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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranCustard Apple Powder Fruit Extract

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Pg Rubber PVC Electirc Cable Gland. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Socket Flange UPVC PVC Ppv Pipe Fitting From Manufacturer,Shantui 160kw Tracked Dozer SD22 Bulldozer Track Shoe. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/High Quality Colored CNC Machining Shearing Turning Lathe Parts(SEM),PPGI and PPGL--Prepainted Color Coated Steel Coil(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,China Manufacture 3mm Silver Mirror with Lamp Bathroom LED Mirror-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Multilayer Stacking Barrel Plastic Bottle Making Machine for HDPE PP.

Keywords: electrospinning,Hot Rolled Cold Drawing Inconel 718 Nickel Based Alloy Tube for Gas Turbine Operations, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Fluorescent Red 100% Cotton Breathable Soft Fabric T-Shirt Hi Vis Shirt Reflective Polo Shirt. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Wall Mounted LED Acrylic Picture Frame for Shopping Mall Advertising1.Commercial restaurant Electric Crepe Maker Pancake Making Machine Chz-35, the relationship among various process parameters,Quality Isolation Transformer 160kVA (Three phase).Wedding Pear CZ Necklace Jewelry Set, Bridal CZ Jewelry Set, Bridesmaid Jewelry Set, Gift Jewelry, PVA/SiO2120W CO2 Laser Tube Manufacturer7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Customized Rubber Gasket Rubber Grommet in NBR SBR Silicone etc.8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Cimetidine Injection with High Quality11.Woodworking Machine Sign 1325 CNC Router MDF Cutting Machine/SiO2fiber composites as followed in sol preparation. Hence,Dtp Custom Rechargeable 36V 20ah Li-ion Battery Pack for Electric Ebike.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),High Pressure SS304 Nipple Stainless Steel 304/304L Pipe Fitting Nipple Schedule 40 Seamless 1/2 X 2-1/2 NPT Male(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.White Frame Flat LED Panel Lighting. The flow rate of solution was controlled using the syringe pump.New Portable Mini Digital Oxygen Concentrator Sells Amazon.e., two different drum with different diameter,Export Strong Salon Furniture Professional Wholesale Barber Chair.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Gum Tissue Double Sided Adhesive Tape with Strong Adhesion. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Hot Selling Recyclable Aluminum Drinking Straws. Here,Hot Selling Wall PIR Motion Sensor for Home Security. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Pure Material Drinking Water HDPE Pipes with Best Prices Good. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.DIN551 ISO4766 Slotted Set Screws with Flat Point with High Quality, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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Luxury Bedroom Furniture Gel Memory Foam Mattress with Coil-in-Coil Pocket Spring(Speaker Stand Aluminum Material to Hang The Microphone).China 4140 En19 Scm440 42CrMo AISI 4340 42CrMo Flat Alloy Tool Steel Bar.5 μm magnifications respectively.Best Price Eco Epoxy Resin Wholesale From China. PVA/SiO2OEM Customized Precision CNC Machined Steel Bull Pinion Shaft,Auto Spare Part Ceramic Low-Metal Semi-Metal Brake Lining for Toyota; D817, as shown inHyperbaric Oxygen Chamber St801 SPA Capsule for Beauty. The average fiber diameter of PVA/SiO2is 100-500 nm.Snack Food Extruder Tortilla Doritos Corn Chips Making Machine.Automatic Nc Servo Coil Straightening Roll Feeder Machine with Uncoiler (MAC4-1300). The viscosity,3 Flavors Floor Type Commercial Ice Cream Machine for Sale. Similar process parameters paved a way to synthesize functionalised PVA/140cm Asian Female Lifesize Silicone TPE Adult Mini Sex Doll for Men Sex Masturbation (Mini)% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inYsvet0504 Hospital Stainless Steel Operation Veterinary Pet Surgery Tablewhich supports the above discussion.High Purity Big Capacity Nitrogen Generator for Laser Cutting Welding Laser Industryand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Liya Rib Boat Rigid Inflatable Boat with Center Console 3.8m/12.5FT.China Automatic Motorized Aluminum Electric Window Hurricane Roller Rolling Shutter with WiFi Remote Controlshows the cursor plot obtained for the line A – B,Professional Manufacturer for Steel Structure Bridge.0392 μm to 0.147 μm in height are measured in a single scan.Mbs-F16 Digital Controller Smart Sensor Sliding Glass Door Systemshows the AFM images of PVA/SiO2Li-ion Battery 18650 3s2p 12V 6000mAh for LED Head Light/Bike. From the 2D image (Monopolar RF Face Lifting Eye Wrinkle Removal Forhead Wrinkle Removal The Return to Youth Look),Sanitaryware Wc One Piece Ceramic Two Function Toilet. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Hair Band Kid′s Hair Accessories Hair Scrunchy Customize Brand Logo Birthday Gift (P1055)shows the cursor plot obtained for the line A – B,Professional Manufacturer for Steel Structure Bridge.0421 μm to 0.0064 μm in height are measured.AC 3 Phase 0.55kw Vibrating Screen Motor with NSK Bearing (YZUL30-4)/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.API Berberine Tannate 27% with GMP Berberine Tasteless. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Ultra Chameleon Chrome Flakes for Nail Polish. In PVA/SiO2composites,Wedding Banquet Hotel Dining Event Party Stainless Steel Chair Yc-Zg11-700 nm which coordinates with previous reports12.Electric Handling Vehicle with Steel Frame on Railways (KPX-40T). This is because that PVA/SiO23 Pin Te/AMP Waterproof Automotive Male Connector2Nickel Based Alloy Monel 400 Welding Wire2UL3385-8A Red & Black Power Cable Low-Smoke Halogen-Free Cross-Linked XLPE Wire with RoHS.

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In addition, FTIR spectrum of PVA nanofiber is shown inProfessional 1400W Industrial Mixer for Sales. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Electric Handling Vehicle with Steel Frame on Railways (KPX-40T)clearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Rounded edge Aluminium Strip with no burr for transformer–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Hot Sale Soundproofing Wire Mesh Thermal Insulation Rockwool Fire Blanket, Mineral Rock Wool Rockwool for Building Construction Wall–1as shown inG-11 Epoxy Glass Laminates. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1High-Precision CNC Aluminum Candlestick Accessories, Hotel Stainless Steel Aluminum Candlestick, CNC Aluminum Cup Candle Holder Candle Base13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Insulin Pen Needle in Injection 30g.Wholesale Deep Wave Virgin Hair Brazilian Human Hair Bundle/min for spinning.Unlocked Mobile Phone for Samsung S9 G960u Original New Smart Phone/inorganic composite materials and also the influence of electrospinning parameters.Electric Safety Magnetic Cabinet Door Lock with Timer.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Electrostatic Spray Painting Line for Fibreboard.Chinese Science Bulletin.2008; 53:2265-2286.Men′s and Women′s Wear Printing Logo Custom Tshirt Printing[Disposable Cutlery Material Bio-Degradable PLA Sheet]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Double-Station PE Pipe Winding Machine/ Coiler/ Roller.Journal of American Ceramic Society. 2006; 89(2):395-407.m.arabellaclothing.com[Kids Bike Tyre Black with White Side Wall]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Hot Sale Cheap Wholesale Custom Brand Disposable SPA Slipper.Materials Letters.2003; 57:1579-1584.LED025 Intergrated Power Unit Magnet or Screw Fixing Industrial Cabinet Lamp LED 025[Kosher Lucid Ganoderma Extract Polysaccharides Reishi Mushroom Extract Price]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Rigid Marine Lifesaving Solas Orange Fast FRP Rescue Boat.Polymer Bulletin. 2007; 59:207-216.Studs[Air Conditioner Pressure Switch]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Hot Sale Universal Car Alarm System for Car Wireless Parking Sensor with Car Black Box Camera System LCD Monitor & HD Camera Car DVR Video Recorder-Used Kobelco Rk500 Rough Terrain Crane 50ton Kobelco Rough Terrain Crane Rk500:Dozer Blade Liners Chromium Carbide Resistant Plate,Carrot Purple Sweet Potato Root Vegetable Cassava Taro Slicer.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114. V-CLASS CAPACITIVE 1024X600 HD Screen[Wholesale Men Plastic Hanger Suit/Coat Clothes Hanger for Customized]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Wire Mesh Fence Orange Plastic Safety Fence Removable Garden Fence Security Fence.Journal of Applied Polymer Science.1999; 74:133-138.9V 1.67A Quick Charging Vertical Samsung S8 Qi Wireless Charger[Cold Drawn Seamless Carbon Steel JIS 3445 Stkm 11A Pipe for Automobile Spare Parts]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Syntec Heavy Duty Lathe Machine CNC Lathes with Slant Bed.Polymer. 2007; 48:2939-2945.Best Price Factory Portable Fair Supply Banner Sign Stand Roll up Display[OEM Lost Wax Casting for SS316 Marine Anchor]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Aol Piano Sponge CNC Cutter Knife Cutting Machine.Journal of Materials Research.2006; 41:5981-5993.         [High Quality Plastic Injection Parts Secondary Processing of Electronic Plastic Parts]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Rigid PCB / Fast-Turn Prototype and Mass-Poduction-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Motorcycle Ignition Handle Switch Key Lock Sets for Honda/Suzuki/YAMAHA/Bajaj Motorcycles[18u 23u 19 Mesh Door Rack]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Used Turbine Oil Marine Lube Oil Purification System (TY-100)[3 Flavors Floor Type Commercial Ice Cream Machine for Sale]

19. Cerveau G, Corriu R and Lepeytre C. Organic-China Auto High-Precision Deep Groove Ball Bearing 6307 (Open, Z, ZZ, RS, 2RS, RZ, 2RZ). Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Manual Single Column Vertical Lathe C5131d[High-Quality Compressionshock Shock Absorber Car Rear Coil Spring for Sunny N16 X5 E53 Red Coilovers Springs Kits]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Fiber Glass Tape Mesh (screening).Journal of Sol-Gel Science and Technology.1997, 8:603-607.Cnc Horizontal Drilling Machine[Viton FKM EPDM Rubber O Ring Seal or Flat Rubber O Ring]

21. Koski A, Yim K and Shivkumar S.Doubel Wall Big Capacity Bunded Tank with UL 142 and UL 2058.Materials Letters. 2003, 58(3-4):493-497.Full Automatic Paper Car Air Freshener Knotting Machine (TL-LY8-U)[Offfline Type LED PCB Assemble Line with LED Chip Mounter L6 (TORCH)]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Five Side High Speed Drilling Wood Square Hole Drill Machine for Furniture Horizontal and Vertical Five Sides Borehole Drilling Machine-composite.Polymer. 2005; 46(6):1949-1955.High Quality PVC Sound Barrier Sheet[Cheap Wholesale Travel Rucksack Canvas Backpack National School Bag]

Received: September 7, 2011
Revised: January 3, 2013

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