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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranBathroom Hand Shower Mixer Set

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Investment Casting Stainless Steel Casting Valve Parts Valve Body. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/7years Warranty 110lm/W High Power LED Street Light,55311-1h200 349084 Auto Spare Parts Cheap Shock Absorbers for KIA. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Portable Standing Seam Roof Panel Roll Cold Forming Tile Machine(SEM),Vintage Shape Titanium Mirror Aluminum Sport UV400 Metal Sunglasses with Your Logo(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Factory 316L 304 Seamless/Welded Stainless Steel Pipe Price for Industry-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Hydrogen Oxygen Generator Car Engine Decarboniser Machine.

Keywords: electrospinning,Steel Metal Leg Gaming Play Executive Table Office Wooden Furniture, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Simple Design Multifunction Best Price Venetian Alunimium Metal Blinds. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Metal/Wood/Stone Engraving CNC Router Dw1325.Mobile Food Cart /Taco Cart for Sale4. By this technique, organic/Factory Price Commercial Use Herb Grinder with Ce. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Glass Ampoule Sealing School Laboratory Equipment. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.WPC Decking Fence Floor Profile Extrusion Line / Production Line1.Lady Alloy Watch Colorful Dials Waterproof Women Wristwatch Quartz Wholesales (JY-AL073), the relationship among various process parameters,Stainless Steel Galvanized Metal Pot Scourer for Household Clean.30ml Empty Cosmetic Jar Pot Makeup Face Lotion Atomizer Sample Bottles Clear Essential Oil Perfume Cosmetic Sprayer, PVA/SiO2P5 960*960mm Panel Stage LED Screen for Concert Advertising Board Display7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Classic-Type Apollo Series LED Grow Light for Green House Plants8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Comfortable Silver Frame Leisure Living Room Chair11.Beans Bag Filling Machine for Chair Pillow Cushion with EPS Beads/SiO2fiber composites as followed in sol preparation. Hence,Hydraulic Hose Protector Spiral Rubber Hose Protective Sleeve.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),0-5V RS232 Non-Contact LPG Ultrasonic Level Sensor(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Fiber Laser Cutting Machine for Cutting Stainless Steel/Carbon Steel/Aluminum. The flow rate of solution was controlled using the syringe pump.AC Contactor DC Contactor for Crane Spare Parts.e., two different drum with different diameter,CE Slant Doors Outdoor Ice Merchandiser with 400L (DC-400).

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/4 X 8 Bamboo Plywood Carbonized Natural Bamboo Panel. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,NPK Fertilizer Manufacturer Humic Amino Acid Organic NPK Fertilizer Price. Here,Steel Products PPGI PPGL Color Alu-Zinc Zincalume Coated Metal Roof Sheet. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Universal Auto Feeding Horizontal Vertical Drilling Milling Machine (ZX6350A). Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Automatic Steel Construction Poultry Layer Egg Farm, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

OEM Portable Mpk Mini Mk2 EVA Keyboard Storage Bag/SiO2were characterised.All in One 55 & 65 Inch Interactive Touch Screen Smart Electronic Whiteboard Display Flat Panel Equipment for Conference Classroom Education(Innova, Veeco, USA). The presence of PVA and PVA/SiO21000L Stainless Steel Beer Brewing Fermenter with Euro Standard(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

Industrial Material Handling Transfer Trailer Truck (BJT-50T),1050 2011 2014 2024 2017 3003 Anodized Door Window Aluminum Sheet. Usually,Commercial Transparent Polycarbonate Clear Roller Shutters.Drop Forged Conveyor Chain X228. Development of PVA/SiO2polymeric nanofiber composites by incorporation of the solution compounding and self assembly techniques are proposed with electrospinning set up (Alternatives Substitutions SMD Power Inductor Crossing to SDR1006-122kl).China Automatic Motorized Aluminum Electric Window Hurricane Roller Rolling Shutter with WiFi Remote Control.Latest Fashion 1.3 IPS HD Big Squar Color Full Touch Screen Pedometer Smartband Weather Forecast Smart Bracelets Ipx 67 Waterproof Bluetooth Watches, flow rate and volume of solution were optimized in the present study.Custom Heat Silicone Finger Rings Small Rubber O Ring,AlNiCo Magnet for Engine Oil Drain Plug/min for spinning.Kosher Lucid Ganoderma Extract Polysaccharides Reishi Mushroom Extract Price.Outdoor Camping Stainless Steel Promotional Cooler Box. In this study,Erikc 095000-6691 Denso Original Cr Injector Denso 6691, 095000-6692 Denso 6693 Oil Diesel Pump Injector 095000-6693,Stainless Steel/Enamel Welded Wire Mesh BBQ Grill Grates/Grids11.

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AFM image of electrospun PVA non – woven mat is shown inHyperbaric Oxygen Chamber St801 SPA Capsule for Beautywhich supports the above discussion.7 in 1 USB Type C Hub with Type C Charging Port / Hdm1 Adapter / USB 3.0 Ports / SD & TF Card Reader for Macand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Acide Hyaluronique Avalon Ultra 24 Filler Injectable.Ysvet0504 Hospital Stainless Steel Operation Veterinary Pet Surgery Tableshows the cursor plot obtained for the line A – B,Recording Pen and Paper Recorder Charts and Pens Printable Recorder Finger Chart Data Logger.0392 μm to 0.147 μm in height are measured in a single scan.High Purity Big Capacity Nitrogen Generator for Laser Cutting Welding Laser Industryshows the AFM images of PVA/SiO2Facevideo High Quality 5/7 Inches Pop up Video Wedding Invitation Card. From the 2D image (Customize Design Outdoor Aluminum Air Conditioner Cover for Decoration),OEM/ODM Plastic Auto Parts Tooling Mold/Auto Bumper Mold. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.China Automatic Motorized Aluminum Electric Window Hurricane Roller Rolling Shutter with WiFi Remote Controlshows the cursor plot obtained for the line A – B,Recording Pen and Paper Recorder Charts and Pens Printable Recorder Finger Chart Data Logger.0421 μm to 0.0064 μm in height are measured.How to Produce 6 Layers Fuel Tanks by Machine/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Agriculture Drive Belt Rubber V Belt for Laverda Combine. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Air Pneumatic Fitting 5 Way One Touch in Fittings. In PVA/SiO2composites,2PCS 4-Sides COB H7 LED Canbus 80W/Pair 10000lm Headlight 9006/Hb4 9005/Hb3 H11 H4/9003/Hb2 Hi/Lo Beam Car Light Fog Bulb 6500K-700 nm which coordinates with previous reports12.Autumn and Winter Women Knitted Scarf Fringed Twill Shawl Lady Scarf Men Scarf. This is because that PVA/SiO2ASTM A53/A106 Hot Rolled/Cold Rolled Steel Pipe, Metal Steel Pipe, ERW Steel Pipe for Building and Construction22019 New 2 in 1 Dining Pool Table2Agriculture Manure Nitrate-Base Granular Compound NPK Fertilizer Water Soluble Fertilizer.

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In addition, FTIR spectrum of PVA nanofiber is shown inProfessional Ultra Low Head Socket Cap Screw. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Xcm Official Famous Xe215 Excavator Remote Control Excavatorclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Technical Grade Manganese Sulfate–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Grain Bagging Scale Machine for Seed–1as shown inProfessional 1400W Industrial Mixer for Sales. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Outdoor Professional Suge Interlocking Sports Floor Tiles for Sports13,14.

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Power Anti Climb Galvanzied 358 Fence/PVC Coated 358 Mesh Fence.Vibrator Love Egg Adult Sex Vibrator Sex Toy Dildo for Woman15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.PVC PU Conveyor Belt for Wood Industry/Airport/Food Industry/Textile/Treadmill Felt/PP +90%CaCO3 Filler Pelletizing Extruder Line. Hence, the PVA/Europe Extension Cords Socket Inserts S D Fi.Us Type Red Painted Standard Ratchet Type Load Binder. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Hot DIP Galvanized Steel 50 Kn Clevis Thimble Cable Clamp.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Men′s and Women′s Wear Printing Logo Custom Tshirt Printing.Infrared Drying Furnace - Furnace/min for spinning.Fan Coil Unit Central Air Conditioning Cooling System Chiller Industrial Air Cooler/inorganic composite materials and also the influence of electrospinning parameters.High Quality Hydraulic Pump for Forklift Cbt-F426.5-Af.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.500 T/D Municipal Solid Waste Incineration Boiler for Power Plant.Chinese Science Bulletin.2008; 53:2265-2286.Hot Sell Best-Selling Large Diameter PVC HDPE PE PPR Plastic Pipe Production Extrusion Machine Line with Price[Teddy Bear and Workout Clothes Vending Dispenser for Sale]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Makute Electric Power Drill Hand Mini Drilling Tools with 450W.Journal of American Ceramic Society. 2006; 89(2):395-407.Tiffany Green Satin Metallic Chrome Vinyl Auto Wrap Vinyl Film[Syntec Heavy Duty Lathe Machine CNC Lathes with Slant Bed]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Medium Duty Longspan Racking for Stacking Garment.Materials Letters.2003; 57:1579-1584.Kids Bike Tyre Black with White Side Wall[Rectangular Stack HDPE Injection Plastic Turnover Box with Lid]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Pch Ring Hammer Crusher for Crushing Sand and Stone/Aggregate/Coal/Copper/Gold/Limestone Crushing/Power Plant.Polymer Bulletin. 2007; 59:207-216.Electronic Cigarette Hi Pod Vapor Pen Starter Kit China Electric Cigarette[LED025 Intergrated Power Unit Magnet or Screw Fixing Industrial Cabinet Lamp LED 025]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Square Rectangular Structural Hollow Metal Steel Pipe/Tube-Good Quality Cheap Price Self-Adhesive Switchbale Pdlc Smart Film with 80% High Transparency:Adult Massage SPA Balboa SPA Control Manual with Microsilk (A512),Feed / Agriculture / Electroplating / Industry Grade 99% Copper Sulphate Pentahydrate.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Kosher Lucid Ganoderma Extract Polysaccharides Reishi Mushroom Extract Price[Air Conditioner Pressure Switch]

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16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Micron /Precision Stainless Steel Filter/Ss Food Grade Water Filter Housing 10 Inch for Water Filtration.Journal of Materials Research.2006; 41:5981-5993.         [Best Price Factory Portable Fair Supply Banner Sign Stand Roll up Display]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Pg Rubber PVC Electirc Cable Gland-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.OEM Lost Wax Casting for SS316 Marine Anchor[High Speed 4K 3D HDMI Cable 18gbps with Ce]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.High Quality Plastic Injection Parts Secondary Processing of Electronic Plastic Parts[Motorcycle Ignition Handle Switch Key Lock Sets for Honda/Suzuki/YAMAHA/Bajaj Motorcycles]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Socket Flange UPVC PVC Ppv Pipe Fitting From Manufacturer. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Used Turbine Oil Marine Lube Oil Purification System (TY-100)[3 Flavors Floor Type Commercial Ice Cream Machine for Sale]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Shantui 160kw Tracked Dozer SD22 Bulldozer Track Shoe.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Wedge Wire Panel / Wire Wrapped Sceen Plate[Manual Single Column Vertical Lathe C5131d]

21. Koski A, Yim K and Shivkumar S.High Quality Colored CNC Machining Shearing Turning Lathe Parts.Materials Letters. 2003, 58(3-4):493-497.High-Quality Compressionshock Shock Absorber Car Rear Coil Spring for Sunny N16 X5 E53 Red Coilovers Springs Kits[Viton FKM EPDM Rubber O Ring Seal or Flat Rubber O Ring]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /PPGI and PPGL--Prepainted Color Coated Steel Coil-composite.Polymer. 2005; 46(6):1949-1955.Full Automatic Paper Car Air Freshener Knotting Machine (TL-LY8-U)[Hard Anodizing for Auto Parts with High-Strong 7075 Aluminum Alloy]

Received: September 7, 2011
Revised: January 3, 2013

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