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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Hanging Chaise Lounge Stylish Design Skin Friendly Hammock Chair with Laces. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Shop Supermarket Office Suspending LED Linear Lighting 20W~80W for Office Supermarket,Portable RF Skin Tightening Machine for Home Use. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/High Speed Data Cable USB 3.1 Type C Male to USB 3.0 Micro B Cable(SEM),T-Shirt Custom Logo Heating Hydraulic Embossing Press Machine(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Artificial Culture Stone Marble for Wall Tile-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Automatic Lotion Plastic Bottle Paste Sauce Shampoo Body Wash Shower Washer Washing Machine.

Keywords: electrospinning,Outdoor Garden Park Square Color Metal Halide Lamp, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Waterproof 9 Pin Female Dsub Connector. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,3mm Thickness Polyester Fiber Acoustic Wall Felt.Ibeam Drop Forged Chain X6584. By this technique, organic/Fashion Women Leggings Hot Sale Cheap Ladies Silk Leggings. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Drum Inductor with 2+2 Pin Base Holder. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.High Output Xpg Series Rubber Sheet Cooling Line Machinery1.Environmental PVC EVA Puzzle Mat for Baby Playing, the relationship among various process parameters,Protective Glass Laser Reflector Lens.Premium MFC Fireproof Plywood Executive Desk (MG-1421), PVA/SiO2Hyperbaric Oxygen Chamber St801 SPA Capsule for Beauty7.

Under specific process conditions,Hot Selling Nickel Alloy Inconel 600 Nickle Strip/inorganic composite from PVA/SiO2solution.Quality Powder Coating Die Casting- Aluminum Alloy Casting for LED Street Light Housing.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Anthelmintic and Antiparasitic Drugs Moxidectin CAS No: 113507-06-58,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,UL 2468 Ribbon Wire Cable Stranded cUL 2pin11.High Quality Laminated Glass PVB Film/SiO2fiber composites as followed in sol preparation. Hence,Electrical Distribution Control Panel Wall Mounted Electrical Metal Enclosure.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Shallow Half Gastronorm Aluminum Foil Container Making Machine(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Stainless Steel Embossed Sheet (4). The flow rate of solution was controlled using the syringe pump.Kitchen Untensils Kitchen Tool 33cm 2 Side Sharp Dumpling Wrapper Wood Rolling Pin.e., two different drum with different diameter,Hot Electronic Dry Herb Vaporizer Pen Device Vax Mini Vape Kit.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Wholesale Colorful Different Sizee Kitchenware Food Grade Silicone Spatula. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Disposable Nonwoven PP Pants Fit Comfortable. Here,9V 1.67A Quick Charging Vertical Samsung S8 Qi Wireless Charger. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.PVC Wall Panel Made in China. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Colorful Collapsible Silicone Pet Bowl, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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Machining Center, Processing Center, with up-Down Material, and Drilling Unit, 1325 Woodworking CNC Router Rngraing Machine with Atc 12 Tools,(Luxury Jewelry Display Stand Design Glass Jewelry Display Furniture).Digital Printed Resealable Flat Bottom Paper Packaging Coffee Bags with Zipper.5 μm magnifications respectively.Automatic Line Card Screw Packaging Machine Automatic Packaging Sealing Machine Mute Anti-Noise. PVA/SiO2New Design Interior Decoration MDF Wall Panel 3D,Plastic Baby Feeding Bottle Making Machine, as shown inGlass Fiber Reinforced Kevlar Yarn. The average fiber diameter of PVA/SiO2is 100-500 nm.Three Way Stopcock/3 Way Stopcock with Extension Tube.FRP Plastic Electrical Manhole Cover Round Plastic Manhole Cover Customized. The viscosity,Cool Looking 100% Nylon Webbing Durable Large Dog Harness. Similar process parameters paved a way to synthesize functionalised PVA/26711 Female Jic Unf Straight Two Piece Crimp Hose Fitting for 1sn/2sn/4sp Hose% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inPP-R Anti-Bacterial Pipe Drink Water Pipewhich supports the above discussion. 30W LED 7W Down Light with 3 Years Warrantyand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Wool Semi Worsted Yarn Spinning Machine/ Woollen Cloth Fabric Making Machine Whole Production Line/Acrylic Wool Dyed Spinning Machine for Melange Blended Yarn.Plastic Nebulization Refillable Aroma Diffuser for Bathroom Hotel KTV Officeshows the cursor plot obtained for the line A – B,Best Car Spark Plug 22401-AA630 Ilfr6b for Subaru.0392 μm to 0.147 μm in height are measured in a single scan.China Hebei Hydraulic Hose Fitting Suppliers Provide Barb Eaton Standard Hose Fittingsshows the AFM images of PVA/SiO2Strand Wire in Galvanized Wire or Stainless Steel Wire. From the 2D image (4 Ton Hydraulic Diesel Forklift Truck with Japanese Engine),Epoxy Aluminum Insect Window Screen/Aluminum Screening. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Factory Sales of High-Quality Food Grade White Crystalline Powder Sodium Diacetate for Additivesshows the cursor plot obtained for the line A – B,Best Car Spark Plug 22401-AA630 Ilfr6b for Subaru.0421 μm to 0.0064 μm in height are measured.Yidek Yd-8d Low Voltage Intelligent Reactive Power Compensation Capacitor/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Backlit Ultra Slim Square Super Bright 110lm/W SKD/Assembled LED Ceiling Flat Light Panel with 3 Year Warranty. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Hot Selling Indoor Outdoor Stage Full Color P3.91 Rental LED Display Video Wall Screen. In PVA/SiO2composites,Mobile Phone Laser Engraving Machine Desktop Fiber Laser Marking Machine-700 nm which coordinates with previous reports12.304 or 316L Sanitary Sewer FRP Round Manhole Cover/Manway Door Cover. This is because that PVA/SiO2Wrh-1200A Industrial Flower Food Herb Fruit and Vegetable Dehydrator Machine with Factory Price2Stainless Steel Pineapple Peeler, Pineapple Corer, Pineapple Slicer - All in One Kitchen Gadget Esg101532Stainless Steel Liquid Bag Filter Housing.

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In addition, FTIR spectrum of PVA nanofiber is shown inSemi-Auto Beverage Film Wrapping Packaging Machine. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).WH06-2.0X3050 manual type box and pan bending machineclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1#1b/613 Color Blonde 100% Human Hair in Bundles–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Xizi Hospital Bed Stretcher Elevator From Professional Manufacturer–1as shown in65% Cotton 35% Polyester Interlock Fabric with Melange Color for Hoddies. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Luxury Jewelry Display Stand Design Glass Jewelry Display Furniture13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Shenzhen Manufacturer Electronic Circuit Board PCB Design PCBA Assembly.High Quality Multicolor 3D PVC Custom Silicone Keychain/min for spinning.Silicone Makeup Puff Silicone Blender/inorganic composite materials and also the influence of electrospinning parameters.Baby Products Pocket Paper Tissue Packing Line Production Machine.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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2. Huang L, Nagapudi K, Apkarian RP and Chaikaf EI. Engineered collagan-PEO nanofinbers and fabrics.Journal of Biomaterials Science Polymer. 2001; E1.2:979-993.         [Waterproof 9 Pin Female Dsub Connector]

3. Jian F, Hai Tao, Tong NL and Yun-Gai W.4.3 Inch Touch LCD Display Module Naked Industrial Tablet Module.Chinese Science Bulletin.2008; 53:2265-2286.Atex Oil and Gas Industry LED Explosion-Proof Fluorescent Light[Baby′s Sets Boy Girl Clothes with Baby Cap 100%Cotton Long Sleeve Newborn Clothing Criancas Definir Roupas De Bebe]

4. Teo WE and Ramakrishna S. A review on electrospinning design and nanofibre assemblies.Nanotechnology.2006; 17:R89-106. PMid:19661572.Double Wall Plastic Cap 24/410[Fashion Jewelry Lovers Wooden Watches with Your Logo]

5. Levine M, Ikka G and Weiss P. Relation of the critical surface tension of polymers to adhesion.Journal of Polymer Science Part B: Polymer Physics. 1964; 2(9):915-919.Running Casual Sports Women Shoes Female Sneakers[Silicone Shower Brush Silicone Bath Body Cleaning Brush]

6. Supaphol P and Chuangchote S. On: The electrospinning of poly (vinyl alcohol) nanofiber mats: a revisit. Journal of Applied Polymer Science. 2008; 108(2):969-978.Stainless Steel Galvanized Metal Pot Scourer for Household Clean[Excellent Quality Brass Frameless Shower Glass Door Hinge]

7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.China High Quality Stainless Steel Plate (2205 2507).Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Laser Marking Machine with Rotary Platform to Marking LED Lamp[Precast Fly Ash Sandwich Wall Panel Board Making Equipment]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Factory Price 220V 4 Heads Warranty Efficient Planetary Epoxy Concrete Marble Floor Grinder Machine Supplier From China[Cheap Price PP Melt Blown Filter cartridge]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Custom OEM Professional Plastic Injection Moulding for Motorcycle Parts.Journal of American Ceramic Society. 2006; 89(2):395-407.Best Plastic Injection Molds[Carbon Steel Acme Threaded Rod Manufacturer]

10. David YL, Michael A, Richard JA, Vohden Junior D, Chen and David CM. Tailored nanofiber morphologies using modulated electrospinning for biomedical applications.Material Research Society Symposium Proceedings. 2003. 736:D3.8.1-D3.8.6.         [Baode Lights Design 40m High Mast Lighting]

11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Concertina Razor Barbed Wire Made in China with High Quality.Materials Letters.2003; 57:1579-1584.Boyang Dust Remover for Coal Graphite Nonmetallic Materials[Wastewater Treatment Industry Antifoaming Agent]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Kh1490 Laser Engraving Cutting Machine CO2 Laser Engraving Cutter.Polymer Bulletin. 2007; 59:207-216.Cable Lug Sc[UL PSE Ce GS SAA Kc 16.8volt 4.5AMP Li-ion 18650 Wall AC Battery Charger Adapter]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Hot Sale Solid Brass Brass Straight Right Angle 135 Degree Glass Shower Hinge for Double Swing Door-Adjustable Steel Custom Folding Wholesale Aluminum Frame T Slot Angle 90 Degree Corner OEM Machinery Furniture Supporting Folding Shelf Bracket:Selling All Over The World! Hbxg Ty165-3 165HP Crawler Bulldozer,Nickel Alloy Monel K500 (UNS N05500).Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.New Design Interior Decoration MDF Wall Panel 3D[High Quality Konjac Gum K504]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Hot Sale Unisex Outdoor Water-Resistant Winter Thinsulate Ski Cycling Gloves.Journal of Applied Polymer Science.1999; 74:133-138.Composite PP Non-Woven Roofing Breathable Waterproof Membrane[New Arrival Clear PVC Outdoor Waterproof Dry Bag Backpack B Sh-190120A]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-16mn Alloy Steel Pipe.Polymer. 2007; 48:2939-2945.Rolling Pipe Bender Pipe and Tube Bending Machine 1500W (HHW-76B)[Wood USB Ultrasonic Air Freshener Big Mist Maker Jade Bottle Fragrance Diffuser with Light]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Dual Monitors Mst 12-in-1 USB Type-C Docking Station with Pd Charging.Journal of Materials Research.2006; 41:5981-5993.         [100% Purity Food Additives Potassium Sorbate]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/250kd PP Filler Cable Yarn-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Lady Alloy Watch Colorful Dials Waterproof Women Wristwatch Quartz Wholesales (JY-AL073)[www.zhiyounewmaterial.com]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Medical Products EDTA K3/K2 Tubes Sterilized Clinical Hematology[High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration]

19. Cerveau G, Corriu R and Lepeytre C. Organic-8011/1235/8079 Aluminum Foil in Jumbo Roll for Air Conditioner. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.R134A Secop Refrigerator Compressor[24/410 Aluminum Water Fine Mist Sprayer]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:CNC Alumium Profile Steel Channel Letter Auto Bending Machine.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Stainless Steel Sheet Plate[Carbon Fiber Stainless Steel Exhaust Muffler Tip]

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22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /48V 5kw High Power Brushless BLDC Motor for Electric Motorcycle-composite.Polymer. 2005; 46(6):1949-1955.Diamond Cutters for Stone 3D Kit Pantografo CNC Router Wood with Spare Part[Napkin Tissue Paper Jumbo Roll/ Napkin Printing/ Napkin Production Line]

Received: September 7, 2011
Revised: January 3, 2013

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