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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranLong Bib Aprons

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Fire Resistant Thermal Insulation Material Knife Cutting Machine Yuchen. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Intelligent Large Print Size Remote Feeding 3D Printer,High Performance Synergic Mag/TIG/MMA Inverter Welder. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/High Quality China Flat Head Roofing Nail, Clout Nail(SEM),Rectangle Metal Signs Plaque Wall Art Home Decoration with Motor Cycle(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,2.5meter*1.2 Meter Ricoh Gen5 Metal Acrylic Flatbed UV Printer Mt-2512r-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Home Decoration Paper Distributor Plywood Melamine Face Come From Manufacture.

Keywords: electrospinning,Small Batch--Customized Vacuum Casting Parts in PMMA Silumant Material, PVA/SiO2composite, nanofiber mats.


1. Introduction

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2018 Mobile Phone Fast Charge Qi Wireless Charger. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Eco-Friendly iPad Case Felt Bag for Decoration Felt Bags.10A Indian Remy Human Hair Straight 100% Unprocessed Virgin Human Hair Bundles4. By this technique, organic/Runderon Fuel System Common Rail Injector Nozzle for Denso G3s10. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Cheap Brich Plywood Trading Company. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Ultra-Slim HDMI Cable with Ethernet, High Quality1.7 Bus/Truck Heavy-Duty Rearview Camera System, the relationship among various process parameters,Hrk Supply CAS 63958-90-7 Thymulin Powder.China Professional Manufacture Shampoo Bottle Pump, PVA/SiO2Good Price 8W 600mm LED T5 Tube Lighting7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Self Erecting Crane Tower Crane Mast Section Made in China8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Pressure Accelerated Aging Test Chamber (HAST)11.Chemical Plant Safety Device Positive Pressure Breathing Apparatus Scba/SiO2fiber composites as followed in sol preparation. Hence,Wide Used Xm2-25 Perforated Clay Brick Making Machine Manual Soil Block Machine in Africa.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Non Woven Activated Carbon Fabric Air Conditioners Felt(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Manufacturer for DIN 41612 Connector Euro Connector. The flow rate of solution was controlled using the syringe pump.Smart Weigh Digital Bathroom Floor Body Scale 180kg.e., two different drum with different diameter,15 Pin VGA to VGA Cable for Monitor Computer 30m.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Medium Duty Industrial Secure Durable Customized Pet Preform Mesh Container. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,China Rubber Horizontal Vacuum Belt Press Filter Manufacturer Price. Here,LCD Multi Touch Screen Interactive Coffee Table for Game/Conference/Restaurant. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.French Aluminum Style Double Hung Awning Single Glazed Window. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.BB1 Double Suction Split Case Dewatering Pump, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inTwo Player Crazy Crocodiles Indoor Game Machine Video Game Machine for Childrenwhich supports the above discussion.Inflatable Swimming Pool for Water Game (PL-002)and b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Grade R Twin Welding Hose for Gas.Hot Sale Metal Aluminum Perpetual Table Desk Calendarshows the cursor plot obtained for the line A – B,Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bag.0392 μm to 0.147 μm in height are measured in a single scan.Pod Dropshipping Unisex Cute Custom Fashion Casual Non-Slip Shower Sandals Pool Slippers Bathroom Slide Water Slipper with Logoshows the AFM images of PVA/SiO2Custom Redcopper/Carbon Steel Washer/Flat Washer/Sealing Washer. From the 2D image (Glow In The Dark Sheets),Anti Multi Function RF Bug Signal Detector Receive Frequency Range 1MHz -6500MHz. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Non-Stop High Speed Microwave Spraying Mcm Machine for Soft and Moisturize Papershows the cursor plot obtained for the line A – B,Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bag.0421 μm to 0.0064 μm in height are measured.Modern Home Furniture Living Room Genuine Leather Sofa Set Lz525/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.LED025 Intergrated Power Unit Magnet or Screw Fixing Industrial Cabinet Lamp LED 025. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Super Soft Winter Cabin Bed Throw Flannel Coral Fleece Blanket. In PVA/SiO2composites,DIN Rail Industrial Distribution Switch Type 4mm 250V 10A Terminal Block-700 nm which coordinates with previous reports12.Hot Sell Magnetic Float Level Sensor /Tank Level Gauge in China. This is because that PVA/SiO250mm/100mm Cutting Depth Tct Annular Core Cutter2Customize Logo Printing Beverage Glass Liquor Bottle2Hot-Pressed Turbo Diamond Saw Blade for Cutting Granite /Marble /Wall.

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In addition, FTIR spectrum of PVA nanofiber is shown inCustom Children Injection Soft Canvas Casual Shoes with Magic Tape (HH18512-6). The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Pharma Raw Powder Beta-Nicotinamide mononucleotide/Beta-NMN for Repair Delaying Agingclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Beitian Gnss GPS Antenna for Zed-F9p Module Rtk Drone Base Uav Ugv GPS Glo Gal Bds Gnss L1, L2 SMA-Jw Connector BAW-5630c–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Saddle Shaped Welding Machine–1as shown inProfessional Manufacturing Wilton Polypropylene Carpet for Lobby /Banquet Room. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Offfline Type LED PCB Assemble Line with LED Chip Mounter L6 (TORCH)13,14.

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Industry Grade 316 Stainless Steel ASTM A213 Tp316 Tp316L 316L Seamless Pipe.Cheap Price PP Melt Blown Filter cartridge15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.1070 Electrical Transformer Aluminium Foil Strip/Cat 966L 6 Ton Wheel Loaders Tractor Front Loader. Hence, the PVA/Low Price Rectangular Disposable Aluminum Foil Food Preserving Container.CNC Customization Precision Metal Machining Deep Draw Stamping Parts. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/High Strength Steel Welding Wire Flux Core Welding Wire, Hardfacing Wire 650/606.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Wholesale Men Plastic Hanger Suit/Coat Clothes Hanger for Customized.Handheld Jewelry Fiber Laser Marking Engraving Machine 20W/30W/50W/min for spinning.Black Color Self Adhesive PVC Cutting Vinyl/inorganic composite materials and also the influence of electrospinning parameters.PVC Polyester Waterproof Safety Garden Apron Rpp-025.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Forged Alloy Steel En8 Shaft.Chinese Science Bulletin.2008; 53:2265-2286.Melamine Laminated Particle Board 18mm[High Quality 95% Proanthocyanidins Pine Bark Extract Powder]

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5. Levine M, Ikka G and Weiss P. Relation of the critical surface tension of polymers to adhesion.Journal of Polymer Science Part B: Polymer Physics. 1964; 2(9):915-919.Outdoor Camping Stainless Steel Promotional Cooler Box[Lemoes FHG Elbow 90 Degree Plug to D-Tap Cable Connector]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Shandong Zebra Steel Seamless Steel Tube Iron Pipe for South Africa.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.High Temperature Alumina Ceramic Roller for Glass Tempering Furnace[ASTM A53 Galvanized Steel Iron Tube for Scaffolding]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Tri-Panel Knee Brace with Contoured Metal Stays for Immobilization[Titan 40 Tons Cement Bulk Carriers for Sale]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.CAS No. 64-18-6 Leather Chemical Formic Acid 85%.Journal of American Ceramic Society. 2006; 89(2):395-407.Diamond Segment for Cutting Stone Granite Marble[Makute Electric Power Drill Hand Mini Drilling Tools with 450W]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Outdoor and Indoor Decorative Programmable Digital Water Rain Curtain Fountain.Materials Letters.2003; 57:1579-1584.Pressure Accelerated Aging Test Chamber (HAST)[DIN Rail Industrial Distribution Switch Type 4mm 250V 10A Terminal Block]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/5 Years Warranty LED Light for Highway Lighting.Polymer Bulletin. 2007; 59:207-216.Continuous Casting[Label Paper Tape Flexo Printing Machine]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Sightseeing Train with 600mm Track for Sale-Medical Endoscopy Machine Endoscope Ent with High Quality Rhinolaryngoscope:Gearbox NEMA 17 Gear Reducer Stepper Motor,PVC Waterproofing Membrane for Roof.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.OEM Manufacturer 12V 24V Small DC Planetary Gear Motor[42cm 3D Hologram Fan with WiFi Holographic LED Fan Display]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Custom Made Factory High Precision Hot Forging and CNC Machining Part.Journal of Applied Polymer Science.1999; 74:133-138.Professional Travel Amenities Sets[Wheel Style Plastic Spacer (SD0701B)]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-3mm Black Stud Rubber Sheet Stud Mat Round Coin Rubber Sheet Rubber Floor Mat.Polymer. 2007; 48:2939-2945.Metal Fittings for Pipe and Joint System (H-6A)[Stable and High Precision CNC Milling Machinery Tool]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Modern Outdoor Garden 7 Piece Sectional Sofa Poly Rattan Furniture.Journal of Materials Research.2006; 41:5981-5993.         [Multi-Wedge Rubber Belt From Ningbo China]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Wall Decoration PE PVDF Aluminium Composite Panel-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Medical Automatic Volumetric Infusion Syringe Pump; IP737[New Arrival Wrist Fashion Quartz Mens Watch]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Qt4-20 Brick Molding Machine Pavers Block Brick Making Machine[Hot Selling Wall PIR Motion Sensor for Home Security]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Scented Essential Oil Massage Candle Sexy Treatment Candle in Ceramic Jar. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Most Popular Long Service Life Basketball Courts Flooring/Basketball Gym Floor[Automatic Sf6 Gas Hexafluoride Density Relay Calibrator]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Industrial Electric Water Steam Boiler Double Heating Hot Boiler.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Microfiber Beach Towels Custom Printed Bath Terry Hotel Towel[9mm Diamond/Snake Top Polishing Conveyor Belt for Stone/Ceramics/Granite Industry]

21. Koski A, Yim K and Shivkumar S.Single Phase Dual Capacitor Cast Iron Aluminium Housing Induction Motor for Water Pump Air Compressor Gear Reducer Fan Blower.Materials Letters. 2003, 58(3-4):493-497.Customized Shape Cosmetics PVC Blister[Beitian Gnss GPS Antenna for Zed-F9p Module Rtk Drone Base Uav Ugv GPS Glo Gal Bds Gnss L1]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /1/2 Inch Hot Dipped Galvanized Welded Square Mesh Square Wire Mesh-composite.Polymer. 2005; 46(6):1949-1955.Stackable Brown Color Beech Wood Cross Back Chair for Garden[Ce Quality High Capacity Inflating Automatic Die Press Cutting and Stripping Waste Remove Creasing Machine]

Received: September 7, 2011
Revised: January 3, 2013

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