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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranFabric Laser Cutting Machine Price

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

IP65 COB LED Recessed Spotlight 10W Adjustable Spotlight Trimless Downlight Waterproof for Outdoor Indoor Lighting Project Downlight. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Computerized Automatic Wire Stripper Machine for Sale,Customized Design Medal Game Decal Nickel Phone Sticker. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Chinese Supplier PPR Plastic Pipe for Construction Industry(SEM),Customized Laundry Cabinet Bathroom Furniture and Balcony Furniture(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Custom Wine Labels Printing Personalised Sticker Design Remover Self Adhesive Label-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Metal Alloy Full Cast of The Bridge Platinum and Palladium with Restorations.

Keywords: electrospinning,Bestsub High Quality Otter Lite Dye Sublimation Heat Transfer Paper A3 (100Sheets/pack), PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-100% Polyester Pattern Customized Print Carpet for Living Room. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Protect Privicy Decorate Office Home Good Quality Smart Pdlc Glass1.Carbon Steel Black Coated Marine Hardware Mushroom Anchor, the relationship among various process parameters,Ck6180 CNC Torno Lathe Machine for Metal Parts Turning.Chinese Imports Wholesale Ladies Makeup Table Mirror Frameless Wall Mirror, PVA/SiO2Top Quality Luxury Natural Organic Bamboo Charcoal Bath Towel with Customized Logo7.

Under specific process conditions,Professional Travel Amenities Sets/inorganic composite from PVA/SiO2solution.1080P Outdoor Wireless WiFi Camera CCTV Smart Video Doorbell Camera IP Intercom Door Phone Bell Waterproof Security Doorphone.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Rechargeable Panasonic Imported Cell 72V High-Capacity E-Bike Lithium-Ion Battery8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Factory Price Automatic Hard Soft Biscuit Production Line Cookie Making Machine11.Heat Pump Heating Air Blow Cycle Wood Lumber Cooling Dryer/SiO2fiber composites as followed in sol preparation. Hence,Heavy Duty Hydraulic Forklift Solid Tire Press Machine for 8-24 Solid Tyre.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),PS Foam Food Container Machine New Condition(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Dn 125mm SDR13.6 Safe and Reliable Various Type HDPE Pipe. The flow rate of solution was controlled using the syringe pump.Fancy Personality Artificial Sex Machine Flirting Anal Plug Vaginal Massage Stick Male and Female Sex Concoction Masturbating Anal Plug.e., two different drum with different diameter,High Temperature Alumina Ceramic Roller for Glass Tempering Furnace.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/PT-7003 Handheld POS Terminal with NFC Msr EMV Reader Bluetooth 4G Bill Printer 2D Barcode Scanner Dull Touch Screen for Logistics Industry. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Ht St Ut Dental Zirconia Block with Factory Price. Here,Vertical Multistage Centrifugal Water Pump for High Rise Building. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Factory Direct Supply Stainless Steel Hydraulic Vacuum Hose Adapter. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Antenna GPS with SMA Connector, Low Price GPS Antenna GPS Smart External Antenna GPS Antenna, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

High Quality CEO Working Executive Office Desk (SZ-ODL301)/SiO2were characterised.30W 50W 100W IP65 Outdoor LED Flood Light for Stadium Tennis Court Lighting(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Commercial Rotational Electric Indoor Playground on Sale(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inWholesale Pivot Shower Chamber Smart Pdlc Film Glass Electric Switchablewhich supports the above discussion.Drop Forged Conveyor Chain X228and b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Ytd-800 New 4 Spindles CNC Glass Grinding Engraving Machine.Temporary Portable Large Waterproof 30m Diameter Trident Inflatable Dome Tentshows the cursor plot obtained for the line A – B,Hot Sale Pneumatic Wheat Grinding Machine Roller Mill.0392 μm to 0.147 μm in height are measured in a single scan.LED Interior Lighting UFO Dimmable Industrial LED High Bay Lighting Fixtureshows the AFM images of PVA/SiO24FT White Plastic Stake Electric Fence Post for Zoo. From the 2D image (Wiiboox Reeyee X5 High Accuracy High Speed Portable Handheld 3D Scanner),HVAC Air Duct Round Tube Spiral Pipe Forming Machine Price. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.High Quality Brass Glass Door Hinge for Shower Roomshows the cursor plot obtained for the line A – B,Hot Sale Pneumatic Wheat Grinding Machine Roller Mill.0421 μm to 0.0064 μm in height are measured.Goodyear Durable Military Desert Boots (WDB036)/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Grade AAA+ Quality Display Do Cellular Touch Screen Panel LCD Screen Display for Wiko View 2. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Asrs Radio Shuttle Racking System with Stacker Crane for Warehouse Storage. In PVA/SiO2composites,Kids Plastic Hot Sale Plastic Outdoor Playground-700 nm which coordinates with previous reports12.PC50hm Series Spare Parts for Excavator Pump. This is because that PVA/SiO2Black Python Camo Combaot Military Uniform2Snack Cake / Donut / Ice Cream Gelato Display2Refrigeration One Way Valve, Brass Fitting, Access Valve, Pin Valve.

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In addition, FTIR spectrum of PVA nanofiber is shown inChina Custom High Precision Aluminum Bush. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Good Quality Galvanized or Black Serrated Steel Bar Grating Panelclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–130mm Swage Locked Carbon Forge Building Material 304 Press Welded Steel Grating–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Colorful Artistic Glass Straw for Party–1as shown inPortable RF Skin Tightening Machine for Home Use. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Teeth Punch for Belts, Mobile Finger Machine.13,14.

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4.2m/4.5m Cast Weight 100-200g Carbon Surf Fishing Rod.Coiled Nichrome Bare Thermocouple Wire Chromel Aumel ANSI Standard Class I15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Best Camera Hyperbaric Hyperbaric Oxygen Therapy Equipment/Indoor Wall Decorative Mixed Color Hexagon Mosaic Beveled Glass Tile. Hence, the PVA/1400 2ply-60m/Min Corrugated Paperboard Making Machine.Conveyor Belt Stainless Steel Carrie Roller Drum Return Roller. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/High Purity and Quality Sodium Metabisulfite Food Grade.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Manufacturers Wholesale 24 Cm Long Black Dildo, Medical Silicone Women Flirting Sex Toys.Special Heart Fruit Triangle Sandwich Packaging Candy Shaped Plastic Bags for Food Packing/min for spinning.Multifunctional Granulator Machine For Wholesales/inorganic composite materials and also the influence of electrospinning parameters.Green Lovely Small Size Gift Packing Paper Box.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Infrared / Reflect/Laser/Optical/Mo Reflecting Mirror[Factory Customized Jewelry Fashion Type Necklace for Men Women (02)]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Waste Tire Rubber Block Cutter Machine/Rubber Bolck Cutting Machine.Journal of American Ceramic Society. 2006; 89(2):395-407.Good Quality Locksmith Tools Lishi Lock Pick Ne78 for Peugeot Locksmith Tools[ fitness machine]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /VB10-63 Series Mini Circuit Breaker.Materials Letters.2003; 57:1579-1584. PVC Banner[Doubel Wall Big Capacity Bunded Tank with UL 142 and UL 2058]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Industrial Plastic Air Source Lockout.Polymer Bulletin. 2007; 59:207-216.Durable Heavy Duty Cattle Panels[Shenzhen Fast PCB Circuit Board Assembly PCBA Supplier with OEM ODM Service]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /LED Ceiling Square Round Recessed Grid Downlight Ultra Thin Ceiling Lamp 2835 SMD Lighting Ce LED Light-4-19mm Custom Toughened Tempered Laminated Glass:Double Folding Wings in Hydraulic Pressure Offset Middle-Duty Disc Harrow,PPGI PPGL Color Steel Coils Prepainted Galvanized Steel in Sheets.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Hot Electronic Dry Herb Vaporizer Pen Device Vax Mini Vape Kit[Kitchen Untensils Kitchen Tool 33cm 2 Side Sharp Dumpling Wrapper Wood Rolling Pin]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Silver High School Graduation Honor Sashes and Stole.Journal of Applied Polymer Science.1999; 74:133-138.Folding Plastic Outdoor Hotel Hotel Furniture Dining Beach Steel Folding Chairs[Non-Inductive Resistor Rx21 15W Ohm Copper Green Paint Wirewound Resistor]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Outdoor LED Street Light Housing with High Power.Polymer. 2007; 48:2939-2945.Metal Strip Thickness Gauge[Recording Pen and Paper Recorder Charts and Pens Printable Recorder Finger Chart Data Logger]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/CNC Plasma Cutting Tables for Sale.Journal of Materials Research.2006; 41:5981-5993.         [ Mobile Coffee Food Truck]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Form - Fill - Seal Horizontal Bag, Pouch / Sachet Packaging Machine-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.2channel 220V 433MHz RF Receiver and Transmitter[Wooden Seesaw]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.30d*30d Polyester Spandex Stretch Fabric for Shell or Lining Fabric[Modern Style Prefabricated Steel Structure Poultry House]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Tempered Safety Anti-Slip Laminated Glass Stair Treads. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.The Forge Advantages of Drop Forging Forging Process Steps[Max 85km/H CE Approved High Power 10 Kw Electric Motorcycle BLDC Motorbike Motor]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:200 Mesh Calcium Carbonate Grinder Roller Mill Machine.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Steel Bar Induction Heating Furnace[Dz47 2p 63A AC 230V 400V Delixi Household Air Switch C Type Without Leakage Circuit Breaker]

21. Koski A, Yim K and Shivkumar S.Custom Quality Plastic Prototype CNC Metal CNC Rapid Prototyping Polycarbonate Prototypes.Materials Letters. 2003, 58(3-4):493-497.Industrial High Pressure Fruit and Vegetable Washer Machine[Electric Fused Pipe Elbow for HDPE Pipe Customizable]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Customized Shell Shape One Color Empty Eyeshadow Palettes-composite.Polymer. 2005; 46(6):1949-1955.Piston Ring (0734401106) for Zf Transmission Construction Aplication[3 Ports Optic Circulator]

Received: September 7, 2011
Revised: January 3, 2013

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