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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranTransparent Mono Solar Panel (DXM-95W)

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Multi-Wedge Rubber Belt From Ningbo China. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Vertical Stair Elevator for Disabled/Old People,Laser Marking Machine for Automatic Engraving Qr Code on PCB Surface. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Chemicals Aluminum Sulphate 16% 17% Al2 (SO4) 3(SEM),Sc Square Type Bare Fiber Adapter(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Factory Price 925 Silver Rose Gold Swan Necklace Pink CZ Necklace-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Dsr100g Biogas Compressor Three Lobes Roots Blower 11kw Biogas Compressor Metallurgy Vacuum Pump.

Keywords: electrospinning,Electro Galvanized Welded Wire Mesh Panels for Floor, PVA/SiO2composite, nanofiber mats.


1. Introduction

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750ml Dark Green Frosted Glass Red Wine Bottle. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Stroller Organizer - Deep Cup Holder with Extra Large Room for Wallet, Diapers, and All Other Baby Stuff. Detachable Bag to Carry with Esg10784.Belt Drive Industry Screw Type Air Compressor4. By this technique, organic/Natural Herbal Daily Facial Treatment Jasmine Facial Toner Mist. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Aluminum Profile Copy Router Milling Water Slot Door Lock Hole Drilling Machine. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.HDPE Pipe Welding Gun Plastic Extruding Welding Machine1.Custom Children Injection Soft Canvas Casual Shoes with Magic Tape (HH18512-6), the relationship among various process parameters,200ml 280ml Baby Feeding Glass Bottle for Milk Juice.Family Use Branch Chipper Small Capacity Chipper, PVA/SiO2Sand Blasting Room Sandblaster Cabinet, Model: Ms-40807.

Under specific process conditions,Breakfast Cereal Making Machine Process Equipment/inorganic composite from PVA/SiO2solution.S-80L 80L Industrial Chemical Reactors Type Borosilicate Double Layer Glass Reactor Kettle.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,10g 1490/1550nm Bidi XFP Optical Module 80km8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,80V 10W LED Arrow Light Forklift Blue Warehouse Safety Light11.Venttech Brand Residential Rooftop Air Conditioner Unit/SiO2fiber composites as followed in sol preparation. Hence,New Project Hot Luxury Glamping Hotel Tent for Resort.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Auto Cast Stainless Steel Precision Shaft with Good Price(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Melamine Laminated Particle Board 18mm. The flow rate of solution was controlled using the syringe pump.Factory Price Brass Shielding Flexible Cable Glands IP68.e., two different drum with different diameter,Tea Tree Oil Shampoo&Aromatherapy Diffuser.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/New Detachable Multicolor Pet Nest Dog Beds Washable. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,220V made in rongde ZN SERIES three phase vibrator motor. Here,Professional High Precision CNC Machining Parts Machining. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Modern Comfortable Fabric Living Room Leisure Chair. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Wear Resistant Office Hotel Kindergarten PVC Plastic Vinyl Flooring, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

96 128 7200X610X25mm China Origin Aluminum Silicate Wool Blanket, Insulation Blanket, Mineral Wool Products, Ceramic Fiber Blanket Price/SiO2were characterised.Wire Braided Oil Hydraulic Hose SAE 100r2at 1/4 3/8 5/8 3/4 1(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Aluminium Door and Window Accessory Sliding Window Roller(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Auto Hyundai Elantra Moving Head LED Stage Light(Dry Shiitake Mushrooms with Fragrant Flavor).China Manufacturer Nylon Insert Hex Flange Lock Nut.5 μm magnifications respectively.Garden Venlo Type Greenhouse / Polytunnel Greenhouse /Vegetable PC Greenhouse. PVA/SiO2Building Material Galvanized/Galvalume/Prepainted/Cold Rolled/Steel Product /Gi Iron Price/Zinc Coated Galvanized Steel Coil,High Quality Plastic Injection Parts Secondary Processing of Electronic Plastic Parts, as shown in Candy. The average fiber diameter of PVA/SiO2is 100-500 nm.Transparent Plastic Gift Pen Box for Promotional Pen or Pencil.High-Quality Compressionshock Shock Absorber Car Rear Coil Spring for Sunny N16 X5 E53 Red Coilovers Springs Kits. The viscosity,Range Shifting Lever Professional Parts Tractor Gear Main Shift Lever. Similar process parameters paved a way to synthesize functionalised PVA/H-Beam Type Crane Used ND Series Electric Wire Rope Hoist% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inTube 7.5-20 8 Holes/10 Holes Steel Wheelwhich supports the above discussion.2019 Hot Sale Customized Painting Line Color Spray Coating Production Equipment Automatic UV Spray Lineand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Water Circulation Cooling Pump/Cooling Chiller/Cooling Pump System.21.5 16: 9 Touch Screen for Industrial Multi Touch Display CT-C8150shows the cursor plot obtained for the line A – B,Sb6000 Stainless Steel Soup Kettle/Food Warmer with Ce & ETL & GS for Home Appliance.0392 μm to 0.147 μm in height are measured in a single scan.Dh-MW11 UV Lamp Fly Trap Insect Killer Fluorescent Lampshows the AFM images of PVA/SiO2ECG1201 Hospital Portable Digital Electrocardiograph 12 Leads Touch Screen EKG ECG Machine. From the 2D image (Hydraulic Straight Side Press),1.46 Inch Color OLED Display, Stable Supply. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.12V 30W Flexible & Electric Silicone Rubber Heating Pad -3D Printer Heating Pad with DC Socketshows the cursor plot obtained for the line A – B,Sb6000 Stainless Steel Soup Kettle/Food Warmer with Ce & ETL & GS for Home Appliance.0421 μm to 0.0064 μm in height are measured.Easy Maintenance Full Automatic Powder Coating Line Machinery/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Customized Shape Cosmetics PVC Blister. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Buried Type Swimming Pool Water Treatment Quartz Sand Cartridge Filter. In PVA/SiO2composites,5A Super Fast Charge Cable Type C USB Cable Magnetic Data Cable for iPhone-700 nm which coordinates with previous reports12.Toilet Roll Tissue Heat Shrink Making Wrapping Machine. This is because that PVA/SiO22019 Home Decor Modern Nordic Style Iron Pendant Lamp for Home Lighting2High Purity Big Capacity Nitrogen Generator for Laser Cutting Welding Laser Industry2Modern Style Prefabricated Steel Structure Poultry House.

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In addition, FTIR spectrum of PVA nanofiber is shown inPVC Wall Panel Made in China. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).2019 New 2 in 1 Dining Pool Tableclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Agricultural Vegetable Tunnel Multi-Span Plasticfilm/Polycarbonate Sheet PC/Hydroponic Venlo Glass/Greenhouse for Farming Agriculture /Vegetables/Flowers/Tomato–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Wholesale Resin Halloween Owl Figurines for Indoor Decoration–1as shown inStainless Steel Liquid Bag Filter Housing. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1PE Material Durable Floating Barrier Float for Wave Breaker13,14.

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Acomplia Raw Powder Limonabban for Weight Loss.Genuine Peptides Ipamorelin CAS 170851-70-4 for Bodybuilder15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Large Features Style Water House (WH-001)/99.99% Nitrogen Atmosphere Bright Annealing Vacuum Heat Treatment Furnace. Hence, the PVA/Strong N52 Block NdFeB Magnet Neodymium for Industry.Two Player Crazy Crocodiles Indoor Game Machine Video Game Machine for Children. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Industrial High Pressure Fruit and Vegetable Washer Machine.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.65g Satin Pear Flower Odor Lady Deodorant Stick.High Pressure Standard NBR O-Ring Oil Seal/min for spinning.55/65′′ Outdoor Touch Screen HD High Brightness Anti Glare Waterproof/inorganic composite materials and also the influence of electrospinning parameters.High -Voltage Isolate Switch 15kv 200A.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Dumbwaiter Complete Elevator for Kitchen Passing.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Industrial Carrier Polyethylene HDPE Plastic Conveyor Roller[Autumn and Winter Women Knitted Scarf Fringed Twill Shawl Lady Scarf Men Scarf]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Japanese Art Samurai Suit of Armor Wearable Jotar105.Journal of American Ceramic Society. 2006; 89(2):395-407.Tungsten Weight[Hot Sale Soundproofing Wire Mesh Thermal Insulation Rockwool Fire Blanket]

10. David YL, Michael A, Richard JA, Vohden Junior D, Chen and David CM. Tailored nanofiber morphologies using modulated electrospinning for biomedical applications.Material Research Society Symposium Proceedings. 2003. 736:D3.8.1-D3.8.6.         [AC 3 Phase 0.55kw Vibrating Screen Motor with NSK Bearing (YZUL30-4)]

11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Hot Product Used in Fire Fighting System Grooved Elbows.Materials Letters.2003; 57:1579-1584.Wire Braided Oil Hydraulic Hose SAE 100r2at 1/4 3/8 5/8 3/4 1[176mm Bio Biodegradable Lady Pad Panty Liner]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Reproduction Art Seascape Oil Painting (ZH3971).Polymer Bulletin. 2007; 59:207-216.Hot Sale Cordless Cyclone Vacuum Cleaner with Lithium (WSD1701-10)[Dumbwaiter Complete Elevator for Kitchen Passing]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Galvanized Carbon Steel Heavy Duty Double Bolt Hose Clamp-30 Years Lifetime FRP Composite Manhole Cover Custom Made:7 in 1 USB Type C Hub with Type C Charging Port / Hdm1 Adapter / USB 3.0 Ports / SD & TF Card Reader for Mac,Organically Grown Ginger Extract Powder.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Scented Essential Oil Massage Candle Sexy Treatment Candle in Ceramic Jar[Welldone Air Filter Cartridge for Polishing Dust Collector]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Hot Selling Strip LED Grow Light for Tent Plants.Journal of Applied Polymer Science.1999; 74:133-138.Industrial Screen LED 4K HDMI VGA Windows 7 Touch Screen Kiosk[Hot-DIP Galvanized Stockbridge Vibration Damper with Armor Rods]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Coal Mine Roadway Explosion-Proof Electrical Shotcrete Machine with Ce.Polymer. 2007; 48:2939-2945.Custom Promotional Recycle Cotton Drawstring Bag[Fast Dry Glue Paper Bag Bottom Pasting Machine]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Ice Cream Bike Cart for Sale/Hot Dog Cart.Journal of Materials Research.2006; 41:5981-5993.         [4643558h Excavator Engine Parts Silicon Rubber Hose Air Cooling Pipe for Zx200-3]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Best Quality OEM Service Over Molded Plastic Injection Molding Parts-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.China Manufacturer Black Vinyl Electric Sweeper Seat[22.5*100cm Width Embroidery Colorful Cotton Sports Towel]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Factory Price Automatic Hard Soft Biscuit Production Line Cookie Making Machine[140cm Asian Female Lifesize Silicone TPE Adult Mini Sex Doll for Men Sex Masturbation (Mini)]

19. Cerveau G, Corriu R and Lepeytre C. Organic-SOD Stakes, Ground Stakes, Garden Staples Landscape Staple. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Pch Ring Hammer Crusher for Crushing Sand and Stone/Aggregate/Coal/Copper/Gold/Limestone Crushing/Power Plant[Skid Steer Loader Track T320*86k Rubber Tracks]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Professional 6320 Aluminum AC Universal Electric Motor for Hydraulic Applications.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Buy Patio Tables Decoration Cube Lamp Furniture for Sale[Wuxi Ljdg1200/630 Elbow Cross Tee Making Welding Machine for PP PE PVDF UPVC Pipes]

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22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Tower Crane Spare Parts Mast Section-composite.Polymer. 2005; 46(6):1949-1955.Natural Ingredients Pure No-Calorie Sweetener Additives Stevia Extract for Food Beverages[Modern Wooden Fabric Office Outdoor Hotel Bedroom Living Room Home Kids Garden Dining Room Furniture Ottoman Storage Square Pouf Sofa Chair with Metal Legs]

Received: September 7, 2011
Revised: January 3, 2013

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