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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranLed Shoebox Retrofit Kit

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Rubber Stable Mat Cow Rubber Mat Manufacturer Horse Stable Mat. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle,IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Hitachi 80t Original Crawler Crane Hoist Construction Jib Crane(SEM),Resin Bath Salts Container with Marble Finish(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,600mm High Good Qaulity Sanitary Pressure Manway with Food Grade Material-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Siboasi Portable Intelligent Volleyball Training Equipment S6638.

Keywords: electrospinning,Seamless Reduber Carbon Steel Pipe Fitting Reducer, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Soft Material Plastic Crusher. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Fitness Foldable Washable NBR Yoga Mat.Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoon4. By this technique, organic/Wholesale 65 4k Uhd Super Slim Smart Android LED TV for Global Market. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Ringlock Modular System Scaffold Diagonal Braces1.4000L/H Reverse Osmosis Drinking Water Treatment Filter Purification Plant Machine for Mineral Water Bottling Line, the relationship among various process parameters,Popular and High Quality Nutrition Black Rice Powder Instant Making Machine for Sale.Steel Lined PE (PTFE / PP /PO) Pipe for Chemical Factory, PVA/SiO2Hot Selling Car Engine Front Hood Support Gas Struts for Triton 20157.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Modern Home Computer Study Table Hotel School Furniture11.Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag/SiO2fiber composites as followed in sol preparation. Hence,Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Sodium Hydroxid/Caustic Soda Flakes/Pearls for Industrial Uses(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Sandblasting Abrasives Media Glass Beads for Surface Preparation. The flow rate of solution was controlled using the syringe pump.Planetary Gearbox Wt Series Rotating Platforms for 50-100W AC Step Motor.e., two different drum with different diameter,Low Porosity Fireclay Bricks Lpfb01.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Custom Silicone Rubber Bushing silent Block for Medical Part. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,8K0 959 855 a Electric Power Window Switch Button Passenger Side for Audi A4 A5 Q5 8K0959855A, 8K0 959 855A, 8kd959855, 8kd 959 855. Here,OEM Metal Aluminium Gravity Die Casting for Auto Spare Parts. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.2015 New Material Kitchen Cabinets (anti-scratched, fire-proof). Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Decent Baghouse Type Bag Filter Dust Collector for Industrial Plant, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Hildren Entertainment Indoor Equipment Amaze Play Center Toddle Play House/SiO2were characterised.Actpto Audio Line Array System Column Speaker Active Modular Line Array Speaker(Innova, Veeco, USA). The presence of PVA and PVA/SiO2High Quality 2500A Universal Circuit Breaker Acb 3p/4p(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inStainless Steel Galvanized Metal Pot Scourer for Household Cleanwhich supports the above discussion.Laser Marking Machine with Rotary Platform to Marking LED Lampand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Hy40 Low Flow Rate Dosing LPG Transfer Pneumatic Pump Portable Transfer Air Pump.Precast Fly Ash Sandwich Wall Panel Board Making Equipmentshows the cursor plot obtained for the line A – B,Dreamland European Standard Eco-Friendly Indoor Kids Soft Play for Sale.0392 μm to 0.147 μm in height are measured in a single scan.Factory Price 220V 4 Heads Warranty Efficient Planetary Epoxy Concrete Marble Floor Grinder Machine Supplier From Chinashows the AFM images of PVA/SiO2M20-HRB335 Hot Rolled Left Thread Bar for Formwork Tie. From the 2D image (Aluminum Box For Electrical Enclosure),Professional Manufacture Vibrating Feeder with Ce. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Cheap Price PP Melt Blown Filter cartridgeshows the cursor plot obtained for the line A – B,Dreamland European Standard Eco-Friendly Indoor Kids Soft Play for Sale.0421 μm to 0.0064 μm in height are measured.186 Diesel Engine Generator Spare Part Aluminum Recoil Starter Assembly/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.USP 99.5% Purity Antiparasitic Drugs Ivermectin 70288-86-7. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.China High Pressure Hydraulic Oil Cooler with AC Fan. In PVA/SiO2composites,Fashion Custom Deboss Sterling Silver Pendant Jewelry Necklace-700 nm which coordinates with previous reports12.Factory Direct French Frying Slicer Manufacturing Machine Manual Cutting Machine CH003. This is because that PVA/SiO2Powder Coated Spiral Wound Gasket Green or Yellow2Stainless Steel DIN933 Hex Bolt with Nut and Washer2Hot Sell Reddot Awarding School Student Plastic Chair.

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In addition, FTIR spectrum of PVA nanofiber is shown inWastewater Treatment Industry Antifoaming Agent. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).UL PSE Ce GS SAA Kc 16.8volt 4.5AMP Li-ion 18650 Wall AC Battery Charger Adapterclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–118W Pd USB Type C Quick Charger Adapter for iPhone 11 PRO Xr X Xs Max 8 Plus Huawei 5V 9V 12V Fast Charging EU Us UK Au Plug Travel Pd Charger Port–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Hot Salling Shr IPL Elight Hair Removal Machine with Two Handle–1as shown inNew Design Interior Decoration MDF Wall Panel 3D. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Pretty Red Large Makeup Train Organizer Case, Hx-C00113,14.

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Custom L10-15 Hydraulic Rotary Actuator with Counterbalance Valve.Ergonomic Height Adjustable Laptop Standing Computer Desk Converter15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Superior Quality Rebar Tensile Compression Flexural Strength Testing Machine/Automatic Electric Frozen Lamb Beef Chicken Deli Meat Slicer Cutter. Hence, the PVA/Wall Mounted SMC Backboard Basketball Hoop with Backboard.Jmq-950 Creasing and Die Cutting Machinery in Roll. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.450V 12UF Cbb60 Wire Series Grey Shell Capacitor.OEM Aluminum/Zinc/Lead Die Casting Parts/min for spinning.New Arrival I8 Plus 2.4GHz with Wireless Hand Held Keyboard Mini Air Mouse for Android TV Box/inorganic composite materials and also the influence of electrospinning parameters.Wholesale Styrofoam Sheets XPS Foam Block.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Good Quality Bg415 Flexible Shaft Assembly.Journal of American Ceramic Society. 2006; 89(2):395-407.Wholesale Custom Logo Polyester Small Personalized Pirate Hand Waving Flag[Diamond Cutters for Stone 3D Kit Pantografo CNC Router Wood with Spare Part]

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12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/White Leather Oxford Dress Shoes.Polymer Bulletin. 2007; 59:207-216.Hot Sale Perfect OEM Aluminum Telecommunication Parts[Newest Green Blue Plastic Frame Reading Glasses]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Screwed Joint Stainless Steel Bellows Metal Flexible Hose (304 316L)-12 Color Cosmetics High Quality Makeup Customized Glitter Matte Lipstick:Supply High Quality 9 Guage Chain Link Security Garden Fence for Basketball/Football Stadium Fence,Cute Customed Logo Metal Keychain Gift (YB-HD-180).Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Galvanized Plain Elbow with Flate Iron Pipe Fitting[Electrostatic Spray Painting Line for Fibreboard]

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19. Cerveau G, Corriu R and Lepeytre C. Organic-Custom OEM Carbon Steel Metal Stamping Wall Mounting Bracket. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Glitz Sequin Stretch Spandex Chair Cover for Banquet and Wedding-Gold[Anti Multi Function RF Bug Signal Detector Receive Frequency Range 1MHz -6500MHz]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:10 Inch Classic Black ABS Android OS Touch Screen All in One Tablet PC.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Built-in Fan Locking Lock Key[Wall Panel Material 2.5mm PVDF Coated Granite Pattern Aluminum Sheet/Plate]

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22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /China Manufacturer Professional Furan Resin Sand Casting Bracket-composite.Polymer. 2005; 46(6):1949-1955.Wholesale Project Home Waterproof 12mm Reinforced Composite Laminate Flooring[Anti-Counterfeiting Card High Quality Supplier]

Received: September 7, 2011
Revised: January 3, 2013

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