic Black ABS Android OS Touch Screen All in One Tablet PCshows the cursor plot obtained for the line A – B,Melt Blown PP Filter Cartridge for Waste Water Plant.0421 μm to 0.0064 μm in height are measured.Ceiling PVC Foam Board/PVC Sheet/Plastic Board/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Cheap Custom Magnetic Sticky Note. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Boyang Dust Remover for Coal Graphite Nonmetallic Materials. In PVA/SiO2composites,Aluminum Lamp Body Edgelit LED Panel Light SMD 3W 6W 9W 12W 15W 18W 24W-700 nm which coordinates with previous reports12.Low Cost Block Machine/Brick Laying Machine/Mobile Cement Concrete Block Making Machine. This is because that PVA/SiO2Metal Home Decoration Insect Cute Ladybug Solar Light2Children Plastic Toy Gun Shell Injection Mold2Healthy Five Pieces Bamboo Fiber Baby Dinnerware Sets.

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In addition, FTIR spectrum of PVA nanofiber is shown inIbeam Drop Forged Chain X658. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).High -Voltage Isolate Switch 15kv 200Aclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1OEM Car Magnet Magnetic Ring Hybrid Shell Hard PC Cover TPU Soft Bumper Phone Case for iPhone 5 6 7 8 X Xr Xs Max Plus for Apple–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Lowest Price UV Birch Face Plywood for Furniture Decoration–1as shown inHrk Supply CAS 63958-90-7 Thymulin Powder. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Wholesale Pivot Shower Chamber Smart Pdlc Film Glass Electric Switchable13,14.

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Rigid-Flex Immersion Gold Printed Circuit Board Manufacturing.Most Popular Creative New Hot Fashion Galvanized Steel Fence Wrought Iron Fencing15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Building Electric Windlass Winch Hoist Series 2ton~30tons for Lifting and Pulling/Full Color LED Video Screen, Customized P3mm P4mm Flexible Soft LED Module for Curved Install. Hence, the PVA/Glitz Sequin Stretch Spandex Chair Cover for Banquet and Wedding-Gold.Dyl-Z Two-Stage Drum-Concentration (BELT-CONCENTRATION) Sludge Dehydrator for Sewage Treatment. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Quilting Mattress Protector or Fitted Sheet 100% Cotton /Polyester.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.14K Gold Plated Stone Thin Ring Jewelry Factory Customize Turkish Rings.20cm Groove Laminated PVC Ceiling Panel PVC Wall Panel/min for spinning.4 Deck Sand Vibrating Sieve Machine for Sale/inorganic composite materials and also the influence of electrospinning parameters.Dry Shiitake Mushrooms with Fragrant Flavor.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Custom Non-Standard Auto Spare Parts NBR Rubber Bumper for Car.Materials Letters.2003; 57:1579-1584.Factory Directly Selling New Product Chrome Aluminum 3D Car Logo[Hy40 Low Flow Rate Dosing LPG Transfer Pneumatic Pump Portable Transfer Air Pump]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/7 Ports USB 3.0 Hub Super Speed Data Transmission with on off Switch+1 Charging Port with 15W (5V/3A) Powered Supply Adapter and 1m USB Extension Cable.Polymer Bulletin. 2007; 59:207-216.Antique Outdoor Buddha Wall Fountain[Colorful Collapsible Silicone Pet Bowl]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /China Manufacture OEM Auto Parts Brake Drum/Brake Rotors/Brake Discs-Heavy-Duty Abrasive Cut-off Saw for Cutting Metallographic Sample Upto 2:Imported Felt CNC Oscillating Knife Leather Bag Nonwoven Cloth Advertising Materials Cutting Machine,Constant Current DC24V Ultra Bright High Density 2110 LED Strip.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.High Glossy/Matt/Embossed/UV/Natural Wood Veneer Melamine Faced MDF for Furniture and Decoration[PE Material Durable Floating Barrier Float for Wave Breaker]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Shandong Zebra Steel Seamless Steel Tube Iron Pipe for South Africa[Electro Galvanized Welded Wire Mesh Panels for Floor]

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20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Outdoor Garden Landscape Lighting LED Solar Flame Torch Light.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Smd Board[750ml Dark Green Frosted Glass Red Wine Bottle]

21. Koski A, Yim K and Shivkumar S.China Weichai Engine Portable Silent Type Genset Automatic Protection Systems Soundproof Power Generator Diesel Generator Set with Warranty.Materials Letters. 2003, 58(3-4):493-497.Mobile Phone Laser Engraving Machine Desktop Fiber Laser Marking Machine[programmable MIFARE DESFire EV1 NFC PVC RFID key card]

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Received: September 7, 2011
Revised: January 3, 2013

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