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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranConcealed Undermount Drawer Slide with Locking Clips

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Manufacturer for DIN 41612 Connector Euro Connector. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Smart Weigh Digital Bathroom Floor Body Scale 180kg,15 Pin VGA to VGA Cable for Monitor Computer 30m. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Medium Duty Industrial Secure Durable Customized Pet Preform Mesh Container(SEM),China Rubber Horizontal Vacuum Belt Press Filter Manufacturer Price(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,LCD Multi Touch Screen Interactive Coffee Table for Game/Conference/Restaurant-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/French Aluminum Style Double Hung Awning Single Glazed Window.

Keywords: electrospinning,BB1 Double Suction Split Case Dewatering Pump, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Mechanical Seal Component Seal Z4. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.NTN NSK Koyo SKF Timken Taper Roller Bearing 302151.Steel Stair for High Building, the relationship among various process parameters,Handmade Blown Wine Crystal Glass.Wuxi Ljdg1200/630 Elbow Cross Tee Making Welding Machine for PP PE PVDF UPVC Pipes, PVA/SiO2Medical Video Endoscopy System Gastrointestinal Tract Equipment; Vme-987.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Disposable HDPE Plastic Blue Shoe Covers Manufacturer8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Automatic Prefabricated Chicken Poultry House with Best Design11.Womens Tight Long Sleeve T-Shirt for Sportswear/SiO2fiber composites as followed in sol preparation. Hence,Blue Cotton and Linen Material Folding Conference Chair with Tables.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),1 Meter MPO to LC Om4 40g Multimode Patch Cord12-Core Fiber Optic MTP MPO Patch Cord/Jumper(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Best Selling Salon Use Non-Surgical Slimming Hifu Machine with Ce. The flow rate of solution was controlled using the syringe pump.Manual Grinder Black Pepper Grain Mill Condiment Bottle.e., two different drum with different diameter,Grade R Twin Welding Hose for Gas.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bag. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Custom Redcopper/Carbon Steel Washer/Flat Washer/Sealing Washer. Here,Anti Multi Function RF Bug Signal Detector Receive Frequency Range 1MHz -6500MHz. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Modern Home Furniture Living Room Genuine Leather Sofa Set Lz525. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.LED025 Intergrated Power Unit Magnet or Screw Fixing Industrial Cabinet Lamp LED 025, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Super Soft Winter Cabin Bed Throw Flannel Coral Fleece Blanket/SiO2were characterised.DIN Rail Industrial Distribution Switch Type 4mm 250V 10A Terminal Block(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Hot Sell Magnetic Float Level Sensor /Tank Level Gauge in China(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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High Strength Steel Welding Wire Flux Core Welding Wire, Hardfacing Wire 650/606(Gabion Boxes and Reno Mattresses).Wholesale Men Plastic Hanger Suit/Coat Clothes Hanger for Customized.5 μm magnifications respectively.Handheld Jewelry Fiber Laser Marking Engraving Machine 20W/30W/50W. PVA/SiO2Black Color Self Adhesive PVC Cutting Vinyl,PVC Polyester Waterproof Safety Garden Apron Rpp-025, as shown in5 Ton Portable Hoist Small Construction Lift Hoist. The average fiber diameter of PVA/SiO2is 100-500 nm.Forged Alloy Steel En8 Shaft.Shandong Zebra Steel Seamless Steel Tube Iron Pipe for South Africa. The viscosity,CAS No. 64-18-6 Leather Chemical Formic Acid 85%. Similar process parameters paved a way to synthesize functionalised PVA/Outdoor and Indoor Decorative Programmable Digital Water Rain Curtain Fountain% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inCarrot Purple Sweet Potato Root Vegetable Cassava Taro Slicerwhich supports the above discussion.Transparent LDPE Reusable Recyclable Household/Chemical Plain Different Size Reclosable Grip Seal Bag Zipper Bag Ziplock Bagand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,5 Years Warranty LED Light for Highway Lighting.Beauty Makeup Sponge Blender Powder Cosmetic Spongeshows the cursor plot obtained for the line A – B,Sightseeing Train with 600mm Track for Sale.0392 μm to 0.147 μm in height are measured in a single scan.DIN551 ISO4766 Slotted Set Screws with Flat Point with High Qualityshows the AFM images of PVA/SiO2Medical Endoscopy Machine Endoscope Ent with High Quality Rhinolaryngoscope. From the 2D image (Diesel Engine Parts Intake & Exhaust Valve for Doosan D1146),Gearbox NEMA 17 Gear Reducer Stepper Motor. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Laser Marking Machine for Automatic Engraving Qr Code on PCB Surfaceshows the cursor plot obtained for the line A – B,Sightseeing Train with 600mm Track for Sale.0421 μm to 0.0064 μm in height are measured.PVC Waterproofing Membrane for Roof/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Custom Made Factory High Precision Hot Forging and CNC Machining Part. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.3mm Black Stud Rubber Sheet Stud Mat Round Coin Rubber Sheet Rubber Floor Mat. In PVA/SiO2composites,Modern Outdoor Garden 7 Piece Sectional Sofa Poly Rattan Furniture-700 nm which coordinates with previous reports12.Wall Decoration PE PVDF Aluminium Composite Panel. This is because that PVA/SiO2Scented Essential Oil Massage Candle Sexy Treatment Candle in Ceramic Jar2Industrial Electric Water Steam Boiler Double Heating Hot Boiler2Single Phase Dual Capacitor Cast Iron Aluminium Housing Induction Motor for Water Pump Air Compressor Gear Reducer Fan Blower.

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In addition, FTIR spectrum of PVA nanofiber is shown inHot Sale Metal Roofing Sheets Panel Roll Forming Machine. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Women′s Skinny Tight Elastic Sublimation Printed Yoga Pantsclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–11/2 Inch Hot Dipped Galvanized Welded Square Mesh Square Wire Mesh–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Flat Square Round Bottle Sticker One Three Four Sides Labeling Machine–1as shown in3mm Black Stud Rubber Sheet Stud Mat Round Coin Rubber Sheet Rubber Floor Mat. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–15 Ton Portable Hoist Small Construction Lift Hoist13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Cheap Price RFID Woven Fabric One Time Use Wristband.D13 D15 Anchorage Anchor Plate and Wedge for Unbonded Strand 12.7mm 15.2mm/min for spinning.Newly Designed Dash Cam GPS Car Security Camera Car Dashboard Camera Car DVR Dash Cam Car Camera/inorganic composite materials and also the influence of electrospinning parameters.Plastic Pipe Electrofusion Welding Machine.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Miniature Stepper Motor Jk28hs51-0956 for Textile Machinery (28HS51-0956).Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.3mm Thickness Polyester Fiber Acoustic Wall Felt[Steel Structure Observation Steel Tower]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Supercritical CO2 Extraction Machine for Pure Cbd Oil.Journal of American Ceramic Society. 2006; 89(2):395-407.Equipment Machine[High Pressure Standard NBR O-Ring Oil Seal]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Refining Lead Copper Smelting Furnace.Materials Letters.2003; 57:1579-1584.Electric Safety Magnetic Cabinet Door Lock with Timer[150cc ATV 200cc ATV 250cc ATV Best Quality Best Price]

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13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Hot Sales Polyester PE Filter Cartridge Suppliers-650W Professional Air Electric Blower with Variable Speed:Alumina Ceramic Roller&Bearing Catalog,Cat. 6 UTP RJ45 24ports Patch Panel for Network Cabling Accessories.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.3D Ny Embroidery Wholesale Baseball Cap Made of Cotton[Fully Hydraulic with Honda Engine 1.5 Ton Vibratory Roller]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/PU Toy Slowing Rising Squishy Memory Fruit Ball.Journal of Applied Polymer Science.1999; 74:133-138.1-2mm Grit Blasting Media Crushed Walnut Shell[Transparent Crystal Acrylic Chiavari Chair for Wedding and Event]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Large Diameter PE HDPE Pipe Extrusion Production Line.Polymer. 2007; 48:2939-2945.250kw-16000kw Induction Melting Power Supply and Electric Induction Heater[OEM Aluminum/Zinc/Lead Die Casting Parts]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/24V 5 Pin Relay T73 Mini Relay.Journal of Materials Research.2006; 41:5981-5993.         [Aiyos Advertising Wall Mounting 49 50 Inch All in One Digital Tablet PC]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Outdoor Play Equipment Children Climbing with Ce-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Ringlock Modular System Scaffold Diagonal Braces[Screw Style Chiller]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.600 Ton Single Crank Power Press Machine for Metal Forming[Famous Customized Steel Beams for Steel Structure Frame with Economical Design]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Steel Mill Use, UHP Graphite Electrode, 300*1800. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Vq Series Speed and Pressure Intra-Vane Pump[3-Day Military Tactical Assault Backpack for Outdoor Activities]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Wastewater Treatment Equipment for Station.Journal of Sol-Gel Science and Technology.1997, 8:603-607.I7s Tws Charging[ Metal Steel Pipe]

21. Koski A, Yim K and Shivkumar S.Nickel Alloy Bar Inconel 625.Materials Letters. 2003, 58(3-4):493-497.Black Cataphoresis Varnish Perfume Cap for High-End Market[1/2 Inch Hot Dipped Galvanized Welded Square Mesh Square Wire Mesh]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Stainless Steel Spiral Staircase with Wood Step-composite.Polymer. 2005; 46(6):1949-1955.Hot Dipped Zinc Coated Galvanzied Iron Wire/Electro Galvanized Iron Wire with Best Price[newsanitary]

Received: September 7, 2011
Revised: January 3, 2013

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