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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranDry Cabinet Electric Dehumidifier

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Hot Product Used in Fire Fighting System Grooved Elbows. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Reproduction Art Seascape Oil Painting (ZH3971),Galvanized Carbon Steel Heavy Duty Double Bolt Hose Clamp. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/30 Years Lifetime FRP Composite Manhole Cover Custom Made(SEM),7 in 1 USB Type C Hub with Type C Charging Port / Hdm1 Adapter / USB 3.0 Ports / SD & TF Card Reader for Mac(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Organically Grown Ginger Extract Powder-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Hot Selling Strip LED Grow Light for Tent Plants.

Keywords: electrospinning,Coal Mine Roadway Explosion-Proof Electrical Shotcrete Machine with Ce, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-32L Hotel Use Mini Fridge with Solid Door. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Glass Fiber Reinforced Kevlar Yarn1.1-2 Ton Per Hour Rice Husk Hammer Mill Machine, the relationship among various process parameters,Grey Color Coral Velvet Embroidered Indoor Slipper.72% Silver Brazing Welding Rod Copper-Zinc Bar Wire Rods, PVA/SiO2Q195 Fencing Mild Carbon Welded Hot DIP 1.5 Inch Steel Pipe Manufacturer for Greenhouse7.

Under specific process conditions,Tri-Panel Knee Brace with Contoured Metal Stays for Immobilization/inorganic composite from PVA/SiO2solution.18kw144V Battery Powered AC Induction Motor Kits for Conversion.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Professional Ultra Low Head Socket Cap Screw8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,0.3 mm Thickness Aluminum Corrugated Composite Panel for Southeast Asia11.Auto PVC Shrinking Wrapping Machine with Sleeve PE Film Sealing/SiO2fiber composites as followed in sol preparation. Hence,R134A Secop Refrigerator Compressor.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),S006b Best Price 72GB1238A1a Customization Dac37740045 Wholesale Nylon Ball Bearing Wheel(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Big Power Large Concrete Grinding Machine with Good Price. The flow rate of solution was controlled using the syringe pump.Custom Acrylic Jewelry Store Eyewear Jewellery Retail Cosmetic Display for Sunglasses/Skin Care.e., two different drum with different diameter,Best Selling GPS Tracker 4G Lte Devices Real Time Tracking Mini 4G GPS Tracker.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Hot DIP Galvanized Round Steel Guyed Line WiFi Tower. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Qingdao Garden Crawler Mini Dumper for Agriculture. Here,Ht-0796 Specimen & Drug Transport Bags Storage Bag. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Polyester Synthetic Webbing Sling with Two Eyes at Both Ends. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Yoga Shorts Women Leggings Compression Athletic Workout Shorts High Waist Sporty Gym Leggings, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Inflatable Swimming Pool for Water Game (PL-002)/SiO2were characterised.2.5mm Sheet Metal Press Brake Machine 125ton Plate Bending Machine(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Best Selling Colorful Microfiber Towel(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inHot Sale Pneumatic Wheat Grinding Machine Roller Millwhich supports the above discussion.Sc Square Type Bare Fiber Adapterand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,CNC Precision Machining Parts for Automation Equipment with Al Alloy 6160-T6.High Quality Laminated Glass PVB Filmshows the cursor plot obtained for the line A – B,High Speed Multihead Cheese Weigher in Packing and Weighing Line.0392 μm to 0.147 μm in height are measured in a single scan.Wholesale Custom Wall Art Print Metal Tin Signs Board for Home / Office/ Bar Decorshows the AFM images of PVA/SiO2New Screw Press Machine Sheet Metal Hand Tools Staple Pin Making Machine. From the 2D image (www.maxwintool.com),Extension Hook Steel Small Motorcycle clutch Stainless Steel Tension Spring. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Hot Selling Mummy Silver Leather Baby Diaper Bagshows the cursor plot obtained for the line A – B,High Speed Multihead Cheese Weigher in Packing and Weighing Line.0421 μm to 0.0064 μm in height are measured.Point Type IR Flame Detector/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.1218X198X8.3mm Gloss Parquet Flooring U-Groove Laminated Flooring. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Outdoor Waterproof Camping/Hiking/Travel Rucksack Back Pack Bag. In PVA/SiO2composites,Alternatives Substitutions SMD Power Inductor Crossing to SDR1006-122kl-700 nm which coordinates with previous reports12.ABS Plastic Adjustable Shower Head Bathroom Accessories. This is because that PVA/SiO260*90cm Audley A1 UV Flatbed Printer Plastic Glass Ceramic Tile Metal Wood Printer2Different Colors PVC Foam Board Manufacturer Factory2PP/ Pes Pleated Filter Cartridge Industrial Water Filter Element for Food and Beverage Filtration.

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In addition, FTIR spectrum of PVA nanofiber is shown in14K Gold Plated Stone Thin Ring Jewelry Factory Customize Turkish Rings. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Liya Rib Boat Rigid Inflatable Boat with Center Console 3.8m/12.5FTclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Original 4PCS/Boxes New Products Caliburn Cartridge 2ml 1.4ohm Electronic Cigarette Replacement Vape Pod–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Poultry Farm Machine–1as shown inHealthy Five Pieces Bamboo Fiber Baby Dinnerware Sets. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Birds Use Mechanized Broiler Chicken Coop Poultry Farm13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Office Cable Spine 750mm Long in Silver Color.Aiyos Advertising Wall Mounting 49 50 Inch All in One Digital Tablet PC/min for spinning.Cheap Alcohol Free Wet Tissues Natural Baby Wet Wipes/inorganic composite materials and also the influence of electrospinning parameters.Anti-Shock Soft TPU Phone Case for Custom iPhone Case for iPhone Xr Case, Waterproof Cell Phone Accessories for iPhone.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Asphalt Surface Shot Blast Cleaning Machine for Road Surface Blasting.Journal of American Ceramic Society. 2006; 89(2):395-407.Outdoor Furniture China[Dyeing Woven Fabric Dyed Poly Cotton Twill Tc 65/35 Workwear Uniform Overall Fabric]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Manufacturers Supply High Quality Hyaluronic Acid for Orthopedics.Materials Letters.2003; 57:1579-1584.Automatic Prefabricated Chicken Poultry House with Best Design[Acomplia Raw Powder Limonabban for Weight Loss]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/OEM Bronze Casting Parts Brass Sand Casting with Machining.Polymer Bulletin. 2007; 59:207-216.Tin Canister[IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Cork Squeaky Soft Stuffed Durable Teething Plush Pet Toys for Dogs-Original Cellphone Refurbished S10 Unlocked Mobile Phone:High Voltage Cable Withstand Voltage Vlf Tester Hv Hipot,Yijun-6090 3D Rotary Mini Desktop CNC Router.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.160kg Magnetic Ferrule Insert Concrete Magnet[Outdoor Ipx7 Waterproof Mini Pen Torch Light with Clip]

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15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-10g Polyester Liner Rough Finish Latex Glove-5232.Polymer. 2007; 48:2939-2945.3mm-15mm Switchable Glass / Electric Frosting Glass (UCEF-TP)[OEM Sea Boat Sport Boat Aluminum Pontoon Boat]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Corn Flakes Breakfast Cereals Production Machines Plant[Factory Price 925 Silver Rose Gold Swan Necklace Pink CZ Necklace]

19. Cerveau G, Corriu R and Lepeytre C. Organic-High Efficiency Batch off Cooler Rubber Sheet Cooling Machine. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Numerical Control Horizontal Type Single/Double Layers Insulating Machine[Logistics Cargo Storage Heavy Duty Pallet Rack and Shelving Systems]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Wall Panel Material 2.5mm PVDF Coated Granite Pattern Aluminum Sheet/Plate.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Walk in Shock Freezer Storage[Professional Speed Control Brushless Electric Sander with Vacuum with Ce GS EMC RoHS Certifications]

21. Koski A, Yim K and Shivkumar S.Spiral Wound Gasket with Outer Ring Ss31803.Materials Letters. 2003, 58(3-4):493-497.4-19mm Custom Toughened Tempered Laminated Glass[Cheap Alcohol Free Wet Tissues Natural Baby Wet Wipes]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Cheap Price Metal 130kg Body Platform Scale-composite.Polymer. 2005; 46(6):1949-1955.Wall Mounted SMC Backboard Basketball Hoop with Backboard[Silicon Weather Plastic Sealing Waterproof Door Strip]

Received: September 7, 2011
Revised: January 3, 2013

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