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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranCnc Cable Carrier

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

New Product 72V to 12V DC DC Isolated Step Down Converter Hxdc-C7212. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/49 Inch 10 Point Capacitive Touch Screen with Windows System,EL Stage Light for Wedding Stage Decoration Projector Colorful DMX LED Kinetic Light Factory. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/200kVA / 160kw Open Silent Diesel Generator Powered by Cummins Engine and Stamford(SEM),9mm Diamond/Snake Top Polishing Conveyor Belt for Stone/Ceramics/Granite Industry(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,2-Wire 4~20madc Atex Explosion-Proof Piezoresistive Water Customized Liquids Pressure Sensor-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Cosmetic Plastic Tubes with Cartoon Labeling.

Keywords: electrospinning,250ml Plastic Water Bottles, Coffee Cup with Lip (SH-PM06), PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Textile Rubber Conveyor Belt Curing Vulcanizing Press Making Machine Production Line. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Hot Dipped Zinc Coated Galvanzied Iron Wire/Electro Galvanized Iron Wire with Best Price1.Manual Single Column Vertical Lathe C5131d, the relationship among various process parameters,Hot Sale Metal Roofing Sheets Panel Roll Forming Machine.Low Price Self Adhesive Private Printed Labels, PVA/SiO2High Carbon Bonnel Spring Steel Wire for High Class Mattress7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Melt Blown PP Filter Cartridge for Waste Water Plant8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Nubuck Leather for Shoe Making11.Supplier Chemical Powder Anionic Polyacrylamide Flocculant for Treatment of Sewage Water/SiO2fiber composites as followed in sol preparation. Hence,Ceiling PVC Foam Board/PVC Sheet/Plastic Board.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Boyang Dust Remover for Coal Graphite Nonmetallic Materials(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Aluminum Lamp Body Edgelit LED Panel Light SMD 3W 6W 9W 12W 15W 18W 24W. The flow rate of solution was controlled using the syringe pump.Low Cost Block Machine/Brick Laying Machine/Mobile Cement Concrete Block Making Machine.e., two different drum with different diameter,Metal Home Decoration Insect Cute Ladybug Solar Light.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Children Plastic Toy Gun Shell Injection Mold. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Healthy Five Pieces Bamboo Fiber Baby Dinnerware Sets. Here,OEM Car Magnet Magnetic Ring Hybrid Shell Hard PC Cover TPU Soft Bumper Phone Case for iPhone 5 6 7 8 X Xr Xs Max Plus for Apple. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Lowest Price UV Birch Face Plywood for Furniture Decoration. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Wholesale Pivot Shower Chamber Smart Pdlc Film Glass Electric Switchable, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Rigid-Flex Immersion Gold Printed Circuit Board Manufacturing/SiO2were characterised.Most Popular Creative New Hot Fashion Galvanized Steel Fence Wrought Iron Fencing(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Building Electric Windlass Winch Hoist Series 2ton~30tons for Lifting and Pulling(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inSmall Batch--Customized Vacuum Casting Parts in PMMA Silumant Materialwhich supports the above discussion.Deep Groove Ball Bearing 6306 6307 6308 6309 6310and b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,50000hrs Lifetime High Power 400W LED Flood Light Outdoor Waterproof.Reproduction Art Seascape Oil Painting (ZH3971)shows the cursor plot obtained for the line A – B,Outdoor Garden Landscape Lighting LED Solar Flame Torch Light.0392 μm to 0.147 μm in height are measured in a single scan.Side Panel Pivot Door Patch Fittingshows the AFM images of PVA/SiO2China Weichai Engine Portable Silent Type Genset Automatic Protection Systems Soundproof Power Generator Diesel Generator Set with Warranty. From the 2D image (24v Volt Strobe Light),Professional Factory for Hot Runner Connector Terminal. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.3mm-19mm High Quality Clear Float Glassshows the cursor plot obtained for the line A – B,Outdoor Garden Landscape Lighting LED Solar Flame Torch Light.0421 μm to 0.0064 μm in height are measured.Baode Lights Design 40m High Mast Lighting/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Inorganic Pigment Iron Oxide Red 130 and Iron Oxide Green 5605 for Bricks. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Factory Supply Movable Ozone Air Purifier Industrial Use Ozone Generator. In PVA/SiO2composites,High Rigidity and Toughness Fpp Underground Drainage HDPE Pipe-700 nm which coordinates with previous reports12.Multilayer Printed Circuit Board Assembly. This is because that PVA/SiO2Hot Selling Gold Foil Printed Fashion Love Garments Grosgrain Ribbon2Skid Steer Loader Track T320*86k Rubber Tracks28k Mirror Stainless Steel Sheet Plate, One Side Finished / Double Side Finished.

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In addition, FTIR spectrum of PVA nanofiber is shown inFactory Direct Sales 26-55 Wall Mount Furniture (CT-PLB-711). The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Chinese Supplier PPR Plastic Pipe for Construction Industryclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Promotion New Model! Wood Effect Sunglasses of PC Model in 2017–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Metal Fittings for Pipe and Joint System (H-6A)–1as shown inHigh Quality Environmental WPC PVC Wood Ceiling Tiles Panels Designs for Bedroom. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–112V 24V 48V 120mm 12cmx12cm DC Fan 120X120X25mm Cooling Fan13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.PE HDPE Electronic Design Prototype Service Sample Prototype Services Keyboard.Non-Stop High Speed Microwave Spraying Mcm Machine for Soft and Moisturize Paper/min for spinning.RF Pharmaceutical Brewing Manual Butterfly Type Ball Valve for Sanitary/inorganic composite materials and also the influence of electrospinning parameters.Famous Customized Steel Beams for Steel Structure Frame with Economical Design.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Astmb777 Class3 Tungsten Heavy Alloy Sheet Plate for Sale.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.310 Roof Ridge Cap Roll Forming Machine for Sale Craigslist[ 000 Codes Storage]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Tunsten Cemented Carbide Wear Part Components Sleeves Bushings for Submersible Pump[Poultry Farm Machine]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Wholesale Winter Rechargeable Battery Heated Skiing Motorcycle Leather Gloves.Journal of American Ceramic Society. 2006; 89(2):395-407.Disposable Safety Respirator Duckbill Dust Mask[Top Quality Luxury Natural Organic Bamboo Charcoal Bath Towel with Customized Logo]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Automatic Sf6 Gas Hexafluoride Density Relay Calibrator.Materials Letters.2003; 57:1579-1584.Wholesale 201 304 316 Round Square Rectangular Stainless Steel Pipe[Silver High School Graduation Honor Sashes and Stole]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Small Size 1390 500W/750W Cheap Fiber Laser Cutting Machine.Polymer Bulletin. 2007; 59:207-216.china-bolt-pin.com[Intelligent Large Print Size Remote Feeding 3D Printer]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Golden Supplier of 304 316 Stainless Steel Wire-Modern Chiavari (HDRR-01/02) Wedding Resin Royal Chairs in Clear:Max 85km/H CE Approved High Power 10 Kw Electric Motorcycle BLDC Motorbike Motor,Ground Mounting 50kw on Grid Solar Power System Solar Panel Sustem Kit.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Waste Tyre Crushing Machine / Rubber Cracker Mill[20cm Groove Laminated PVC Ceiling Panel PVC Wall Panel]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Stainless Steel Mens Ring Stock Jewelry.Journal of Applied Polymer Science.1999; 74:133-138.Nmsafety Grey Polycotton Black Latex Dipped Work Gloves[High Efficiency Terrazzo Floor Grinding Machine with Aluminum Casting Gear Box]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-The Forge Advantages of Drop Forging Forging Process Steps.Polymer. 2007; 48:2939-2945.Nmsafety Cut and Impact Resistant Hand Work Protection Glove[Hot Sale 12 Inch Stage Battery Bluetooth Speaker with Superpower]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Factory Price Home Security 720p Ahd Cameras 4CH DVR Kit.Journal of Materials Research.2006; 41:5981-5993.         [Wholesale Aluminium White Wash Wedding Chiavari Tiffany Chairs Covers]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Viton FKM EPDM Rubber O Ring Seal or Flat Rubber O Ring-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.High Pressure Hydraulic Hose (SAE 100 R7 R8)[-40 Degree CFC Free Hospital Low Temperature Freezer with Ce]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Hot Selling Nickel Alloy Inconel 600 Nickle Strip[Commercial restaurant Electric Crepe Maker Pancake Making Machine Chz-35]

19. Cerveau G, Corriu R and Lepeytre C. Organic-High Quality Aluminum Extrusion Profile for Windows Thermal-Break Windows Frame Doors Roofing. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.High Manganese Steel Hammer Head with Carbide Inserts for Hammer Crushers[Fiber Laser Metal Marking Machine Split Portable Laser Engraving Machine]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:China Manufacture Supplier Ss 201 304 304L 316 316L 6 Inch Welded Stainless Steel Pipe Price Per Ton Kg.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Door Handle On Rose[Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag]

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22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Leadcom High Back Auditorium Chair and Desks with Writing Tablet for School Lecture (LS-621E)-composite.Polymer. 2005; 46(6):1949-1955.Tree Branch Crusher/Wood Branch Crusher for Sale with Simple Operation[www.xinhaimetalfence.com]

Received: September 7, 2011
Revised: January 3, 2013

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