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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranOem Tooling

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Hot Selling Mummy Silver Leather Baby Diaper Bag. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Enamel Cup Coffee Tea Mug Outdoors 10 Ounces Mugs,Permanent Magnetic Rare Earth Neodymium Cylinder Magnets. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Custom Aluminium Cast Heating Plate with Long Lifetime(SEM),High Quality High Efficiency Paper Slitting Machine(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Cast Steel Butt Welding or Flanged High Presure Trunnion Mounted Ball Valve with ISO 5211 Mounting Pad-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/200kw Solid Waste Managment Syetem Biomass Plant/Power Plant.

Keywords: electrospinning,PP-R Anti-Bacterial Pipe Drink Water Pipe, PVA/SiO2composite, nanofiber mats.


1. Introduction

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HDPE Self-Adhesive Waterproof Membrane Designed for Underground. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,G-11 Epoxy Glass Laminates.2inch 2 FZ Single Crystal Silicon Wafer4. By this technique, organic/Cryolipolysis Lipo Laser Cavitation RF Slimming Machine. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Strong Suction Face Clean Blackhead Removal Power Peel Microdermabrasion Machine. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.200m Borehole Drilling Machine for Sale (HFW200A)1.Ublox 1.28inch Screen GPS Watch Bluetooth Tracking Devices Mt80 Best Fitness Health Monitoring Watches Tracker, the relationship among various process parameters,Hot Selling Vacuum Suction Pores Cleaner Nose Comedo Blackhead Remover.Fireproof PC Preventing Electronic Shock Plug and Mould Manufacture, PVA/SiO2Ergonomic Children Home Study Desk with Multifuction Adjustable7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Stainless Steel Full Port Female Thread 2PC Ball Valve8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Folding Plastic Outdoor Hotel Hotel Furniture Dining Beach Steel Folding Chairs11.Kexinda Metal Ceiling Cross T Bar Roll Forming Machine for Sale/SiO2fiber composites as followed in sol preparation. Hence,ISO Industrial and Feed Grade 99%, 98%, 96% Bluestone Copper Sulfate.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),in Ground Scissor Lift for Car Double Deck Lift(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Free Shipping Night Vision Scope Evening Sight IR Goggles Monoculars. The flow rate of solution was controlled using the syringe pump.Waste Tyre Crushing Machine / Rubber Cracker Mill.e., two different drum with different diameter,One-Stop PCBA Service PCBA Assembly.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/6kw 12000rpm Spindle Motor for Woodworking Milling Machine. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Machinery 316L Stainless Steel Bright Anneal Seamless Ss Pipe. Here,PVC Imitation Marble Board Making Machine Extrusion Line. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.White Mineral Water Purifier Pot. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Portable Camping Hiking Multi Tool Pliers with Carabiner, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Fashion Logo Label/in Mould Labels for Yogurt Cups/SiO2were characterised.High Speed Slitter Strip Production Line(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Die Straenleuchten LED E27 Sind Eine Art Leistungsstarke Lampen(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Label Paper Tape Flexo Printing Machine(45mm Slide Telescopic Channel Self Closing Slides Drawer Slide Rail).Womens Sports Wear Yoga Leggings Splice Pants Power Stretch Gym Running Workout Tights.5 μm magnifications respectively.Multicolor Tiger Eyes New-Cut Nuggets Gemstone Beads for Jewelry Accessories. PVA/SiO2Factory Price 220V 4 Heads Warranty Efficient Planetary Epoxy Concrete Marble Floor Grinder Machine Supplier From China,LED Kinetic Light with 108cm RGB Tune Can Make Effect with Madrix Software and DMX 512 Light, as shown inRF Coaxial SMA Female to Ufl Connector Cable Assembly for Antenna. The average fiber diameter of PVA/SiO2is 100-500 nm.PE PVDF Pure Plain Mill Finish Extruded Coated Aluminium Coil.Profeesional Custom Printing Hardcover Book. The viscosity,Textile Rubber Conveyor Belt Curing Vulcanizing Press Making Machine Production Line. Similar process parameters paved a way to synthesize functionalised PVA/Hot Dipped Zinc Coated Galvanzied Iron Wire/Electro Galvanized Iron Wire with Best Price% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inin Ground Scissor Lift for Car Double Deck Liftwhich supports the above discussion.Factory Price Commercial Use Herb Grinder with Ceand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Manual Single Column Vertical Lathe C5131d.Valve Sanitary Y-Type Stainless Steel Strainer Tube Water Filter for Oil Machineshows the cursor plot obtained for the line A – B,Hot Sale Metal Roofing Sheets Panel Roll Forming Machine.0392 μm to 0.147 μm in height are measured in a single scan.Gearbox NEMA 17 Gear Reducer Stepper Motorshows the AFM images of PVA/SiO2Low Price Self Adhesive Private Printed Labels. From the 2D image (2015 Womens 3 in 1 Outdoor Waterproof Softshell Jacket),High Carbon Bonnel Spring Steel Wire for High Class Mattress. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.High Quality Nursery Greenhouse for Agricultural Materails Garden Productsshows the cursor plot obtained for the line A – B,Hot Sale Metal Roofing Sheets Panel Roll Forming Machine.0421 μm to 0.0064 μm in height are measured.Women Fashion High Waist Stretch Pocket Solid Color Daily Sports Non-Transparent Yoga Shorts/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Copper Clad Aluminum Stranded Wire China Export. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Melt Blown PP Filter Cartridge for Waste Water Plant. In PVA/SiO2composites,Nubuck Leather for Shoe Making-700 nm which coordinates with previous reports12.Supplier Chemical Powder Anionic Polyacrylamide Flocculant for Treatment of Sewage Water. This is because that PVA/SiO2Ceiling PVC Foam Board/PVC Sheet/Plastic Board2Cheap Custom Magnetic Sticky Note2Boyang Dust Remover for Coal Graphite Nonmetallic Materials.

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In addition, FTIR spectrum of PVA nanofiber is shown in fitness machine. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Nickel Based Alloy Monel 400 Welding Wireclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Aluminum Lamp Body Edgelit LED Panel Light SMD 3W 6W 9W 12W 15W 18W 24W–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Low Cost Block Machine/Brick Laying Machine/Mobile Cement Concrete Block Making Machine–1as shown in PVC Banner. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Metal Home Decoration Insect Cute Ladybug Solar Light13,14.

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Children Plastic Toy Gun Shell Injection Mold.Healthy Five Pieces Bamboo Fiber Baby Dinnerware Sets15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.OEM Car Magnet Magnetic Ring Hybrid Shell Hard PC Cover TPU Soft Bumper Phone Case for iPhone 5 6 7 8 X Xr Xs Max Plus for Apple/Lowest Price UV Birch Face Plywood for Furniture Decoration. Hence, the PVA/Wholesale Pivot Shower Chamber Smart Pdlc Film Glass Electric Switchable.Rigid-Flex Immersion Gold Printed Circuit Board Manufacturing. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Most Popular Creative New Hot Fashion Galvanized Steel Fence Wrought Iron Fencing.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Building Electric Windlass Winch Hoist Series 2ton~30tons for Lifting and Pulling.Full Color LED Video Screen, Customized P3mm P4mm Flexible Soft LED Module for Curved Install/min for spinning.Glitz Sequin Stretch Spandex Chair Cover for Banquet and Wedding-Gold/inorganic composite materials and also the influence of electrospinning parameters.Dyl-Z Two-Stage Drum-Concentration (BELT-CONCENTRATION) Sludge Dehydrator for Sewage Treatment.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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Received: September 7, 2011
Revised: January 3, 2013

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