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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. Rajendranm.zgnfsjx.com

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Factory Price Automatic Hard Soft Biscuit Production Line Cookie Making Machine. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Heat Pump Heating Air Blow Cycle Wood Lumber Cooling Dryer,Heavy Duty Hydraulic Forklift Solid Tire Press Machine for 8-24 Solid Tyre. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Fashion Housing 12 Volt Rectangular Aluminum Ceiling LED Modern Pendant Light(SEM),PS Foam Food Container Machine New Condition(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Dn 125mm SDR13.6 Safe and Reliable Various Type HDPE Pipe-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Fancy Personality Artificial Sex Machine Flirting Anal Plug Vaginal Massage Stick Male and Female Sex Concoction Masturbating Anal Plug.

Keywords: electrospinning,High Temperature Alumina Ceramic Roller for Glass Tempering Furnace, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Durable High Sensitive Black PIR Fresnel Lens for Outdoor. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Big Taper EDM Wire Cutting Machine Dk7740f1.Hot Sale Customized Luxury Hand Made Gift/Dressing Accessories Cartoon Box, the relationship among various process parameters,Big 25X80m Flooring Exhibition Tent for Sale.Classic Water Drop Element Earrings with Copper Microset Zircon Studs (03), PVA/SiO2Motorcycle Ignition Handle Switch Key Lock Sets for Honda/Suzuki/YAMAHA/Bajaj Motorcycles7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Valve Sanitary Y-Type Stainless Steel Strainer Tube Water Filter for Oil Machine8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,6521 Presspaper/Polyester Film Composite Insulation Paper11.Calcium Plaster Dewatering Machine Selling/SiO2fiber composites as followed in sol preparation. Hence,Dtl Series Bimetal Lugs and Cable Connector.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),High Manganese Steel Hammer Head with Carbide Inserts for Hammer Crushers(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Baby′s Sets Boy Girl Clothes with Baby Cap 100%Cotton Long Sleeve Newborn Clothing Criancas Definir Roupas De Bebe. The flow rate of solution was controlled using the syringe pump.Banner Manufacturer, PVC Banner, Advertising Banner, Outdoor Banner (TJ-66).e., two different drum with different diameter,Printing PVC Ceiling Wall Panel of Middle Groove Cielo Raso De PVC.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/PP Geogrid Biaxial Geogrid with UV 30kn 40kn 50kn. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Deep Groove Ball Bearing 6306 6307 6308 6309 6310. Here,Pharma Raw Powder Beta-Nicotinamide mononucleotide/Beta-NMN for Repair Delaying Aging. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.(R) -2- (2, 5-difluorophenyl) Pyrrolidine (R) -2-Hydroxysuccinate Lorlatinib Intermediate CAS: 1919868-77-1. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Ytd-800 New 4 Spindles CNC Glass Grinding Engraving Machine, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown in8mm 10mm 12mm HRB500 Reinforcing Steel Rebar Deformed Iron Barwhich supports the above discussion.Tempered Safety Anti-Slip Laminated Glass Stair Treadsand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Green Lovely Small Size Gift Packing Paper Box.Yc Excellent Quality 120 to 150 Degree Resistance Dust Collector Spare Parts Dust Filter Bagshows the cursor plot obtained for the line A – B,Running Casual Sports Women Shoes Female Sneakers.0392 μm to 0.147 μm in height are measured in a single scan.6kw 12000rpm Spindle Motor for Woodworking Milling Machineshows the AFM images of PVA/SiO2Ss Wide Angle Flat Fan Water Jet Spray Nozzle. From the 2D image (hongxin-ec.com),Waste Tire Rubber Block Cutter Machine/Rubber Bolck Cutting Machine. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Us Type Red Painted Standard Ratchet Type Load Bindershows the cursor plot obtained for the line A – B,Running Casual Sports Women Shoes Female Sneakers.0421 μm to 0.0064 μm in height are measured.VB10-63 Series Mini Circuit Breaker/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Industrial Plastic Air Source Lockout. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.LED Ceiling Square Round Recessed Grid Downlight Ultra Thin Ceiling Lamp 2835 SMD Lighting Ce LED Light. In PVA/SiO2composites,4-19mm Custom Toughened Tempered Laminated Glass-700 nm which coordinates with previous reports12.Double Folding Wings in Hydraulic Pressure Offset Middle-Duty Disc Harrow. This is because that PVA/SiO2PPGI PPGL Color Steel Coils Prepainted Galvanized Steel in Sheets2Silver High School Graduation Honor Sashes and Stole2Outdoor LED Street Light Housing with High Power.

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In addition, FTIR spectrum of PVA nanofiber is shown inExcellent Eco Solvent Printer Mt-3207de Dx7 Printhead 1440dpi. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).High Quality Shackle Carbon Steel Large Bow Shackleclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1CNC Plasma Cutting Tables for Sale–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Form - Fill - Seal Horizontal Bag, Pouch / Sachet Packaging Machine–1as shown inNew Project Hot Luxury Glamping Hotel Tent for Resort. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Tempered Safety Anti-Slip Laminated Glass Stair Treads13,14.

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4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.32-100mm Pipe Drain Cleaner Machine Cleaning.Christmas Custom Made Knitted Winter Beanies with Embroidery Logo/min for spinning.Surface Mounted LED Downlight, Round and Square Options/inorganic composite materials and also the influence of electrospinning parameters.Compatible CF280A Toner Cartridge for HP Laserjet PRO 400/M401 Toner.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Wholesale Custom Lycra Printed Sport Leggings.Chinese Science Bulletin.2008; 53:2265-2286.Commercial Rotational Electric Indoor Playground on Sale[Medium Duty Longspan Racking for Stacking Garment]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Scrap Plastic PE Pet PVC PC PP Bottle Recycling Machine.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Infrared Quartz Heating Emitter 2500W 240V[Easy Maintenance Full Automatic Powder Coating Line Machinery]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Anti Climb Security Airport Fence with Razor Barbed Wire Top[NTN NSK Koyo SKF Timken Taper Roller Bearing 30215]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Top Sale Canada PVC Portable Garden Temporary Fence Panel.Journal of American Ceramic Society. 2006; 89(2):395-407.Anti-Insect Soft Flexible Clear Transparent Standard PVC Plastic Roll PVC Door Curtains[Decoration Exhibition Fashion Digital Printing Knitted Football Fans Bandana Scarf]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /China Custom High Precision Aluminum Bush.Materials Letters.2003; 57:1579-1584.Automatic Broiler Chicken Slaughter Machine/Chicken Slaughter Line for Sale[Pure Material Drinking Water HDPE Pipes with Best Prices Good]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Multi-Wedge Rubber Belt From Ningbo China.Polymer Bulletin. 2007; 59:207-216.Telescopic Hydraulic Cylinder for Sale[4.3 Inch Touch LCD Display Module Naked Industrial Tablet Module]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Vertical Stair Elevator for Disabled/Old People-Laser Marking Machine for Automatic Engraving Qr Code on PCB Surface:Chemicals Aluminum Sulphate 16% 17% Al2 (SO4) 3,Sc Square Type Bare Fiber Adapter.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Permanent Magnetic Rare Earth Neodymium Cylinder Magnets[PS Foam Food Container Machine New Condition]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Factory Price 925 Silver Rose Gold Swan Necklace Pink CZ Necklace.Journal of Applied Polymer Science.1999; 74:133-138.CNC Alumium Profile Steel Channel Letter Auto Bending Machine[Bb Tuba Brass Instrument À Venda]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Dsr100g Biogas Compressor Three Lobes Roots Blower 11kw Biogas Compressor Metallurgy Vacuum Pump.Polymer. 2007; 48:2939-2945.Single Phase Dual Capacitor Cast Iron Aluminium Housing Induction Motor for Water Pump Air Compressor Gear Reducer Fan Blower[WPC Decking Fence Floor Profile Extrusion Line / Production Line]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Electro Galvanized Welded Wire Mesh Panels for Floor.Journal of Materials Research.2006; 41:5981-5993.         [a-One Precision Wire Cut Vise with Fine Adjustment Function 3A-200005]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Granules Packaging Machine Grain Food Filling Sealing Packing Equipment Rice Filling Line Monosodium Glutamate Packaging Machine-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Shenzhen Manufacturer Electronic Circuit Board PCB Design PCBA Assembly[6 Person Office Desk White Executive Office Desk Modular]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Rubber Roller Conveyor[High-Quality Fine Pixel Pitch Ultra HD LED Display / Flat LED Video Screen Panel 400*300mm (P1.25]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Light-Weight Portable Hand Sandblaster, Shot Blasting Equipment, Sand Blasting Machine. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Wide Used Xm2-25 Perforated Clay Brick Making Machine Manual Soil Block Machine in Africa[Green Lovely Small Size Gift Packing Paper Box]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Rutile Grade of Titanium Dioxide TiO2 for Printing Ink.Journal of Sol-Gel Science and Technology.1997, 8:603-607.m.cnbdlift.com[Fiber Glass Tape Mesh (screening)]

21. Koski A, Yim K and Shivkumar S.Bestseller 2019 Heart Shaped Hip Flask.Materials Letters. 2003, 58(3-4):493-497.Coal Mine Roadway Explosion-Proof Electrical Shotcrete Machine with Ce[Machinery 316L Stainless Steel Bright Anneal Seamless Ss Pipe]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /750ml Dark Green Frosted Glass Red Wine Bottle-composite.Polymer. 2005; 46(6):1949-1955.Plastic Hood for D-SUB Connector Waterproof D-SUB Connector[Custom Pcb Manufacturing]

Received: September 7, 2011
Revised: January 3, 2013

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