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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


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Keywords: electrospinning,38mm 42mm Hot Selling Fashion Double Straps Design Black Leather Apple Watch Strap, PVA/SiO2composite, nanofiber mats.

1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Cable Trench Rollers, Manhole Guide Rollers. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.316L/0Cr17Ni12Mo2 Stainless Steel Welding Rectangle Pipe1.Industrial Bag Filter System Wood Dust Collector Machine, the relationship among various process parameters,Ebay Hot Style Alloy Tassel Earrings Long Drop Tassel Earrings.Food Industry 316L Stainless Steel Pneumatic Diaphragm Valve, PVA/SiO2Cheapest Meat Smoking Machine with High Quality7.

Under specific process conditions,Portable Electric Mini Manual Scissor Hydraulic Lifter for 3m/inorganic composite from PVA/SiO2solution.Nmsafety Grey Polycotton Black Latex Dipped Work Gloves.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,C10100 Cw008A of-Cu T2 Copper Wire in Coils with Bright Surface8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Indoor 9*10W Battery Powered Wireless LED Flat PAR Light11.Excellent Eco Solvent Printer Mt-3207de Dx7 Printhead 1440dpi/SiO2fiber composites as followed in sol preparation. Hence,High Quality Environmental WPC PVC Wood Ceiling Tiles Panels Designs for Bedroom.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Experienced Graphite Electrode Manufacturer on Made in China(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Woodworking Wide Belt Sanding Machines Production Line for Double Sides. The flow rate of solution was controlled using the syringe pump.Blue Non Woven Cloth Suit Garment Bag Cover with PVC Window.e., two different drum with different diameter,Luxry Big Door Handle, Stainless Steel Glass Door Handle Without Lock.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/3 Ton Lifting Magnet Permanent Magnetic Plate Lifter. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Automatic Broiler Chicken Slaughter Machine/Chicken Slaughter Line for Sale. Here,Professional 1400W Industrial Mixer for Sales. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Plastics EPE Foam/Foaming/Foamed Sheet Extruder/Making Machine/Machinery. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Medical White Industrial Kiosk IP65 Waterproof IR Touch 19 Inch Open Frame Touch Screen Monitor, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.


Beautiful Customized Mobile Food Cart, Fast Food Van Trailer Truck/SiO2were characterised.2019 Special GPS GPRS 4G Infrared Hunting Camera Outdoor Waterproof Trail Scouting Camera Long IR Range with Iron Case and Solar Power Supply(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Metal Strip Thickness Gauge(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inDomestic RO System with Coverwhich supports the above discussion.2018 Mobile Phone Fast Charge Qi Wireless Chargerand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Automatic Horizontal Flow Wrapper/Wrapping Pillow Bakery/Bread Packing Packaging Machine Made in China (AHP-500-S3).High Speed Eco Friendly Degradable Corn Starch HDPE LDPE Biodegradable Trash Coreless Rolling Garbage Flat Plastic Bag Making Machineshows the cursor plot obtained for the line A – B,Shockproof PP Plastics Hollow Corrugated Board /Sheet.0392 μm to 0.147 μm in height are measured in a single scan.Industrial Carrier Polyethylene HDPE Plastic Conveyor Rollershows the AFM images of PVA/SiO2Dyeing Woven Fabric Dyed Poly Cotton Twill Tc 65/35 Workwear Uniform Overall Fabric. From the 2D image (High Strength Floor Level Underlay MGO Board),2019 Jomo Lite 60 Vape Kit 1600mAh Electronic Cigarette. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Autumn and Winter Women Knitted Scarf Fringed Twill Shawl Lady Scarf Men Scarfshows the cursor plot obtained for the line A – B,Shockproof PP Plastics Hollow Corrugated Board /Sheet.0421 μm to 0.0064 μm in height are measured.Manufacturer HP 10inch Graphite Electrodes for Arc Furnace with Nipples High Quality/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Stretch UV Resistant Hay Baling Plastic Film Silage Roll. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.2019 Hot Sale Customized Painting Line Color Spray Coating Production Equipment Automatic UV Spray Line. In PVA/SiO2composites,Tws V5.0 Aviation Stereo Headphones Best Earphone Earpods Earbuds MP3 Waterproof Bluetooth Wireless Headset-700 nm which coordinates with previous reports12.Chademo/CCS DC and AC Intergrated EV Charger for EV Charging Station. This is because that PVA/SiO2Laser Die Board Cutter for Wooden Die From Yitai Die Making2Factory Wholesale Customized Cheap New Plastic Antique Soft PVC Zinc Alloy Die Casting Laser Engrave Bottle Shape Magnet Keyring Beer Bottle Opener2Plastic PVC Drainage Conduit Water Pipe Belling Machine/Socketing Expander.

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In addition, FTIR spectrum of PVA nanofiber is shown inAC 3 Phase 0.55kw Vibrating Screen Motor with NSK Bearing (YZUL30-4). The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Wire Braided Oil Hydraulic Hose SAE 100r2at 1/4 3/8 5/8 3/4 1clearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Rotary Hydraulic Actuators Price–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Slim Metal Frame Glass Mobile Phone Case with Magnet Flip Cover for Apple iPhone X–1as shown in176mm Bio Biodegradable Lady Pad Panty Liner. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Socket Type HDPE Pressure Pipe Fittings Male/Female Coupling13,14.

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Black Carbon Welded Square Steel Pipe.Wholesale Project Home Waterproof 12mm Reinforced Composite Laminate Flooring15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Fiber Cable Trunk or Fanout MPO Cable/RF Facial Machine Face Lifting Wrinkle Remover Home Use Machine. Hence, the PVA/Customized colorful cute animal wholesale promotional funny stuffed graduation owl plush toy.Die Cast Zinc Alloy Gold Plated Half Marathon Medal for Promotion Sale (160). The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Newest Green Blue Plastic Frame Reading Glasses.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.2018 Spring Fashion Waterproof Outdoor Hoody Rain Jacket.Large Scale Countertop Stone Granite Edge Profiling Machine/min for spinning.ASTM A312 304L Stainless Steel Pipe Price with Cheap Price/inorganic composite materials and also the influence of electrospinning parameters.New Bone China Glaze Pure White Porcelain Glass.


The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).


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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.White Metal Babbitt Sliding Bearing Bush /Shoe / Pillow for Cement Mill.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.140cm Asian Female Lifesize Silicone TPE Adult Mini Sex Doll for Men Sex Masturbation (Mini)[Pch Ring Hammer Crusher for Crushing Sand and Stone/Aggregate/Coal/Copper/Gold/Limestone Crushing/Power Plant]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Skid Steer Loader Track T320*86k Rubber Tracks[Wuxi Ljdg1200/630 Elbow Cross Tee Making Welding Machine for PP PE PVDF UPVC Pipes]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Carbon Fiber Stainless Steel Exhaust Muffler Tip.Journal of American Ceramic Society. 2006; 89(2):395-407.Auto Stamping Car Parts with Quick Delivery Time[Hot Sale Unisex Outdoor Water-Resistant Winter Thinsulate Ski Cycling Gloves]

10. David YL, Michael A, Richard JA, Vohden Junior D, Chen and David CM. Tailored nanofiber morphologies using modulated electrospinning for biomedical applications.Material Research Society Symposium Proceedings. 2003. 736:D3.8.1-D3.8.6.         [Drum Inductor with 2+2 Pin Base Holder]

11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Soft PVC Super Clear Film for Window Usage.Materials Letters.2003; 57:1579-1584.Natural Ingredients Pure No-Calorie Sweetener Additives Stevia Extract for Food Beverages[26711 Female Jic Unf Straight Two Piece Crimp Hose Fitting for 1sn/2sn/4sp Hose]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Industrial High Pressure High Temperature Heat Exchanger as Excavator Hydraulic Oil Cooler.Polymer Bulletin. 2007; 59:207-216.D-Isoascorbic Acid[Industry Grade 316 Stainless Steel ASTM A213 Tp316 Tp316L 316L Seamless Pipe]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Hot Sale Eco Friendly XPE Interlocking Floor Baby Play Mat-New Type Round Ball Granular Fertilizer Making Machine:Heavy Duty 2: 1 A4 Size Wire Punching and Binding Machine Cw300t,China A36 Q235B S275 Ss400 Anti-Slip Checkered Ms Carbon Steel Plate.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Continuous Benji Tyre Pyrolysis Oil Plant[13-18 Cubic Meter Waste Garbage Compactor Truck for Sale]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Oil Resistant U-Type Rubber Seal.Journal of Applied Polymer Science.1999; 74:133-138.Dressing Bag[Manhole Cover Composite]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-New Products LED Solar Deck Post Fence Step or Dock Garen Light.Polymer. 2007; 48:2939-2945.2.5mm Sheet Metal Press Brake Machine 125ton Plate Bending Machine[Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/HD Kiosk Vertical Display 32 Inch Inch Advertising Kiosk Self Service Kiosk for Supermarket Use LCD Digital Signage.Journal of Materials Research.2006; 41:5981-5993.         [Best Price 2 Ball Valve 110mm Handle Directional Valve PVC Ball Valve]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Rubber Mixing Mill/Two Roll Open Mill/Rubber Mixing Machine-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Customized Rubber Gasket Rubber Grommet in NBR SBR Silicone etc.[Custom Colorful Food Grade Silicone Rubber Seal O Ring]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Wholesale Flying CO2 High Speed Online Laser Marking System[Outdoor Waterproof Camping/Hiking/Travel Rucksack Back Pack Bag]

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21. Koski A, Yim K and Shivkumar S.ABS Safety Padlock Lockout Tagout Kit Form Padlock Manufacturing Company.Materials Letters. 2003, 58(3-4):493-497.Tempered Safety Anti-Slip Laminated Glass Stair Treads[Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bag]

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Received: September 7, 2011
Revised: January 3, 2013

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