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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. Rajendran9 Gauge Welded Wire Mesh

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Luxury Jewelry Display Stand Design Glass Jewelry Display Furniture. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Non-Curing Rubber Asphalt Waterproof Coating,High Precision Circle Ring Bracelet Rotary Laser Cutter with Gold Dust Recycling. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Cold Stamping Deep Drawn Stainless Steel Sheet Metal Forming Parts(SEM),Pz Dry Concrete Spraying Machine(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,160kg Magnetic Ferrule Insert Concrete Magnet-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/100% Purity Food Additives Potassium Sorbate.

Keywords: electrospinning,High Quality Carbonless Copy Paper for Bank Usage, PVA/SiO2composite, nanofiber mats.


1. Introduction

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4.3 Inch Touch LCD Display Module Naked Industrial Tablet Module. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,China High Quality Stainless Steel Plate (2205 2507).Custom OEM Professional Plastic Injection Moulding for Motorcycle Parts4. By this technique, organic/Concertina Razor Barbed Wire Made in China with High Quality. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Kh1490 Laser Engraving Cutting Machine CO2 Laser Engraving Cutter. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Hot Sale Solid Brass Brass Straight Right Angle 135 Degree Glass Shower Hinge for Double Swing Door1.Adjustable Steel Custom Folding Wholesale Aluminum Frame T Slot Angle 90 Degree Corner OEM Machinery Furniture Supporting Folding Shelf Bracket, the relationship among various process parameters,Selling All Over The World! Hbxg Ty165-3 165HP Crawler Bulldozer.Nickel Alloy Monel K500 (UNS N05500), PVA/SiO2Hot Sale Unisex Outdoor Water-Resistant Winter Thinsulate Ski Cycling Gloves7.

Under specific process conditions,16mn Alloy Steel Pipe/inorganic composite from PVA/SiO2solution.Dual Monitors Mst 12-in-1 USB Type-C Docking Station with Pd Charging.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,250kd PP Filler Cable Yarn8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,8011/1235/8079 Aluminum Foil in Jumbo Roll for Air Conditioner11.CNC Alumium Profile Steel Channel Letter Auto Bending Machine/SiO2fiber composites as followed in sol preparation. Hence,Smart Waterproof Tablet Case for iPad PRO 10.5.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Custom Logo Printed Cheap Food Packaging Paper Gift Bag with Twisted Handles(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Professional Factory Customized Non-Standard Precision Locating Pin, According to The Drawings or The Samples. The flow rate of solution was controlled using the syringe pump.Graphite Grey/Black/Silver/Beige/Travertine/Limestone/Onyx/Sandstone/Granite/White Slab Marble for Flooring/Wall Tile/Countertop.e., two different drum with different diameter,Nestable Heavy Duty HDPE Large Double Deck Plastic Storage Pallet.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Flexible PVC Rubber Air Natural LPG Gas Cooker Hose with High Pressure. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,110 Type Connector Extension Cord Terminal for Male. Here,High-Quality Fine Pixel Pitch Ultra HD LED Display / Flat LED Video Screen Panel 400*300mm (P1.25, P1.56, P1.66, P1.875, P1.92, P2). 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Outstanding Self-adhesive HDPE Pre-applied (non asphalt) Membranes. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.OEM Ozone Generators Parts Cell Assembly Part, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

XCMG Electric Drive Tipper Xde240 Mining Truck/SiO2were characterised.Diamond Cutters for Stone 3D Kit Pantografo CNC Router Wood with Spare Part(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Household Digital Electronic Kitchen Scale with 2L Bowl (SKE203)(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inHigh Quality 95% Proanthocyanidins Pine Bark Extract Powderwhich supports the above discussion.Steel Lined PE (PTFE / PP /PO) Pipe for Chemical Factoryand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Industry Use Wood Sawdust Biomass Wood Chip Burner Price.Outdoor Camping Stainless Steel Promotional Cooler Boxshows the cursor plot obtained for the line A – B,Gypsum Ceiling Board / Access Panel.0392 μm to 0.147 μm in height are measured in a single scan.Lemoes FHG Elbow 90 Degree Plug to D-Tap Cable Connectorshows the AFM images of PVA/SiO2Customized Strong Heat Resistant Rare Earth Permanent SmCo Magnets for Industry. From the 2D image (Custom Made P7.62-16X96 RGB Full Color LED Sign with USB/RS232/TCP-IP Communication Control),Transparent LDPE Reusable Recyclable Household/Chemical Plain Different Size Reclosable Grip Seal Bag Zipper Bag Ziplock Bag. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Free Shipping Night Vision Scope Evening Sight IR Goggles Monocularsshows the cursor plot obtained for the line A – B,Gypsum Ceiling Board / Access Panel.0421 μm to 0.0064 μm in height are measured.Sell Hot Selling High Quality Copper Scrap / Copper Wire/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Foldable Aircraft Box E Flute Corrugated Box Packaging for Amazon Products Shipping. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Carbon Paper Rolls with Carbonless NCR Paper for Rent Receipt. In PVA/SiO2composites,High Quality Handmade Cat House Pet Nest Felt Cat Bed-700 nm which coordinates with previous reports12.Good Quality Project 100W/200W/300W/400W COB LED Floodlight. This is because that PVA/SiO242bly3a78 24VDC 0.1nm Low Voltage DC Motor BLDC Motor/Brushless DC Motor/Brushless Motor for Textile Machinery2White and Black Color Plastic Resin Folding Hotel Chair2Er5183 Chinese Manufacturer of Aluminum Welding Wire (MIG/TIG).

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In addition, FTIR spectrum of PVA nanofiber is shown inTitan 40 Tons Cement Bulk Carriers for Sale. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Makute Electric Power Drill Hand Mini Drilling Tools with 450Wclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Best Price Digital Waterproof Security 6 8 12 18 33 Zone Guard Spirit Portable Walk Through Metal Detector–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Polished Bright AISI 304 Seamless Stainless Steel Tube–1as shown inQt4-20 AAC Brick Block Making Machine Price Nepal. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1High-Performance Engines Iridium Spark Plugs 3144 Dcpr7eix13,14.

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Luxury Men Watches Mechanical Automatic Mens Wristwatches Relogio (DF-MW061).Galvanised Serrated Steel Bar Grating with Close Ends15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Wholesale Price Steel Hotel Hall Banquet Chair for Restaurant Wedding Rental/24 Zones Walk Through Metal Detector for Airport, Station, Exhibition, Police, Public Area Security. Hence, the PVA/Plastic PVC Reinforced Wire Helix Pipe Hose Extrusion Production Line.Zinc Cr Al Coating Low Carbon Steel Alloy Metal Stamping Parts. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Sliding Double Glass Door Roller/ Shower Door Roller Pulley.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.LED Bulb A60, LED Light Bulb E27/B22 5/7/9/12W.Auto Spare Parts Car Accessory Corrugated Flexible Exhaust Pipe Muffler/min for spinning.310 Roof Ridge Cap Roll Forming Machine for Sale Craigslist/inorganic composite materials and also the influence of electrospinning parameters.Lemoes FHG Elbow 90 Degree Plug to D-Tap Cable Connector.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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3. Jian F, Hai Tao, Tong NL and Yun-Gai W.Investment Casting Stainless Steel Casting Valve Parts Valve Body.Chinese Science Bulletin.2008; 53:2265-2286.OEM Manufacturer 12V 24V Small DC Planetary Gear Motor[42cm 3D Hologram Fan with WiFi Holographic LED Fan Display]

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.7years Warranty 110lm/W High Power LED Street Light.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Medical Automatic Volumetric Infusion Syringe Pump; IP737[Qt4-20 Brick Molding Machine Pavers Block Brick Making Machine]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Hot Selling Wall PIR Motion Sensor for Home Security[Most Popular Long Service Life Basketball Courts Flooring/Basketball Gym Floor]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.55311-1h200 349084 Auto Spare Parts Cheap Shock Absorbers for KIA.Journal of American Ceramic Society. 2006; 89(2):395-407.Galvanized Steel Band[Automatic Sf6 Gas Hexafluoride Density Relay Calibrator]

10. David YL, Michael A, Richard JA, Vohden Junior D, Chen and David CM. Tailored nanofiber morphologies using modulated electrospinning for biomedical applications.Material Research Society Symposium Proceedings. 2003. 736:D3.8.1-D3.8.6.         [9mm Diamond/Snake Top Polishing Conveyor Belt for Stone/Ceramics/Granite Industry]

11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Portable Standing Seam Roof Panel Roll Cold Forming Tile Machine.Materials Letters.2003; 57:1579-1584.Customized Shape Cosmetics PVC Blister[Beitian Gnss GPS Antenna for Zed-F9p Module Rtk Drone Base Uav Ugv GPS Glo Gal Bds Gnss L1]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Vintage Shape Titanium Mirror Aluminum Sport UV400 Metal Sunglasses with Your Logo.Polymer Bulletin. 2007; 59:207-216.New Fashion Metallic PU Designer Lady Three Fold Purses[Stackable Brown Color Beech Wood Cross Back Chair for Garden]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Factory 316L 304 Seamless/Welded Stainless Steel Pipe Price for Industry-Hydrogen Oxygen Generator Car Engine Decarboniser Machine:Steel Metal Leg Gaming Play Executive Table Office Wooden Furniture,LED Interior Lighting UFO Dimmable Industrial LED High Bay Lighting Fixture.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Customized colorful cute animal wholesale promotional funny stuffed graduation owl plush toy[Forged Lashing D Ring with Bolt and Bracket]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Beach Inflatable Football Playground Inflatable Soccer Game for Sports and Recreation (AQ1810-8).Journal of Applied Polymer Science.1999; 74:133-138.Outdoor LED Street Light Housing with High Power[Good User Reputation for Stainless Steel Dampers - AC1010-S - Zhuohui]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Hotel Furniture Living Room Fabric Recliner Sofas.Polymer. 2007; 48:2939-2945.At600va 360W High Quality LED Line Interactive UPS with Smart Functions[Kexinda Metal Ceiling Cross T Bar Roll Forming Machine for Sale]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Customize Design 24 Cavity Medical Urine Cup with Lid Mould.Journal of Materials Research.2006; 41:5981-5993.         [Car Parts Cylinder Head for Volkswagen Bora1.6 Jetta/Golf/Passat/Caddy/Touran/Bettle]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Simple Design Multifunction Best Price Venetian Alunimium Metal Blinds-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.DIN928/929 Steel Weld Nut / Square Weld Nut / Hex Weld Nut[Heavy Duty Galvanized Ground Screw Anchor]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Dtp Custom Rechargeable 36V 20ah Li-ion Battery Pack for Electric Ebike[Automatic Electric Frozen Lamb Beef Chicken Deli Meat Slicer Cutter]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Metal/Wood/Stone Engraving CNC Router Dw1325. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.60W CO2 Laser Marking Machine Lx-2000b Apply to Wood Products[Nestable Heavy Duty HDPE Large Double Deck Plastic Storage Pallet]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Mobile Food Cart /Taco Cart for Sale.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Kid′s Cute Portable Finger Shape Silicone Mini Desk Clock[Good Strength Galvanized Iron Wire Binding Wire with Ce and SGS for Building Material]

21. Koski A, Yim K and Shivkumar S.Factory Price Commercial Use Herb Grinder with Ce.Materials Letters. 2003, 58(3-4):493-497.200 Mesh Calcium Carbonate Grinder Roller Mill Machine[Original Cellphone Refurbished S10 Unlocked Mobile Phone]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Glass Ampoule Sealing School Laboratory Equipment-composite.Polymer. 2005; 46(6):1949-1955.High Quality Auto Car Parts Semi Metal Disc Brake Shoes for Nissan K1197[China Cast Foundry High Quality Products]

Received: September 7, 2011
Revised: January 3, 2013

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