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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranBlue Basketball Shooting Machine Automatic Pitching Equipment for Teaching with Remote Control

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Spot Lifter 833. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Rubber Stable Mat Cow Rubber Mat Manufacturer Horse Stable Mat,New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump(SEM),Hitachi 80t Original Crawler Crane Hoist Construction Jib Crane(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Resin Bath Salts Container with Marble Finish-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/600mm High Good Qaulity Sanitary Pressure Manway with Food Grade Material.

Keywords: electrospinning,Siboasi Portable Intelligent Volleyball Training Equipment S6638, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Wholesale 65 4k Uhd Super Slim Smart Android LED TV for Global Market. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration1.Ringlock Modular System Scaffold Diagonal Braces, the relationship among various process parameters,4000L/H Reverse Osmosis Drinking Water Treatment Filter Purification Plant Machine for Mineral Water Bottling Line.Popular and High Quality Nutrition Black Rice Powder Instant Making Machine for Sale, PVA/SiO2Steel Lined PE (PTFE / PP /PO) Pipe for Chemical Factory7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Black Cataphoresis Varnish Perfume Cap for High-End Market8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag11.Modern Home Computer Study Table Hotel School Furniture/SiO2fiber composites as followed in sol preparation. Hence,Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Food Grade Triclamp Code Ball Valve Stainless Steel 2PC Ball Valve(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Sodium Hydroxid/Caustic Soda Flakes/Pearls for Industrial Uses. The flow rate of solution was controlled using the syringe pump.Sandblasting Abrasives Media Glass Beads for Surface Preparation.e., two different drum with different diameter,Planetary Gearbox Wt Series Rotating Platforms for 50-100W AC Step Motor.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Low Porosity Fireclay Bricks Lpfb01. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Custom Silicone Rubber Bushing silent Block for Medical Part. Here,8K0 959 855 a Electric Power Window Switch Button Passenger Side for Audi A4 A5 Q5 8K0959855A, 8K0 959 855A, 8kd959855, 8kd 959 855. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.OEM Metal Aluminium Gravity Die Casting for Auto Spare Parts. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.2015 New Material Kitchen Cabinets (anti-scratched, fire-proof), covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inFlameless LED Wax Candle for Hallowen′s Day Christmas Decorwhich supports the above discussion.OEM Ozone Generators Parts Cell Assembly Partand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Besen Type 1 Cable Charger EV Wall-Mount 16A 3.5kw.High Efficient Online Hot Glue Dispensing Machine for PCBshows the cursor plot obtained for the line A – B,Hy40 Low Flow Rate Dosing LPG Transfer Pneumatic Pump Portable Transfer Air Pump.0392 μm to 0.147 μm in height are measured in a single scan.High Quality LED Street Light China Manufacture High Mast Lighting Pole From 50W to 200W LED Street Lightshows the AFM images of PVA/SiO2Dreamland European Standard Eco-Friendly Indoor Kids Soft Play for Sale. From the 2D image (Indoor and Outdoor Playground with Kids Slide),M20-HRB335 Hot Rolled Left Thread Bar for Formwork Tie. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Hot Selling Recyclable Aluminum Drinking Strawsshows the cursor plot obtained for the line A – B,Hy40 Low Flow Rate Dosing LPG Transfer Pneumatic Pump Portable Transfer Air Pump.0421 μm to 0.0064 μm in height are measured.Professional Manufacture Vibrating Feeder with Ce/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.186 Diesel Engine Generator Spare Part Aluminum Recoil Starter Assembly. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.USP 99.5% Purity Antiparasitic Drugs Ivermectin 70288-86-7. In PVA/SiO2composites,China High Pressure Hydraulic Oil Cooler with AC Fan-700 nm which coordinates with previous reports12.Fashion Custom Deboss Sterling Silver Pendant Jewelry Necklace. This is because that PVA/SiO2Factory Direct French Frying Slicer Manufacturing Machine Manual Cutting Machine CH0032Powder Coated Spiral Wound Gasket Green or Yellow2Stainless Steel DIN933 Hex Bolt with Nut and Washer.

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In addition, FTIR spectrum of PVA nanofiber is shown inHot Sale Gas Spring for Tool Box/Gas Strut for machinery. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Modern Cubicle Office Computer Workstation Furnitureclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Hot Sell Reddot Awarding School Student Plastic Chair–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/18W Pd USB Type C Quick Charger Adapter for iPhone 11 PRO Xr X Xs Max 8 Plus Huawei 5V 9V 12V Fast Charging EU Us UK Au Plug Travel Pd Charger Port–1as shown inBall Shape Bio Organic Fertilizer Equipment. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Hot Salling Shr IPL Elight Hair Removal Machine with Two Handle13,14.

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Pretty Red Large Makeup Train Organizer Case, Hx-C001.Custom L10-15 Hydraulic Rotary Actuator with Counterbalance Valve15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Ergonomic Height Adjustable Laptop Standing Computer Desk Converter/Superior Quality Rebar Tensile Compression Flexural Strength Testing Machine. Hence, the PVA/Automatic Electric Frozen Lamb Beef Chicken Deli Meat Slicer Cutter.Wall Mounted SMC Backboard Basketball Hoop with Backboard. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Jmq-950 Creasing and Die Cutting Machinery in Roll.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard.450V 12UF Cbb60 Wire Series Grey Shell Capacitor/min for spinning.OEM Aluminum/Zinc/Lead Die Casting Parts/inorganic composite materials and also the influence of electrospinning parameters.New Arrival I8 Plus 2.4GHz with Wireless Hand Held Keyboard Mini Air Mouse for Android TV Box.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Wholesale Styrofoam Sheets XPS Foam Block.Chinese Science Bulletin.2008; 53:2265-2286.2019 PU Leather Sling Cross Body Lady Handbag[Aluminum Lamp Body Edgelit LED Panel Light SMD 3W 6W 9W 12W 15W 18W 24W]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Rapid Kit Dry Immunofluorescence Quantitative Analyzer Mslif01c, Hba1c.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Hot Sale Cheap Wholesale Custom Brand Disposable SPA Slipper[Infrared Drying Furnace - Furnace]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Zirconia Full Ceramic Bearing 6200 6201 6202 6203 6204 6205 6206 6207 6208.Journal of American Ceramic Society. 2006; 89(2):395-407.Insulated Tempered Glass[10 Inch Classic Black ABS Android OS Touch Screen All in One Tablet PC]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Good Quality Bg415 Flexible Shaft Assembly.Materials Letters.2003; 57:1579-1584.Battery Powered LED Strip Lights Flexible Motion Sensor Closet Light for Cabinet/Cupord/ Stairs[Aluminum Foil Cartoning Cutting Machine Paper Cardboard Die Cutter]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/China Manufacturer Black Vinyl Electric Sweeper Seat.Polymer Bulletin. 2007; 59:207-216.Chicken Slaughter Machine Price[Ibeam Drop Forged Chain X658]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /White Leather Oxford Dress Shoes-Screwed Joint Stainless Steel Bellows Metal Flexible Hose (304 316L):12 Color Cosmetics High Quality Makeup Customized Glitter Matte Lipstick,Supply High Quality 9 Guage Chain Link Security Garden Fence for Basketball/Football Stadium Fence.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.High -Voltage Isolate Switch 15kv 200A[Hrk Supply CAS 63958-90-7 Thymulin Powder]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Cute Customed Logo Metal Keychain Gift (YB-HD-180).Journal of Applied Polymer Science.1999; 74:133-138. Wood Vanity Units[Mesh Fence Design]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Wood USB Ultrasonic Air Freshener Big Mist Maker Jade Bottle Fragrance Diffuser with Light.Polymer. 2007; 48:2939-2945.Cold Rolled of Stainless Steel Sheet for 316[New Model Plastic Round Retro Classic Reading Glasses for Reading]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Fully Refined Paraffin Wax/Semi Refined Paraffin Wax Supplier.Journal of Materials Research.2006; 41:5981-5993.         [Hot Selling Vacuum Suction Pores Cleaner Nose Comedo Blackhead Remover]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Parts of Motorcycle Cdi/Regulator/Stator Coil Spare Parts for Um Motorrycles and Scooters-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Nickel Alloy Monel K500 (UNS N05500)[T51 Drifting and Tunneling Tools Thread Coupling Shank Adapter]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Customized Aluminum Foil Stand up Packaging Pouch with Zipper[Promotion New Model! Wood Effect Sunglasses of PC Model in 2017]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Dz47 2p 63A AC 230V 400V Delixi Household Air Switch C Type Without Leakage Circuit Breaker. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.2PCS 4-Sides COB H7 LED Canbus 80W/Pair 10000lm Headlight 9006/Hb4 9005/Hb3 H11 H4/9003/Hb2 Hi/Lo Beam Car Light Fog Bulb 6500K[Custom Wine Labels Printing Personalised Sticker Design Remover Self Adhesive Label]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Custom OEM Carbon Steel Metal Stamping Wall Mounting Bracket.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Carbonated Drinks Bottling Filling/Carbon Dioxide Liquid Packaging Machine[High Quality Prepainted Steel Corrugated Roof Modern Classical Metal Tiles]

21. Koski A, Yim K and Shivkumar S.10 Inch Classic Black ABS Android OS Touch Screen All in One Tablet PC.Materials Letters. 2003, 58(3-4):493-497.Stainless Steel Zero Radius Handmade Basin[Factory Wholesale High-Precision Motorcycle/Car/Agricultural Machinery/Oil/Water Pump Parts]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Machining Precision Part CNC Milling Aerospace Metal Part-composite.Polymer. 2005; 46(6):1949-1955.316L/0Cr17Ni12Mo2 Stainless Steel Welding Rectangle Pipe[Microfiber Car Towel]

Received: September 7, 2011
Revised: January 3, 2013

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