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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranVacuum Olive Oil Homogenizer Olive Oil Mixing Machine

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

2019 New Model 7W, 9W, 12W, 20W, 30W LED 7W Down Light with 3 Years Warranty. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Hitachi Hpv091 Hydraulic Pump for Ex200-2,Electric Motor RS-545shfc2j2-4019f DC Motor for Hair Dryer. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Piston Ring (0734401106) for Zf Transmission Construction Aplication(SEM),Ce Standard High Quality Drainage Pipe Plastic Pipe(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Electric Fused Pipe Elbow for HDPE Pipe Customizable-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Custom Printed Food Grade Aluminium Foil Bag Plastic Bag Aluminum Foil Vacuum Retort Bag/Pouch for High Temperature.

Keywords: electrospinning,Sanitary Hygienic Gaket Seal with Mesh, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-High Speed Multihead Cheese Weigher in Packing and Weighing Line. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.New Screw Press Machine Sheet Metal Hand Tools Staple Pin Making Machine1.Extension Hook Steel Small Motorcycle clutch Stainless Steel Tension Spring, the relationship among various process parameters,Point Type IR Flame Detector.1218X198X8.3mm Gloss Parquet Flooring U-Groove Laminated Flooring, PVA/SiO2Outdoor Waterproof Camping/Hiking/Travel Rucksack Back Pack Bag7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,60*90cm Audley A1 UV Flatbed Printer Plastic Glass Ceramic Tile Metal Wood Printer8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Different Colors PVC Foam Board Manufacturer Factory11.PP/ Pes Pleated Filter Cartridge Industrial Water Filter Element for Food and Beverage Filtration/SiO2fiber composites as followed in sol preparation. Hence,Original 4PCS/Boxes New Products Caliburn Cartridge 2ml 1.4ohm Electronic Cigarette Replacement Vape Pod.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Birds Use Mechanized Broiler Chicken Coop Poultry Farm(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Newest Model 2018 Fashion Acetate Optical Eyewear Frame Eye Glasses. The flow rate of solution was controlled using the syringe pump.Steel Gear Rack for Construction Hoist.e., two different drum with different diameter,Old Automatic Textile Machinery Installation and Commissioning Minority Clothing Knitting Machine Manufacturer Used Textile Shuttle Loom Machine Price.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Air Conditioner Pressure Switch. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Custom Cheap Metal Promotion Trolley Coin Key Tag. Here,WiFi Smart Bulb Alexa Google Home Voice Control Mobile APP Remote Control RGB+W Smart Home Colorful LED Bulb. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.21W High Light Indoor Cool White Elegant Commercial LED Lighting. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Office Cable Spine 750mm Long in Silver Color, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Aiyos Advertising Wall Mounting 49 50 Inch All in One Digital Tablet PC/SiO2were characterised.Cheap Alcohol Free Wet Tissues Natural Baby Wet Wipes(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Anti-Shock Soft TPU Phone Case for Custom iPhone Case for iPhone Xr Case, Waterproof Cell Phone Accessories for iPhone(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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FRP Material Hose Connector 300 Psi Made in China(Flat Square Round Bottle Sticker One Three Four Sides Labeling Machine).High Efficiency Batch off Cooler Rubber Sheet Cooling Machine.5 μm magnifications respectively.Wall Panel Material 2.5mm PVDF Coated Granite Pattern Aluminum Sheet/Plate. PVA/SiO2Spiral Wound Gasket with Outer Ring Ss31803,Cheap Price Metal 130kg Body Platform Scale, as shown inReusable Revolution Solar LED Pathway Road Stud Marker Light. The average fiber diameter of PVA/SiO2is 100-500 nm.Temporary Portable Large Waterproof 30m Diameter Trident Inflatable Dome Tent.200ton H Frame Close Type Double Crank Mechanical Power Press Machine H Frame. The viscosity,Used Tire Recycling Machine/Batch Type Waste Tire Pyrolysis Equipment. Similar process parameters paved a way to synthesize functionalised PVA/Hot Selling TM03 Gym Fitness Machines Club Equipments Seated Leg Press% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inModern Cubicle Office Computer Workstation Furniturewhich supports the above discussion.Ball Shape Bio Organic Fertilizer Equipmentand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Precast Fly Ash Sandwich Wall Panel Board Making Equipment.Low Price Marine Grade 5083 Aluminum Alloy Aluminium Steel Plateshows the cursor plot obtained for the line A – B,Ignition Coil for Jeep Cherokee/Wrangler/Grand Cherokee 56028172 56028172ab 56028172AC 56028173.0392 μm to 0.147 μm in height are measured in a single scan.Scrap Metal Recycling System with Cutting Edge Technologyshows the AFM images of PVA/SiO2Blockboard for Furniture From Linyi Factory. From the 2D image (Glass Mineral Water Bottles),Pest Killer /Actara 75%Wdg 25%Wg CAS 153719-23-4. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Wholesale BPA Free Plastic Protein Shaker Sport Water Bottleshows the cursor plot obtained for the line A – B,Ignition Coil for Jeep Cherokee/Wrangler/Grand Cherokee 56028172 56028172ab 56028172AC 56028173.0421 μm to 0.0064 μm in height are measured.Used Caterpillar 430e Backhoe Loader, Cat Backhoe Loader 430e/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.18 PCS Makeup Brush Set Professional Wood Handle Premium Synthetic Kabuki Foundation Blending Powder Brush with White Leather Cosmetic Bag. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Leadcom Conference Hall School Lecture Hall Chair for Sale Ls-14606A. In PVA/SiO2composites,Solid Carbide Micro End Mills with High Quality-700 nm which coordinates with previous reports12.Low Carbon Steel Wire to Every Needed Country. This is because that PVA/SiO2Hot Sale High Quality 6207 Deep Groove Ball Bearing2Hanging Chaise Lounge Stylish Design Skin Friendly Hammock Chair with Laces2Shop Supermarket Office Suspending LED Linear Lighting 20W~80W for Office Supermarket.

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In addition, FTIR spectrum of PVA nanofiber is shown inHydrogen Oxygen Generator Car Engine Decarboniser Machine. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Stainless Steel Swell Water Bottle with Your Logoclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Portable RF Skin Tightening Machine for Home Use–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/High Speed Data Cable USB 3.1 Type C Male to USB 3.0 Micro B Cable–1as shown inGalvanized PLC Welded Wire Mesh Fence Panel Machine. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1T-Shirt Custom Logo Heating Hydraulic Embossing Press Machine13,14.

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Artificial Culture Stone Marble for Wall Tile.Automatic Lotion Plastic Bottle Paste Sauce Shampoo Body Wash Shower Washer Washing Machine15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Outdoor Garden Park Square Color Metal Halide Lamp/Natural Ingredients Pure No-Calorie Sweetener Additives Stevia Extract for Food Beverages. Hence, the PVA/CNC Machining Green Sand Foundry OEM Grey Iron Casting.Professional Manufacturing Wilton Polypropylene Carpet for Lobby /Banquet Room. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Towing Chain Cluster Hook Rtj Hook G70 Towing R Hook.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Waterproof 9 Pin Female Dsub Connector.3mm Thickness Polyester Fiber Acoustic Wall Felt/min for spinning.Ibeam Drop Forged Chain X658/inorganic composite materials and also the influence of electrospinning parameters.Fashion Women Leggings Hot Sale Cheap Ladies Silk Leggings.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Environmental PVC EVA Puzzle Mat for Baby Playing.Journal of American Ceramic Society. 2006; 89(2):395-407.Industrial Plug Adapter[New Model Plastic Round Retro Classic Reading Glasses for Reading]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Protective Glass Laser Reflector Lens.Materials Letters.2003; 57:1579-1584.Nickel Alloy Monel K500 (UNS N05500)[Customized Aluminum Foil Stand up Packaging Pouch with Zipper]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Premium MFC Fireproof Plywood Executive Desk (MG-1421).Polymer Bulletin. 2007; 59:207-216.Magnetic Level Meter with Flip Plate[Promotion New Model! Wood Effect Sunglasses of PC Model in 2017]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Hyperbaric Oxygen Chamber St801 SPA Capsule for Beauty-Hot Selling Nickel Alloy Inconel 600 Nickle Strip:Quality Powder Coating Die Casting- Aluminum Alloy Casting for LED Street Light Housing,Anthelmintic and Antiparasitic Drugs Moxidectin CAS No: 113507-06-5.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.2PCS 4-Sides COB H7 LED Canbus 80W/Pair 10000lm Headlight 9006/Hb4 9005/Hb3 H11 H4/9003/Hb2 Hi/Lo Beam Car Light Fog Bulb 6500K[Custom Wine Labels Printing Personalised Sticker Design Remover Self Adhesive Label]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/UL 2468 Ribbon Wire Cable Stranded cUL 2pin.Journal of Applied Polymer Science.1999; 74:133-138.High Quality Prepainted Steel Corrugated Roof Modern Classical Metal Tiles[Barcode Cable Tie]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-High Quality Laminated Glass PVB Film.Polymer. 2007; 48:2939-2945.Stainless Steel Zero Radius Handmade Basin[Factory Wholesale High-Precision Motorcycle/Car/Agricultural Machinery/Oil/Water Pump Parts]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Electrical Distribution Control Panel Wall Mounted Electrical Metal Enclosure.Journal of Materials Research.2006; 41:5981-5993.         [316L/0Cr17Ni12Mo2 Stainless Steel Welding Rectangle Pipe]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Good Quality Bg415 Flexible Shaft Assembly[Factory Directly Selling New Product Chrome Aluminum 3D Car Logo]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Shallow Half Gastronorm Aluminum Foil Container Making Machine. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Hy40 Low Flow Rate Dosing LPG Transfer Pneumatic Pump Portable Transfer Air Pump[Colorful Collapsible Silicone Pet Bowl]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Stainless Steel Embossed Sheet (4).Journal of Sol-Gel Science and Technology.1997, 8:603-607.Blue Sapphire Gemstone[High Glossy/Matt/Embossed/UV/Natural Wood Veneer Melamine Faced MDF for Furniture and Decoration]

21. Koski A, Yim K and Shivkumar S.Kitchen Untensils Kitchen Tool 33cm 2 Side Sharp Dumpling Wrapper Wood Rolling Pin.Materials Letters. 2003, 58(3-4):493-497.PE Material Durable Floating Barrier Float for Wave Breaker[Portable Camping Hiking Multi Tool Pliers with Carabiner]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Hot Electronic Dry Herb Vaporizer Pen Device Vax Mini Vape Kit-composite.Polymer. 2005; 46(6):1949-1955.Antenna GPS with SMA Connector[New Type C25 220V 415V 6ka Breaking Capacity 2pole Dz47-63 MCCB MCB Miniature Circuit Breaker]

Received: September 7, 2011
Revised: January 3, 2013

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