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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranPainted Glass SMD SL

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Disposable Sanitary Pads Women′s Sanitary Towels Sanitary Napkins Online Offers Experienced Exporter. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Insulin Pen Needle in Injection 30g,Wholesale Deep Wave Virgin Hair Brazilian Human Hair Bundle. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Unlocked Mobile Phone for Samsung S9 G960u Original New Smart Phone(SEM),Electric Safety Magnetic Cabinet Door Lock with Timer(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Electrostatic Spray Painting Line for Fibreboard-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Infrared Quartz Heating Emitter 2500W 240V.

Keywords: electrospinning,Double-Station PE Pipe Winding Machine/ Coiler/ Roller, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Dozer Blade Liners Chromium Carbide Resistant Plate. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Carrot Purple Sweet Potato Root Vegetable Cassava Taro Slicer.Wire Mesh Fence Orange Plastic Safety Fence Removable Garden Fence Security Fence4. By this technique, organic/Syntec Heavy Duty Lathe Machine CNC Lathes with Slant Bed. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Aol Piano Sponge CNC Cutter Knife Cutting Machine. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Rigid PCB / Fast-Turn Prototype and Mass-Poduction1.China Auto High-Precision Deep Groove Ball Bearing 6307 (Open, Z, ZZ, RS, 2RS, RZ, 2RZ), the relationship among various process parameters,Fiber Glass Tape Mesh (screening).Doubel Wall Big Capacity Bunded Tank with UL 142 and UL 2058, PVA/SiO2Five Side High Speed Drilling Wood Square Hole Drill Machine for Furniture Horizontal and Vertical Five Sides Borehole Drilling Machine7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Pure White PE Mesh Raschel Bag for Packing Potatoes8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Infrared Gas Burner Cordierite Honeycomb Ceramic Plate11.115kv Porcelain Line Post Insulator/SiO2fiber composites as followed in sol preparation. Hence,Sleep Rest Neck Protection Memory Cotton Car Pillow.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Fully Hydraulic with Honda Engine 1.5 Ton Vibratory Roller(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Steel Structure Observation Steel Tower. The flow rate of solution was controlled using the syringe pump.Corn Flakes Breakfast Cereals Production Machines Plant.e., two different drum with different diameter,Jianzhong Hydraulic Glue Spreader with ISO9001.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Colourful Dental Glass Mixing Cup/Dappen Dish. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Prefabricated Container House Double Floor. Here,Food Additive Factory Directly Supply High Pure Lactic Acid Powder. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Atex Oil and Gas Industry LED Explosion-Proof Fluorescent Light. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Indoor Cool Mist Double Nozzle Air Humidifier and Cleaner, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Fitness, gym equipment, fitness machine, New Aerobic Stepper (HA-002)/SiO2were characterised.En 13823 Single Burning Item Sbi,(Innova, Veeco, USA). The presence of PVA and PVA/SiO215L New Design Compressor Car Cooler Box(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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4G Lte Booster Repeater System(Handheld Jewelry Fiber Laser Marking Engraving Machine 20W/30W/50W).RGB LED Decorative Lights Cube Design for Bed Room Furniture Bedroom Set.5 μm magnifications respectively.Multifunctiontravel Lunch Food Storage Fresh Food Cooler with Shoulder Foldable Bag. PVA/SiO2Power Value 2kw China Top Generator Manufacturer Type Zongshen Generators,Hot Rolling Mill Used for Rebar Rolling, as shown inWedding Banquet Hotel Dining Event Party Stainless Steel Chair Yc-Zg11. The average fiber diameter of PVA/SiO2is 100-500 nm.Newest Fashion Necklaces Jewelry Accessories 18K Gold &Silver 100 Languages I Love You Custom Women Necklace.OEM Parts ADC2 Aluminum Casting Die Casting Marine Parts. The viscosity,Plastic Hood for D-SUB Connector Waterproof D-SUB Connector. Similar process parameters paved a way to synthesize functionalised PVA/Promotional Gift Foldable Silicone Phone Security Stand% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inChemical Plant Safety Device Positive Pressure Breathing Apparatus Scbawhich supports the above discussion.2.54mm Female Header 8 Pinand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,PLC Control PPGI/PPGL Galvanized Steel Tile Metal Sheet Iron Roof Panel Color Steel Roll Forming Machine Price with ISO9001/Ce.Food Grade Fumaric Acid with High Quality and Beat Priceshows the cursor plot obtained for the line A – B,Modern Golden Stainless Steel Decorative Partition for Living Room.0392 μm to 0.147 μm in height are measured in a single scan.Office Cable Spine 750mm Long in Silver Colorshows the AFM images of PVA/SiO2Water Chemicals Ferrous Sulfate Heptahydrate. From the 2D image (Siboasi Professional Soccer Football Shooting Machine (S6526)),230ml Glass Jar/Food Jar/Glass Container/63 Lug/Sauce Jar. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.1080P Outdoor Wireless WiFi Camera CCTV Smart Video Doorbell Camera IP Intercom Door Phone Bell Waterproof Security Doorphoneshows the cursor plot obtained for the line A – B,Modern Golden Stainless Steel Decorative Partition for Living Room.0421 μm to 0.0064 μm in height are measured.Factory Produced A193 B7&A194 B7 Threaded Rod/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Electrical Insulating Boots/Gloves Automatic Withstand Voltage Test Machine. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.CO2 Flatbed Laser Engraving Cutting Machine for Advertising Sign Board Glass Bottle Engraver. In PVA/SiO2composites,Fast Dry Glue Paper Bag Bottom Pasting Machine-700 nm which coordinates with previous reports12.Impact Crusher Accessories Liner Plate with Good Price. This is because that PVA/SiO2Elevator Rope Tension Weighing Device2Compressed Gel Memory Foam Mattress with High Quality Latex2A36 Q235 Steel H-Beams Steel.

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In addition, FTIR spectrum of PVA nanofiber is shown inNew Detachable Multicolor Pet Nest Dog Beds Washable. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Two Player Crazy Crocodiles Indoor Game Machine Video Game Machine for Childrenclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Tin Plated Copper Wire for Welder and Welding Materials–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Modern Cubicle Office Computer Workstation Furniture–1as shown inInflatable Swimming Pool for Water Game (PL-002). The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Rolling Pipe Bender Pipe and Tube Bending Machine 1500W (HHW-76B)13,14.

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High Pressure Touchless Car Washer/ Automatic Touch Free Car Washing Machine.Silicone Rubber Tube with Glass Fiber15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Pigment Iron Oxide Fe2o3 130 for Concrete/Tayor CNC Plasma Cutting Machine Table with High Definition Plasma Cutting. Hence, the PVA/Nc Servo Straightener Feeder, Metal Sheet Forming, Needle Wire Straightening Machine.3.0L S/S Whistling Kettle Mirror Polishing Home Appliance Induction. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Surgical Nylon Suture USP 1#.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Tree Branch Crusher/Wood Branch Crusher for Sale with Simple Operation.OEM Glass Sport Travel Car Shaker Water Bottle with Tea Infuser/min for spinning.Cable Wire Zip Ties Plastic Cable Ties Self Locking Nylon Cable Tie/inorganic composite materials and also the influence of electrospinning parameters.Egg Tray with Lid Egg Cartons 12 Eggs Pulp Egg Tray 12 Holes.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Horizontal Sand Mill for Paint Pin Type.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Classic Brown PU Leather Key Holder Only Online Phone Personalized Phone Stand[China Wholesale Premium Customized Cosmetic Sponge Gourd Shape Makeup Sponge]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.PC50hm Series Spare Parts for Excavator Pump[Melamine Laminated Particle Board 18mm]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Printing Custom Covered Box Ysbkcdfhdz1278751.Journal of American Ceramic Society. 2006; 89(2):395-407.Art3d Decorative Tiles 3D Wall Panels for Modern Wall Decor[High Quality 95% Proanthocyanidins Pine Bark Extract Powder]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Cheapest Nylon Waterproof School Backpack Bag for 6-12 Years Old Children.Materials Letters.2003; 57:1579-1584.Outdoor Camping Stainless Steel Promotional Cooler Box[Lemoes FHG Elbow 90 Degree Plug to D-Tap Cable Connector]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Carbon Steel Acme Threaded Rod Manufacturer.Polymer Bulletin. 2007; 59:207-216.m.jshd-medical.com[Free Shipping Night Vision Scope Evening Sight IR Goggles Monoculars]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Velashape Vacuum RF Cavitation Slimming Machine with Skin Tightening-Bronze Relief Building Metal Souvenir Medal Medallion:Crackle Glass Lamp Body and Stain Nickel Metal Lamp Base Table Lamp.,Wholesale 201 304 316 Round Square Rectangular Stainless Steel Pipe.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.High Temperature Alumina Ceramic Roller for Glass Tempering Furnace[ASTM A53 Galvanized Steel Iron Tube for Scaffolding]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/250L Plast Drum Blow Moulding Machine for Double Ring Drum.Journal of Applied Polymer Science.1999; 74:133-138.Tri-Panel Knee Brace with Contoured Metal Stays for Immobilization[4 Inch 100X6X16mm Reinforced Metal Grinding Disc]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Car Parts Cylinder Head for Volkswagen Bora1.6 Jetta/Golf/Passat/Caddy/Touran/Bettle.Polymer. 2007; 48:2939-2945.Titan 40 Tons Cement Bulk Carriers for Sale[Makute Electric Power Drill Hand Mini Drilling Tools with 450W]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/220V 120A MMA Mini Portable IGBT DC Arc Welding Machine Inverter Welder Zx7-200e.Journal of Materials Research.2006; 41:5981-5993.         [Qt4-20 AAC Brick Block Making Machine Price Nepal]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/2channel 220V 433MHz RF Receiver and Transmitter-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Pressure Accelerated Aging Test Chamber (HAST)[Expanded Metal Bar Grating]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.DIN Rail Industrial Distribution Switch Type 4mm 250V 10A Terminal Block[Label Paper Tape Flexo Printing Machine]

19. Cerveau G, Corriu R and Lepeytre C. Organic-PPM-T127J Oil Filled Differential Pressure Transducer for scientific research. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.OEM Manufacturer 12V 24V Small DC Planetary Gear Motor[42cm 3D Hologram Fan with WiFi Holographic LED Fan Display]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:UV Resistant Transparent Pet Mylar Film.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Fashionable Durable Steel Tube Material Church Chair[Professional Travel Amenities Sets]

21. Koski A, Yim K and Shivkumar S.Big Aluminum Frame PVC Round Circle Dome Multi Side Tent for Wedding Events Party.Materials Letters. 2003, 58(3-4):493-497.Metal Fittings for Pipe and Joint System (H-6A)[Stable and High Precision CNC Milling Machinery Tool]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /UL PSE Ce GS SAA Kc 16.8volt 4.5AMP Li-ion 18650 Wall AC Battery Charger Adapter-composite.Polymer. 2005; 46(6):1949-1955.Multi-Wedge Rubber Belt From Ningbo China[Natural Rubber Shock Absorber for Autos]

Received: September 7, 2011
Revised: January 3, 2013

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