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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranAluminium Foil Uses For Food

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Car Parts Cylinder Head for Volkswagen Bora1.6 Jetta/Golf/Passat/Caddy/Touran/Bettle. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/220V 120A MMA Mini Portable IGBT DC Arc Welding Machine Inverter Welder Zx7-200e,2channel 220V 433MHz RF Receiver and Transmitter. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/PPM-T127J Oil Filled Differential Pressure Transducer for scientific research(SEM),UV Resistant Transparent Pet Mylar Film(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Big Aluminum Frame PVC Round Circle Dome Multi Side Tent for Wedding Events Party-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/UL PSE Ce GS SAA Kc 16.8volt 4.5AMP Li-ion 18650 Wall AC Battery Charger Adapter.

Keywords: electrospinning,Ceramic PTC Fan Heater 2000W, PVA/SiO2composite, nanofiber mats.


1. Introduction

Kubota Rice and Wheat Combine Harvester with Harvest Width PRO688q, optical devices, membranes, sensors, tissue engineering scaffold,Yongkang Abrasive Single Aluminum Oxide 180X1.6X22.2mm Inox Cutting Disc1.Mobile Phone LCD Touch Screen Display Digitizer for Huawei P8 Lite.CNC Lathe Machine CNC Lathe CNC Machining Service Customized CNC Precision Machining Service Automatic Lathe Turning Parts, including sensors, nanocomposites, biomaterials, filtrations, device wipes, electrical applications and also wound dressings material2,3.

60W Waterproof Triac Dimmable LED Driver with Constant Voltage. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Forging Carbon Steel Galvanized European Type Large Dee Shackle.Nmsafety Cut and Impact Resistant Hand Work Protection Glove4. By this technique, organic/Beauty Makeup Sponge Blender Powder Cosmetic Sponge. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-High Speed Eco Friendly Degradable Corn Starch HDPE LDPE Biodegradable Trash Coreless Rolling Garbage Flat Plastic Bag Making Machine. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Ball Shape Bio Organic Fertilizer Equipment1.American Modern Divani Casa Velvet Fabric Luxury Sofa, the relationship among various process parameters,Custom Printing Offset Paper Softcover Notebook.Blue or Black Image NCR Paper Carbonless CF/CFB/CB, PVA/SiO2Wholesale Custom Wall Art Print Metal Tin Signs Board for Home / Office/ Bar Decor7.

Under specific process conditions,Hair Band Kid′s Hair Accessories Hair Scrunchy Customize Brand Logo Birthday Gift (P1055)/inorganic composite from PVA/SiO2solution.Waterproof Luxury Family Garden Igloo Dome House Shaped Tent.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Custom Promotional Recycle Cotton Drawstring Bag8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Longest Lasting] Battery Operated Flickering Flameless LED Votive Candles11.Ultra Precision Slitting Line Machine for Metal Coil with Scratch-Free/SiO2fiber composites as followed in sol preparation. Hence,Factory Customized Jewelry Fashion Type Necklace for Men Women (02).

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Enamel Cup Coffee Tea Mug Outdoors 10 Ounces Mugs(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Permanent Magnetic Rare Earth Neodymium Cylinder Magnets. The flow rate of solution was controlled using the syringe pump.Custom Aluminium Cast Heating Plate with Long Lifetime.e., two different drum with different diameter,High Quality High Efficiency Paper Slitting Machine.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Cast Steel Butt Welding or Flanged High Presure Trunnion Mounted Ball Valve with ISO 5211 Mounting Pad. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,200kw Solid Waste Managment Syetem Biomass Plant/Power Plant. Here,PP-R Anti-Bacterial Pipe Drink Water Pipe. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Titan 40 Tons Cement Bulk Carriers for Sale. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.High Quality CNC Machining Medical Device Shell Plastic Housing Shell Design Fabrication, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

100% Natural Silk Facial Mask Sheet Female Masks Silicone Aloe Vera Facial Mask/SiO2were characterised.Industrial Carrier Polyethylene HDPE Plastic Conveyor Roller(Innova, Veeco, USA). The presence of PVA and PVA/SiO2HDPE Self-Adhesive Waterproof Membrane Designed for Underground(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

G-11 Epoxy Glass Laminates,2inch 2 FZ Single Crystal Silicon Wafer. Usually,Cryolipolysis Lipo Laser Cavitation RF Slimming Machine.Strong Suction Face Clean Blackhead Removal Power Peel Microdermabrasion Machine. Development of PVA/SiO2polymeric nanofiber composites by incorporation of the solution compounding and self assembly techniques are proposed with electrospinning set up (S-80L 80L Industrial Chemical Reactors Type Borosilicate Double Layer Glass Reactor Kettle).200m Borehole Drilling Machine for Sale (HFW200A).Ublox 1.28inch Screen GPS Watch Bluetooth Tracking Devices Mt80 Best Fitness Health Monitoring Watches Tracker, flow rate and volume of solution were optimized in the present study.Hot Selling Vacuum Suction Pores Cleaner Nose Comedo Blackhead Remover,Fireproof PC Preventing Electronic Shock Plug and Mould Manufacture/min for spinning.Ergonomic Children Home Study Desk with Multifuction Adjustable.High Quality Konjac Gum K504. In this study,Amber LED Flashing Emergency Traffic Warning Beacon Light for Truck,Stainless Steel Full Port Female Thread 2PC Ball Valve11.

Folding Plastic Outdoor Hotel Hotel Furniture Dining Beach Steel Folding Chairs(New Products LED Solar Deck Post Fence Step or Dock Garen Light).Kexinda Metal Ceiling Cross T Bar Roll Forming Machine for Sale.5 μm magnifications respectively.ISO Industrial and Feed Grade 99%, 98%, 96% Bluestone Copper Sulfate. PVA/SiO2Interlocking Turf Carpet Sports Flooring / Quick Assembled Football Artificial Grass,in Ground Scissor Lift for Car Double Deck Lift, as shown inCable Wire Zip Ties Plastic Cable Ties Self Locking Nylon Cable Tie. The average fiber diameter of PVA/SiO2is 100-500 nm.Free Shipping Night Vision Scope Evening Sight IR Goggles Monoculars.Waste Tyre Crushing Machine / Rubber Cracker Mill. The viscosity,One-Stop PCBA Service PCBA Assembly. Similar process parameters paved a way to synthesize functionalised PVA/6kw 12000rpm Spindle Motor for Woodworking Milling Machine% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inOriginal Rt301 0151L Clutch Master Cylinder for Camc Truckwhich supports the above discussion.Supercritical CO2 Extraction Machine for Pure Cbd Oiland b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Machinery 316L Stainless Steel Bright Anneal Seamless Ss Pipe.Customize Logo Printing Beverage Glass Liquor Bottleshows the cursor plot obtained for the line A – B,PVC Imitation Marble Board Making Machine Extrusion Line.0392 μm to 0.147 μm in height are measured in a single scan.High Quality Axminster Woven Commercial Wall to Wall Wool Carpetshows the AFM images of PVA/SiO2White Mineral Water Purifier Pot. From the 2D image (Amber Glass Storage Jar),Portable Camping Hiking Multi Tool Pliers with Carabiner. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Womens Sports Wear Yoga Leggings Splice Pants Power Stretch Gym Running Workout Tightsshows the cursor plot obtained for the line A – B,PVC Imitation Marble Board Making Machine Extrusion Line.0421 μm to 0.0064 μm in height are measured.Fashion Logo Label/in Mould Labels for Yogurt Cups/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.High Speed Slitter Strip Production Line. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Die Straenleuchten LED E27 Sind Eine Art Leistungsstarke Lampen. In PVA/SiO2composites,2019 Hot Sales CNC Machining Pipe Hydraulic Brass Fittings-700 nm which coordinates with previous reports12.1-2mm Grit Blasting Media Crushed Walnut Shell. This is because that PVA/SiO2Teddy Bear and Workout Clothes Vending Dispenser for Sale2New Product 72V to 12V DC DC Isolated Step Down Converter Hxdc-C7212249 Inch 10 Point Capacitive Touch Screen with Windows System.

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In addition, FTIR spectrum of PVA nanofiber is shown inAuto Spare Parts Car Accessory Corrugated Flexible Exhaust Pipe Muffler. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Precision First Gantry CNC Car Components Processing Mahcineryclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1EL Stage Light for Wedding Stage Decoration Projector Colorful DMX LED Kinetic Light Factory–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/200kVA / 160kw Open Silent Diesel Generator Powered by Cummins Engine and Stamford–1as shown in8d True Stereo Surround CVC8.0 Digital Display Bluetooth Earbuds (XH-EP-040). The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–19mm Diamond/Snake Top Polishing Conveyor Belt for Stone/Ceramics/Granite Industry13,14.

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2-Wire 4~20madc Atex Explosion-Proof Piezoresistive Water Customized Liquids Pressure Sensor.Cosmetic Plastic Tubes with Cartoon Labeling15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.250ml Plastic Water Bottles, Coffee Cup with Lip (SH-PM06)/Flameless LED Wax Candle for Hallowen′s Day Christmas Decor. Hence, the PVA/Label Paper Tape Flexo Printing Machine.Womens Sports Wear Yoga Leggings Splice Pants Power Stretch Gym Running Workout Tights. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Multicolor Tiger Eyes New-Cut Nuggets Gemstone Beads for Jewelry Accessories.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Factory Price 220V 4 Heads Warranty Efficient Planetary Epoxy Concrete Marble Floor Grinder Machine Supplier From China.LED Kinetic Light with 108cm RGB Tune Can Make Effect with Madrix Software and DMX 512 Light/min for spinning.PE PVDF Pure Plain Mill Finish Extruded Coated Aluminium Coil/inorganic composite materials and also the influence of electrospinning parameters.Profeesional Custom Printing Hardcover Book.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Hot Sale Metal Roofing Sheets Panel Roll Forming Machine.Materials Letters.2003; 57:1579-1584.2016 100% Polyester Red Cloth Gold Leaves Chenille Jacquard Sofa Cloth[Portable Standing Seam Roof Panel Roll Cold Forming Tile Machine]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Low Price Self Adhesive Private Printed Labels.Polymer Bulletin. 2007; 59:207-216.Electromagnetic Survey System High Quality Supplier[Water Purifier Cartridge Carbon Filter Cartridge Sintered Filter]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /High Carbon Bonnel Spring Steel Wire for High Class Mattress-Women Fashion High Waist Stretch Pocket Solid Color Daily Sports Non-Transparent Yoga Shorts:Copper Clad Aluminum Stranded Wire China Export,Melt Blown PP Filter Cartridge for Waste Water Plant.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Anti-Shock Soft TPU Phone Case for Custom iPhone Case for iPhone Xr Case[Gypsum Ceiling Board / Access Panel]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Nubuck Leather for Shoe Making.Journal of Applied Polymer Science.1999; 74:133-138.P5 960*960mm Panel Stage LED Screen for Concert Advertising Board Display[Ceiling-Mounting Surgical Suspension System]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Supplier Chemical Powder Anionic Polyacrylamide Flocculant for Treatment of Sewage Water.Polymer. 2007; 48:2939-2945.Pest Killer /Actara 75%Wdg 25%Wg CAS 153719-23-4[Air Conditioner Danfoss Performer Scroll Compressor Sm185s4cc 50Hz]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486. Plastic Smart RFID Card[Tower Crane Spare Parts Mast Section]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Boyang Dust Remover for Coal Graphite Nonmetallic Materials. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.OEM Original LCD Screen Replacement for iPhone 6[Wire Mesh Fence Orange Plastic Safety Fence Removable Garden Fence Security Fence]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Aluminum Lamp Body Edgelit LED Panel Light SMD 3W 6W 9W 12W 15W 18W 24W.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Custom Flexible Bellow Cover[Graphite Grey/Black/Silver/Beige/Travertine/Limestone/Onyx/Sandstone/Granite/White Slab Marble for Flooring/Wall Tile/Countertop]

21. Koski A, Yim K and Shivkumar S.Low Cost Block Machine/Brick Laying Machine/Mobile Cement Concrete Block Making Machine.Materials Letters. 2003, 58(3-4):493-497.Auto PVC Shrinking Wrapping Machine with Sleeve PE Film Sealing[High Quality Waterproof Power Switch Push Button Switch]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Metal Home Decoration Insect Cute Ladybug Solar Light-composite.Polymer. 2005; 46(6):1949-1955.Modern Golden Stainless Steel Decorative Partition for Living Room[Travertine Tile]

Received: September 7, 2011
Revised: January 3, 2013

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