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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. Rajendranm.fencing-cn.com

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Chademo/CCS DC and AC Intergrated EV Charger for EV Charging Station. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Laser Die Board Cutter for Wooden Die From Yitai Die Making,Factory Wholesale Customized Cheap New Plastic Antique Soft PVC Zinc Alloy Die Casting Laser Engrave Bottle Shape Magnet Keyring Beer Bottle Opener. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Plastic PVC Drainage Conduit Water Pipe Belling Machine/Socketing Expander(SEM),Rotary Hydraulic Actuators Price(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Slim Metal Frame Glass Mobile Phone Case with Magnet Flip Cover for Apple iPhone X-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Socket Type HDPE Pressure Pipe Fittings Male/Female Coupling.

Keywords: electrospinning,Black Carbon Welded Square Steel Pipe, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Die Cast Zinc Alloy Gold Plated Half Marathon Medal for Promotion Sale (160). The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Newest Green Blue Plastic Frame Reading Glasses.2018 Spring Fashion Waterproof Outdoor Hoody Rain Jacket4. By this technique, organic/Large Scale Countertop Stone Granite Edge Profiling Machine. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-ASTM A312 304L Stainless Steel Pipe Price with Cheap Price. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.New Bone China Glaze Pure White Porcelain Glass1.Mangiferin 90-98%Factory Supply Mango Extract CAS No. 4773-96-0, the relationship among various process parameters,White Metal Babbitt Sliding Bearing Bush /Shoe / Pillow for Cement Mill.Carbon Fiber Stainless Steel Exhaust Muffler Tip, PVA/SiO2Soft PVC Super Clear Film for Window Usage7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,New Type Round Ball Granular Fertilizer Making Machine8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Heavy Duty 2: 1 A4 Size Wire Punching and Binding Machine Cw300t11.China A36 Q235B S275 Ss400 Anti-Slip Checkered Ms Carbon Steel Plate/SiO2fiber composites as followed in sol preparation. Hence,Oil Resistant U-Type Rubber Seal.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),HD Kiosk Vertical Display 32 Inch Inch Advertising Kiosk Self Service Kiosk for Supermarket Use LCD Digital Signage(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Rubber Mixing Mill/Two Roll Open Mill/Rubber Mixing Machine. The flow rate of solution was controlled using the syringe pump.CNC Milling Mill Lathe Machine Hand Turning Cutting Tools.e., two different drum with different diameter,Face Skin Rejuvenation PDT LED Light Therapy for Salon and Clinic.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/ABS Safety Padlock Lockout Tagout Kit Form Padlock Manufacturing Company. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Plastic Injection Flip Top Cap Mould (YS832). Here,High Efficient Online Hot Glue Dispensing Machine for PCB. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Cement Sprayer Mortar Spraying Machine with Mixer. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Large Span Prefabricated Steel Structure Frame for Pre-Engineered Steel Structure Building, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Infrared / Reflect/Laser/Optical/Mo Reflecting Mirror/SiO2were characterised.2019 PU Leather Sling Cross Body Lady Handbag(Innova, Veeco, USA). The presence of PVA and PVA/SiO22018 High Precision New MIM Metal Powder Injection Molding Electric Powder Auto Parts(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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24/410 Aluminum Water Fine Mist Sprayer(Wall Mounted SMC Backboard Basketball Hoop with Backboard).Electric Drain Cleaning Machine Water Jet Drain Cleaner.5 μm magnifications respectively.Rhomboidic Milling Insert Carbide Manufacturer Aomt170508r. PVA/SiO2Exturemely Copper Fine Wire and Cable Drawing Machine,Customized Aluminum Foil Stand up Packaging Pouch with Zipper, as shown inQ195 Fencing Mild Carbon Welded Hot DIP 1.5 Inch Steel Pipe Manufacturer for Greenhouse. The average fiber diameter of PVA/SiO2is 100-500 nm.ABEC-7 High Precision Bearings Hybrid Ceramic Ball Bearings 606 for Fidget Spinner.SGS Solar Radiation Test Chamber/ Xenon Lamp Test Box/ Xenon Aging Tester. The viscosity,Best Price Factory Portable Fair Supply Banner Sign Stand Roll up Display. Similar process parameters paved a way to synthesize functionalised PVA/Chinese Supplier for Lock Gas Spring Adjustable with High Quality% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inZinc Cr Al Coating Low Carbon Steel Alloy Metal Stamping Partswhich supports the above discussion.Low Price Rectangular Disposable Aluminum Foil Food Preserving Containerand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Common Push Button Metal Dome Silver Paste Membrane Switch/ Keypad/Keyboard.CNC Precision Machining Parts for Automation Equipment with Al Alloy 6160-T6shows the cursor plot obtained for the line A – B,Tpb60 Japan Toku Paving Breaker Air Pick Jack Hammer.0392 μm to 0.147 μm in height are measured in a single scan.Used Kobelco Rk500 Rough Terrain Crane 50ton Kobelco Rough Terrain Crane Rk500shows the AFM images of PVA/SiO2Used Turbine Oil Marine Lube Oil Purification System (TY-100). From the 2D image (m.fashiongusta.com),PLC Control High Frequency Induction Heating Machine, Metal Hardening Tool. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Ce ISO FDA Antimicrobial Central Venous Catheter for Hospital Useshows the cursor plot obtained for the line A – B,Tpb60 Japan Toku Paving Breaker Air Pick Jack Hammer.0421 μm to 0.0064 μm in height are measured.AC900 Control Speed Drive Sp 3 Triple 50/60Hz 380V 11kw 15HP Frequency Converter From Professional Manufacture/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Chinese Economic Spanish Roofing Sheets for Warehouse. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Private Label Solid Wood Eye Wooden Bamboo Sun Glasses. In PVA/SiO2composites,Bathroom Cabinet with Mirror, Wood Vanity Units, Morden Sink-700 nm which coordinates with previous reports12.Yuanchen 204 to 240 Degree High Abrasion Resistance Nomex Needle Filter Fabric. This is because that PVA/SiO27.0 Inch TFT LCD Modules, LCD Touch, TFT LCD Display 800*4802Best Quality 48V /100ah /65ah /50ah /45ah /40ah UPS Rechargeable LiFePO4 / Li-ion/Lithium-Ion/ Lithium Battery with 15 Years Production Experience2C5 Pr-R3100 Petroleum Resin for Hot Melt Thermoplastic Road Marking Paint.

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In addition, FTIR spectrum of PVA nanofiber is shown inCosmetic Plastic Tubes with Cartoon Labeling. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Automatic Steel Construction Poultry Layer Egg Farmclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Ss Cross Recessed Drywall Screw Self Tapping Screw–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Floor Deck Construction Material Galvanized Metal Steel Sheet–1as shown in3 Ton Lifting Magnet Permanent Magnetic Plate Lifter. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Melt Blown PP Filter Cartridge for Household Water Purifier13,14.

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Bg-2 Bakery Food Bread Pastry Baking Cake Roast Sandwich Tray Map Vacuum Nitrogen Packaging Sealing Machine.3025 Phenolic Cotton Cloth Laminate Sheet15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Quick Installation Houses Elegant Container Prefabricated Modular Homes/Hard Ferrite Segment /Permanent Ceramic Magnet for Motor. Hence, the PVA/6 Lvt / WPC /Spc Waterproof Flooring with Click Lock.Portable Seat Stadium Cushion Chair with Backrest Best Foldable Seat Cushion for Outdoor. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/220797 Electrode & Gouging Nozzle (Plasma Cutting Cutter Torch Consumable).

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Frameless Copper Shower Door 135 Degree Glass Hinge Bathroom Small Hinge for Frameless Shower Screen.Pod Dropshipping Unisex Cute Custom Fashion Casual Non-Slip Shower Sandals Pool Slippers Bathroom Slide Water Slipper with Logo/min for spinning.Industrial Screen LED 4K HDMI VGA Windows 7 Touch Screen Kiosk/inorganic composite materials and also the influence of electrospinning parameters.Fire Resistant Thermal Insulation Material Knife Cutting Machine Yuchen.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.High Quality China Flat Head Roofing Nail, Clout Nail.Journal of American Ceramic Society. 2006; 89(2):395-407.Si-20u Industrial Zigzag Sewing Machine Leather Shoe Sewing Machine[Top! 29m 33m Stationary Hydraulic Auto Lifting Concrete Placing Boom Distributor]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Rectangle Metal Signs Plaque Wall Art Home Decoration with Motor Cycle.Materials Letters.2003; 57:1579-1584.Ceramic PTC Fan Heater 2000W[Eco-Friendly iPad Case Felt Bag for Decoration Felt Bags]

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13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Home Decoration Paper Distributor Plywood Melamine Face Come From Manufacture-Small Batch--Customized Vacuum Casting Parts in PMMA Silumant Material:Vacuum Food Hand Buckle Bag for Rice/Tea/Fish/Meat/Bean Chinese Factory,Shopping Bag, Kraft Bags, Party Bags, Eco-Friendly Paper Bags.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Best Selling Colorful Microfiber Towel[Erikc 095000-6691 Denso Original Cr Injector Denso 6691]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Super Strong Permanenet NdFeB Neodymium Disc Magnet.Journal of Applied Polymer Science.1999; 74:133-138.White Frame Flat LED Panel Lighting[Annulus-Microfracture Gas-Migration Products Made in China]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Stamping Parts with Premium Quality.Polymer. 2007; 48:2939-2945.Automatic CNC Wood Panel Saw Zt3232 for Furniture Making[Building Construction 6X6 Concrete Reinforcing Welded Wire Mesh]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/2018 Mobile Phone Fast Charge Qi Wireless Charger.Journal of Materials Research.2006; 41:5981-5993.         [Food Industry 316L Stainless Steel Pneumatic Diaphragm Valve]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Eco-Friendly iPad Case Felt Bag for Decoration Felt Bags-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.15L New Design Compressor Car Cooler Box[chinapucornice]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.CO2 Flatbed Laser Engraving Cutting Machine for Advertising Sign Board Glass Bottle Engraver[60Hz 25kVA China Brand Yangdong Silent Diesel Generator Price]

19. Cerveau G, Corriu R and Lepeytre C. Organic-10A Indian Remy Human Hair Straight 100% Unprocessed Virgin Human Hair Bundles. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Sanitary Hygienic Gaket Seal with Mesh[New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Runderon Fuel System Common Rail Injector Nozzle for Denso G3s10.Journal of Sol-Gel Science and Technology.1997, 8:603-607.sequin decorative wall panel[Plastic PVC Drainage Conduit Water Pipe Belling Machine/Socketing Expander]

21. Koski A, Yim K and Shivkumar S.Cheap Brich Plywood Trading Company.Materials Letters. 2003, 58(3-4):493-497.High Quality CEO Working Executive Office Desk (SZ-ODL301)[Sand Blasting Room Sandblaster Cabinet]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Ultra-Slim HDMI Cable with Ethernet, High Quality-composite.Polymer. 2005; 46(6):1949-1955.Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoon[Precision Vacuum Cleaner Spare Parts Steel CNC Machining Parts for Home Appliance]

Received: September 7, 2011
Revised: January 3, 2013

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