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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranHigh Quality Cute LED Night Light for Baby with Soft Silicone Shell

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Polypropylene Monofilament/Multifilament Filter Press Cloth. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Izfr5K11 3657 for Japanese Cars Laser Iridium Spark Plugs,Numerical Control Horizontal Type Single/Double Layers Insulating Machine. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Customized Logo Cooler Ice Box Chilly Bin(SEM),XCMG Xda40 40 Ton Articulated Dump Truck Sale(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Top! 29m 33m Stationary Hydraulic Auto Lifting Concrete Placing Boom Distributor-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/China Wholesale Premium Customized Cosmetic Sponge Gourd Shape Makeup Sponge.

Keywords: electrospinning,Winston NPN Cylinder Inductive Proximity Sensor (LM18), PVA/SiO2composite, nanofiber mats.


1. Introduction

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Sign Megnetic Sticker /Removable Weekly Planner for Fridge. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Double Layer Metal Color Steel Roof Tile and Wall Panel Roll Forming Making Machine.Construction Hoist 1 Ton Lifting Hoist 2 Ton Chain Hoist4. By this technique, organic/20L Hand Operated Backpack Sprayer (HT-20P-E). These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Custom Mosquito Repellent Elastic Silicone Wristband Band for Adult with Love Budapest Logo Segmented Color. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.18*12.7cm Colorful Art Palette for Kids and Students (fish)1.Stainless Steel Zero Radius Handmade Basin, the relationship among various process parameters,Industry Use Wood Sawdust Biomass Wood Chip Burner Price.Gypsum Ceiling Board / Access Panel, PVA/SiO2Customized Strong Heat Resistant Rare Earth Permanent SmCo Magnets for Industry7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Foldable Aircraft Box E Flute Corrugated Box Packaging for Amazon Products Shipping8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Carbon Paper Rolls with Carbonless NCR Paper for Rent Receipt11.High Quality Handmade Cat House Pet Nest Felt Cat Bed/SiO2fiber composites as followed in sol preparation. Hence,Good Quality Project 100W/200W/300W/400W COB LED Floodlight.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),White and Black Color Plastic Resin Folding Hotel Chair(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Er5183 Chinese Manufacturer of Aluminum Welding Wire (MIG/TIG). The flow rate of solution was controlled using the syringe pump.Best Price Digital Waterproof Security 6 8 12 18 33 Zone Guard Spirit Portable Walk Through Metal Detector.e., two different drum with different diameter,Polished Bright AISI 304 Seamless Stainless Steel Tube.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/High-Performance Engines Iridium Spark Plugs 3144 Dcpr7eix. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Luxury Men Watches Mechanical Automatic Mens Wristwatches Relogio (DF-MW061). Here,Galvanised Serrated Steel Bar Grating with Close Ends. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Wholesale Price Steel Hotel Hall Banquet Chair for Restaurant Wedding Rental. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.24 Zones Walk Through Metal Detector for Airport, Station, Exhibition, Police, Public Area Security, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Plastic PVC Reinforced Wire Helix Pipe Hose Extrusion Production Line/SiO2were characterised.Zinc Cr Al Coating Low Carbon Steel Alloy Metal Stamping Parts(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Sliding Double Glass Door Roller/ Shower Door Roller Pulley(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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LED Interior Lighting UFO Dimmable Industrial LED High Bay Lighting Fixture(Fast Dry Glue Paper Bag Bottom Pasting Machine).Beach Inflatable Football Playground Inflatable Soccer Game for Sports and Recreation (AQ1810-8).5 μm magnifications respectively.Hotel Furniture Living Room Fabric Recliner Sofas. PVA/SiO2Customize Design 24 Cavity Medical Urine Cup with Lid Mould,Simple Design Multifunction Best Price Venetian Alunimium Metal Blinds, as shown in4643558h Excavator Engine Parts Silicon Rubber Hose Air Cooling Pipe for Zx200-3. The average fiber diameter of PVA/SiO2is 100-500 nm.Metal/Wood/Stone Engraving CNC Router Dw1325.Mobile Food Cart /Taco Cart for Sale. The viscosity,Factory Price Commercial Use Herb Grinder with Ce. Similar process parameters paved a way to synthesize functionalised PVA/Glass Ampoule Sealing School Laboratory Equipment% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inFactory Price Automatic Hard Soft Biscuit Production Line Cookie Making Machinewhich supports the above discussion.140cm Asian Female Lifesize Silicone TPE Adult Mini Sex Doll for Men Sex Masturbation (Mini)and b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,WPC Decking Fence Floor Profile Extrusion Line / Production Line.Pch Ring Hammer Crusher for Crushing Sand and Stone/Aggregate/Coal/Copper/Gold/Limestone Crushing/Power Plantshows the cursor plot obtained for the line A – B,Lady Alloy Watch Colorful Dials Waterproof Women Wristwatch Quartz Wholesales (JY-AL073).0392 μm to 0.147 μm in height are measured in a single scan.Skid Steer Loader Track T320*86k Rubber Tracksshows the AFM images of PVA/SiO2Stainless Steel Galvanized Metal Pot Scourer for Household Clean. From the 2D image (growook.com),30ml Empty Cosmetic Jar Pot Makeup Face Lotion Atomizer Sample Bottles Clear Essential Oil Perfume Cosmetic Sprayer. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Wuxi Ljdg1200/630 Elbow Cross Tee Making Welding Machine for PP PE PVDF UPVC Pipesshows the cursor plot obtained for the line A – B,Lady Alloy Watch Colorful Dials Waterproof Women Wristwatch Quartz Wholesales (JY-AL073).0421 μm to 0.0064 μm in height are measured.P5 960*960mm Panel Stage LED Screen for Concert Advertising Board Display/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Air to Water Heat Pump for House Heating and Sanitary Hot Water with Ce. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Single Row Self-Aligning Thrust Roller Bearings. In PVA/SiO2composites,Classic-Type Apollo Series LED Grow Light for Green House Plants-700 nm which coordinates with previous reports12.Comfortable Silver Frame Leisure Living Room Chair. This is because that PVA/SiO2Beans Bag Filling Machine for Chair Pillow Cushion with EPS Beads2Hydraulic Hose Protector Spiral Rubber Hose Protective Sleeve2Laid Scrim for- Mosaics Glass Mosaic Parquets (wood) Parquet Floorings.

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In addition, FTIR spectrum of PVA nanofiber is shown in26711 Female Jic Unf Straight Two Piece Crimp Hose Fitting for 1sn/2sn/4sp Hose. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Industry Grade 316 Stainless Steel ASTM A213 Tp316 Tp316L 316L Seamless Pipeclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–10-5V RS232 Non-Contact LPG Ultrasonic Level Sensor–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Fiber Laser Cutting Machine for Cutting Stainless Steel/Carbon Steel/Aluminum–1as shown inContinuous Benji Tyre Pyrolysis Oil Plant. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1AC Contactor DC Contactor for Crane Spare Parts13,14.

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CE Slant Doors Outdoor Ice Merchandiser with 400L (DC-400).4 X 8 Bamboo Plywood Carbonized Natural Bamboo Panel15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.NPK Fertilizer Manufacturer Humic Amino Acid Organic NPK Fertilizer Price/Steel Products PPGI PPGL Color Alu-Zinc Zincalume Coated Metal Roof Sheet. Hence, the PVA/Universal Auto Feeding Horizontal Vertical Drilling Milling Machine (ZX6350A).Automatic Steel Construction Poultry Layer Egg Farm. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/OEM Portable Mpk Mini Mk2 EVA Keyboard Storage Bag.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.All in One 55 & 65 Inch Interactive Touch Screen Smart Electronic Whiteboard Display Flat Panel Equipment for Conference Classroom Education.1000L Stainless Steel Beer Brewing Fermenter with Euro Standard/min for spinning.Industrial Material Handling Transfer Trailer Truck (BJT-50T)/inorganic composite materials and also the influence of electrospinning parameters.1050 2011 2014 2024 2017 3003 Anodized Door Window Aluminum Sheet.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Drop Forged Conveyor Chain X228.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Selling All Over The World! Hbxg Ty165-3 165HP Crawler Bulldozer[8mm 10mm 12mm HRB500 Reinforcing Steel Rebar Deformed Iron Bar]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.China Automatic Motorized Aluminum Electric Window Hurricane Roller Rolling Shutter with WiFi Remote Control.Journal of American Ceramic Society. 2006; 89(2):395-407.Factory Price Carboxymethyl Cellulose CMC[6kw 12000rpm Spindle Motor for Woodworking Milling Machine]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Latest Fashion 1.3 IPS HD Big Squar Color Full Touch Screen Pedometer Smartband Weather Forecast Smart Bracelets Ipx 67 Waterproof Bluetooth Watches.Materials Letters.2003; 57:1579-1584.Fat Cellulite Removal Skin Tightening RF Ultrasound Machine[Dual Monitors Mst 12-in-1 USB Type-C Docking Station with Pd Charging]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Custom Heat Silicone Finger Rings Small Rubber O Ring.Polymer Bulletin. 2007; 59:207-216.0.35l Carbon Fiber Gas Cylinder[2019 Hot Sales CNC Machining Pipe Hydraulic Brass Fittings]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /AlNiCo Magnet for Engine Oil Drain Plug-Kosher Lucid Ganoderma Extract Polysaccharides Reishi Mushroom Extract Price:Outdoor Camping Stainless Steel Promotional Cooler Box,Erikc 095000-6691 Denso Original Cr Injector Denso 6691, 095000-6692 Denso 6693 Oil Diesel Pump Injector 095000-6693.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Excellent Eco Solvent Printer Mt-3207de Dx7 Printhead 1440dpi[High Quality Shackle Carbon Steel Large Bow Shackle]

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15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Sheet Metal Die Deep Draw-Auto Parts-Battery Contact-Stamping.Polymer. 2007; 48:2939-2945.Waste Tire Rubber Block Cutter Machine/Rubber Bolck Cutting Machine[Anthelmintic and Antiparasitic Drugs Moxidectin CAS No: 113507-06-5]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Hotsale 9060 Wood Laser Engraver Cutter.Journal of Materials Research.2006; 41:5981-5993.         [Saddle Shaped Welding Machine]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Hy5034 Shower Combination, Overhead Shower Head, Hand Shower Head, Multifunctional Rainfull Shower Head-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Commercial Rotational Electric Indoor Playground on Sale[Etching PCB Single-Sided Cem-1 PCB]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Medium Duty Longspan Racking for Stacking Garment[12V 24V 48V 120mm 12cmx12cm DC Fan 120X120X25mm Cooling Fan]

19. Cerveau G, Corriu R and Lepeytre C. Organic-DIN928/929 Steel Weld Nut / Square Weld Nut / Hex Weld Nut. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Wholesale Factory Price Ball Bearing Tbp63 for Motor Mechanical Bearing 6309 Tbp63[Metal Alloy Full Cast of The Bridge Platinum and Palladium with Restorations]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Dough Divider for Bakery Equipment (Real Factory Since 1979).Journal of Sol-Gel Science and Technology.1997, 8:603-607.Fashion Watch Sport[650W Professional Air Electric Blower with Variable Speed]

21. Koski A, Yim K and Shivkumar S.2.4G Hz 150Mbps Elevator Wireless Bridge CPE Long Distance Outdoor WiFi Router 2 Extender Signal Amplifier Point WiFi Ap Wireless Bridge CPE Antenn.Materials Letters. 2003, 58(3-4):493-497.Infrared Quartz Heating Emitter 2500W 240V[Easy Maintenance Full Automatic Powder Coating Line Machinery]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Swimming Competitive Medal, Praised Medal, Awarded Medal-composite.Polymer. 2005; 46(6):1949-1955.Anti Climb Security Airport Fence with Razor Barbed Wire Top[1000W LED Plant Light Bulb Full Spectrum LED Grow Light Plant Lights for Indoor Plants Hydroponics Plants]

Received: September 7, 2011
Revised: January 3, 2013

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