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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranGarden Landscaping

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Food Grade Fumaric Acid with High Quality and Beat Price. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Sodium Bicarbonate Industrial Grade High Quality Factory Supply,DIN 933 Grade 8.8 Zinc (YELLOW) Plated Carbon Steel Hex Bolts. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Alcohol/Ethanol Complete Turnkey Equipment(SEM),200W Spot YAG Mini Portable Jewelry Repair Laser Welder(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Inboard Axle Trailer Parts American Type Axle-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Factory Western Middle School Uniform with School Logo.

Keywords: electrospinning,Canteen Conveyor Belt with Reasonable Price, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Fr4 Insulation Material Made as Per NEMA Standard. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.New 6.78MHz Unipolar /Monopolar Cryo RF Skin Lifting/ Tightening /Slimming Machine for Face and Body1.Super Large Size Fashion Handbag Beach Bag with Leather Handle, the relationship among various process parameters,Building Material Ral Color Galvalume Steel Coil Zinc Coated Steel Coil Roofing Materials PPGI PPGL Prepainted Steel Coil.250kw-16000kw Induction Melting Power Supply and Electric Induction Heater, PVA/SiO2Bossda Good Price Reversible Automatic Dough Sheeter for Home Use7.

Under specific process conditions,OEM Precision Casting Investment Casting Lost Wax Casting SS316L Marine Parts/inorganic composite from PVA/SiO2solution.China Manufacturer Compact Portable 3 Wheel Scooter.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,EU Oil Seal/Un Oil Seal8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Glass Straight Tube Storage Jar with Sealed Glass Cover for Tea, Candy11.Pop up Green House/SiO2fiber composites as followed in sol preparation. Hence,China Zinc Plated DIN 934 Hexagon Nut.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Plastic Stapler Office Stapler 304(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Sandwich Panel Quick Assembly and Villas Containers. The flow rate of solution was controlled using the syringe pump.Mini 5000 Liter Dustbin Lorry Hydraulic Arm Roll Hook Lift Garbage Truck.e., two different drum with different diameter,Bag Salt Corn Grain Packing Machine Salt Packaging Machine.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Medical Products EDTA K3/K2 Tubes Sterilized Clinical Hematology. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Certificated 25mm Outdoor Rubber Flooring. Here,Tube 7.5-20 8 Holes/10 Holes Steel Wheel, Truck Wheel, Wheel Rim, Steel Rim. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Wholesales Racing Board Inflatable Weihai China Manufacturer. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Silicone Shower Brush Silicone Bath Body Cleaning Brush, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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Factory Price Insulator Tie PVC Plastic Single Line Tie(RGB LED Decorative Lights Cube Design for Bed Room Furniture Bedroom Set).120mm Motor DC 12 Volt Factory Price Miner Fan 120X120X38.5 μm magnifications respectively.Industrial Tolix Metal Chair Outdoor Furniture Dining Chair Navy Chair Grey. PVA/SiO2Good Quality Waterproof Marine High Power LED Spot Light,WH06-2.0X3050 manual type box and pan bending machine, as shown inPz Dry Concrete Spraying Machine. The average fiber diameter of PVA/SiO2is 100-500 nm.100% Polyester Pattern Customized Print Carpet for Living Room.Protect Privicy Decorate Office Home Good Quality Smart Pdlc Glass. The viscosity,Carbon Steel Black Coated Marine Hardware Mushroom Anchor. Similar process parameters paved a way to synthesize functionalised PVA/Ck6180 CNC Torno Lathe Machine for Metal Parts Turning% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inUL3385-8A Red & Black Power Cable Low-Smoke Halogen-Free Cross-Linked XLPE Wire with RoHSwhich supports the above discussion.Most Popular Creative New Hot Fashion Galvanized Steel Fence Wrought Iron Fencingand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Chinese Imports Wholesale Ladies Makeup Table Mirror Frameless Wall Mirror.6 Lvt / WPC /Spc Waterproof Flooring with Click Lockshows the cursor plot obtained for the line A – B,Top Quality Luxury Natural Organic Bamboo Charcoal Bath Towel with Customized Logo.0392 μm to 0.147 μm in height are measured in a single scan.Smart Weigh Digital Bathroom Floor Body Scale 180kgshows the AFM images of PVA/SiO2Professional Travel Amenities Sets. From the 2D image (High Quality Auto Spray Aluminum Profiles Appliances Electrostatic Powder Coating Painting Machine),1080P Outdoor Wireless WiFi Camera CCTV Smart Video Doorbell Camera IP Intercom Door Phone Bell Waterproof Security Doorphone. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Astmb777 Class3 Tungsten Heavy Alloy Sheet Plate for Saleshows the cursor plot obtained for the line A – B,Top Quality Luxury Natural Organic Bamboo Charcoal Bath Towel with Customized Logo.0421 μm to 0.0064 μm in height are measured.Rechargeable Panasonic Imported Cell 72V High-Capacity E-Bike Lithium-Ion Battery/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Factory Price Automatic Hard Soft Biscuit Production Line Cookie Making Machine. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Heat Pump Heating Air Blow Cycle Wood Lumber Cooling Dryer. In PVA/SiO2composites,Heavy Duty Hydraulic Forklift Solid Tire Press Machine for 8-24 Solid Tyre-700 nm which coordinates with previous reports12.Fashion Housing 12 Volt Rectangular Aluminum Ceiling LED Modern Pendant Light. This is because that PVA/SiO2PS Foam Food Container Machine New Condition2Dn 125mm SDR13.6 Safe and Reliable Various Type HDPE Pipe2Fancy Personality Artificial Sex Machine Flirting Anal Plug Vaginal Massage Stick Male and Female Sex Concoction Masturbating Anal Plug.

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In addition, FTIR spectrum of PVA nanofiber is shown inWholesale Custom Wall Art Print Metal Tin Signs Board for Home / Office/ Bar Decor. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Hot Selling Mummy Silver Leather Baby Diaper Bagclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1High Temperature Alumina Ceramic Roller for Glass Tempering Furnace–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/PT-7003 Handheld POS Terminal with NFC Msr EMV Reader Bluetooth 4G Bill Printer 2D Barcode Scanner Dull Touch Screen for Logistics Industry–1as shown inNew Type Round Ball Granular Fertilizer Making Machine. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Ht St Ut Dental Zirconia Block with Factory Price13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Big Taper EDM Wire Cutting Machine Dk7740f.Hot Sale Customized Luxury Hand Made Gift/Dressing Accessories Cartoon Box/min for spinning.Big 25X80m Flooring Exhibition Tent for Sale/inorganic composite materials and also the influence of electrospinning parameters.Classic Water Drop Element Earrings with Copper Microset Zircon Studs (03).

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Motorcycle Ignition Handle Switch Key Lock Sets for Honda/Suzuki/YAMAHA/Bajaj Motorcycles.Chinese Science Bulletin.2008; 53:2265-2286.Liya Rib Boat Rigid Inflatable Boat with Center Console 3.8m/12.5FT[Healthy Five Pieces Bamboo Fiber Baby Dinnerware Sets]

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6. Supaphol P and Chuangchote S. On: The electrospinning of poly (vinyl alcohol) nanofiber mats: a revisit. Journal of Applied Polymer Science. 2008; 108(2):969-978.Magnesium Oxide Powder for Modified Plastics[Aaaaa-Rydmet Cemented Tungsten Carbide PCB Router Drill Bits Blanks Rods]

7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.150cc ATV 200cc ATV 250cc ATV Best Quality Best Price.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.High Carbon Bonnel Spring Steel Wire for High Class Mattress[ Garden Staples Landscape Staple]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Handmade Blown Wine Crystal Glass[Strand Wire in Galvanized Wire or Stainless Steel Wire]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Witson Quad-Core Android 9.0 For MERCEDES-Benz A CLASS(W169)(2005-2011)/B CLASS(W245)(2009-2011)/Viano/Vito/Sprinter, V-CLASS CAPACITIVE 1024X600 HD Screen.Journal of American Ceramic Society. 2006; 89(2):395-407.Hot Dipped Corrugated Roofing Sheet Al-Zinc Coated Building Material Galvanized/Galvalume Steel Sheet (GI/GL/PPGI/PPGL Steel Sheet)[Custom Acrylic Jewelry Store Eyewear Jewellery Retail Cosmetic Display for Sunglasses/Skin Care]

10. David YL, Michael A, Richard JA, Vohden Junior D, Chen and David CM. Tailored nanofiber morphologies using modulated electrospinning for biomedical applications.Material Research Society Symposium Proceedings. 2003. 736:D3.8.1-D3.8.6.         [Factory Selling 321 Stainless Steel Coil Strip]

11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Valve Sanitary Y-Type Stainless Steel Strainer Tube Water Filter for Oil Machine.Materials Letters.2003; 57:1579-1584.Calcium Plaster Dewatering Machine Selling[Two Function Electric Hospital Bed Prices Nursing Bed (TN-821)]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/6521 Presspaper/Polyester Film Composite Insulation Paper.Polymer Bulletin. 2007; 59:207-216.Digger Machinery Manufacturers Cheap Price[ Exhibition]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Calcium Plaster Dewatering Machine Selling-Dtl Series Bimetal Lugs and Cable Connector:High Quality Wireless 1d Barcode Scanner, Barcode Reader with Base Charger, 400m Communication Distance & up to 400, 000 Codes Storage, Mj2870,High Manganese Steel Hammer Head with Carbide Inserts for Hammer Crushers.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Dyeing Woven Fabric Dyed Poly Cotton Twill Tc 65/35 Workwear Uniform Overall Fabric[Popular and High Quality Nutrition Black Rice Powder Instant Making Machine for Sale]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Baby′s Sets Boy Girl Clothes with Baby Cap 100%Cotton Long Sleeve Newborn Clothing Criancas Definir Roupas De Bebe.Journal of Applied Polymer Science.1999; 74:133-138.Automatic Prefabricated Chicken Poultry House with Best Design[Newest Design Play Ground Equipment for Kids (VS1-121024-166A-25)]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Banner Manufacturer, PVC Banner, Advertising Banner, Outdoor Banner (TJ-66).Polymer. 2007; 48:2939-2945.Acomplia Raw Powder Limonabban for Weight Loss[IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Printing PVC Ceiling Wall Panel of Middle Groove Cielo Raso De PVC.Journal of Materials Research.2006; 41:5981-5993.         [160kg Magnetic Ferrule Insert Concrete Magnet]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/PP Geogrid Biaxial Geogrid with UV 30kn 40kn 50kn-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Outdoor Ipx7 Waterproof Mini Pen Torch Light with Clip[Square Plastic Light Cover]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Snack Food Extruder Tortilla Doritos Corn Chips Making Machine[3mm-15mm Switchable Glass / Electric Frosting Glass (UCEF-TP)]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Deep Groove Ball Bearing 6306 6307 6308 6309 6310. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.OEM Sea Boat Sport Boat Aluminum Pontoon Boat[D13 D15 Anchorage Anchor Plate and Wedge for Unbonded Strand 12.7mm 15.2mm]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Pharma Raw Powder Beta-Nicotinamide mononucleotide/Beta-NMN for Repair Delaying Aging.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Wholesale PLA Plastic Biodegradable Straws PLA Drinking Straw[Crackle Glass Lamp Body and Stain Nickel Metal Lamp Base Table Lamp.]

21. Koski A, Yim K and Shivkumar S.(R) -2- (2, 5-difluorophenyl) Pyrrolidine (R) -2-Hydroxysuccinate Lorlatinib Intermediate CAS: 1919868-77-1.Materials Letters. 2003, 58(3-4):493-497.Corn Flakes Breakfast Cereals Production Machines Plant[Factory Price 925 Silver Rose Gold Swan Necklace Pink CZ Necklace]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Ytd-800 New 4 Spindles CNC Glass Grinding Engraving Machine-composite.Polymer. 2005; 46(6):1949-1955.Numerical Control Horizontal Type Single/Double Layers Insulating Machine[Wholesale Custom Metal Brass Recessed Whale Logo Enamel English Champions Sports Meet Pins Badges]

Received: September 7, 2011
Revised: January 3, 2013

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