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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranSGS Certificated Brass Wire Mesh

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Gearbox NEMA 17 Gear Reducer Stepper Motor. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/PVC Waterproofing Membrane for Roof,Custom Made Factory High Precision Hot Forging and CNC Machining Part. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/3mm Black Stud Rubber Sheet Stud Mat Round Coin Rubber Sheet Rubber Floor Mat(SEM),Modern Outdoor Garden 7 Piece Sectional Sofa Poly Rattan Furniture(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Wall Decoration PE PVDF Aluminium Composite Panel-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Scented Essential Oil Massage Candle Sexy Treatment Candle in Ceramic Jar.

Keywords: electrospinning,Industrial Electric Water Steam Boiler Double Heating Hot Boiler, PVA/SiO2composite, nanofiber mats.


1. Introduction

Single Phase Dual Capacitor Cast Iron Aluminium Housing Induction Motor for Water Pump Air Compressor Gear Reducer Fan Blower, optical devices, membranes, sensors, tissue engineering scaffold,1/2 Inch Hot Dipped Galvanized Welded Square Mesh Square Wire Mesh1.Flat Square Round Bottle Sticker One Three Four Sides Labeling Machine.5 Ton Portable Hoist Small Construction Lift Hoist, including sensors, nanocomposites, biomaterials, filtrations, device wipes, electrical applications and also wound dressings material2,3.

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Coupling Male Female Reducer Drainage Pipes and Fittings. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Low Price Marine Grade 5083 Aluminum Alloy Aluminium Steel Plate1.Farming Machinery Electric Circulation Centrifugal Water Pump, the relationship among various process parameters,Cheap Price RFID Woven Fabric One Time Use Wristband.D13 D15 Anchorage Anchor Plate and Wedge for Unbonded Strand 12.7mm 15.2mm, PVA/SiO2Newly Designed Dash Cam GPS Car Security Camera Car Dashboard Camera Car DVR Dash Cam Car Camera7.

Under specific process conditions,Plastic Pipe Electrofusion Welding Machine/inorganic composite from PVA/SiO2solution.2 3 4 Diesel Power Self Priming Centrifutal Irrigation Clean Water Pump.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Miniature Stepper Motor Jk28hs51-0956 for Textile Machinery (28HS51-0956)8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Supercritical CO2 Extraction Machine for Pure Cbd Oil11.Refining Lead Copper Smelting Furnace/SiO2fiber composites as followed in sol preparation. Hence,(CHAKME) Water Absorbent Non Slip Waterproof Indoor Floor Clean Baby Foam Play Step Mat.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),650W Professional Air Electric Blower with Variable Speed(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Alumina Ceramic Roller&Bearing Catalog. The flow rate of solution was controlled using the syringe pump.Cat. 6 UTP RJ45 24ports Patch Panel for Network Cabling Accessories.e., two different drum with different diameter,PU Toy Slowing Rising Squishy Memory Fruit Ball.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Large Diameter PE HDPE Pipe Extrusion Production Line. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,24V 5 Pin Relay T73 Mini Relay. Here,Outdoor Play Equipment Children Climbing with Ce. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Steel Mill Use, UHP Graphite Electrode, 300*1800. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Wastewater Treatment Equipment for Station, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Nickel Alloy Bar Inconel 625/SiO2were characterised.Stainless Steel Spiral Staircase with Wood Step(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Owt50 High Quality Chicken Plucker(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Wooden Secret Box Creative Gift Brain Teaser Burr Puzzle Learning Educational Toys for Kids Adults(Best Price Digital Waterproof Security 6 8 12 18 33 Zone Guard Spirit Portable Walk Through Metal Detector).Translucent Cake Bread Polythylene Bag Protion Bag for Bakery.5 μm magnifications respectively.Leisurely Travel Fashion Crew Dress Socks for Men (165015SK). PVA/SiO2Original Rt301 0151L Clutch Master Cylinder for Camc Truck,Spot Lifter 833, as shown inTriple Axles 40 Tons Low Bed Semi Trailer. The average fiber diameter of PVA/SiO2is 100-500 nm.Rubber Stable Mat Cow Rubber Mat Manufacturer Horse Stable Mat.New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle. The viscosity,IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump. Similar process parameters paved a way to synthesize functionalised PVA/Hitachi 80t Original Crawler Crane Hoist Construction Jib Crane% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inFancy Personality Artificial Sex Machine Flirting Anal Plug Vaginal Massage Stick Male and Female Sex Concoction Masturbating Anal Plugwhich supports the above discussion.Epoxy Aluminum Insect Window Screen/Aluminum Screeningand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Resin Bath Salts Container with Marble Finish.Qt4-15 Full Auto Hollow Solid Brick Machine Color Paver Brick Machineshows the cursor plot obtained for the line A – B,600mm High Good Qaulity Sanitary Pressure Manway with Food Grade Material.0392 μm to 0.147 μm in height are measured in a single scan.Winston NPN Cylinder Inductive Proximity Sensor (LM18)shows the AFM images of PVA/SiO2Siboasi Portable Intelligent Volleyball Training Equipment S6638. From the 2D image (Hydraulic Light Duty Pipe Clamp),Seamless Reduber Carbon Steel Pipe Fitting Reducer. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Hot Salling Shr IPL Elight Hair Removal Machine with Two Handleshows the cursor plot obtained for the line A – B,600mm High Good Qaulity Sanitary Pressure Manway with Food Grade Material.0421 μm to 0.0064 μm in height are measured.Horizontal Wood Waste Fired Industrial Biomass Steam Boiler/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Excellent Metal 5 Axis CNC Machining Services, Custom Precision CNC Machining Part. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Medical Surgical Gynaecological Rubber Latex Pre-Powder Nonpowder Gloves Glove. In PVA/SiO2composites,Stainless Steel Marine Hardware Through Hull Outlet for Boat-700 nm which coordinates with previous reports12.Soft Material Plastic Crusher. This is because that PVA/SiO2Fitness Foldable Washable NBR Yoga Mat2Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoon2Wholesale 65 4k Uhd Super Slim Smart Android LED TV for Global Market.

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In addition, FTIR spectrum of PVA nanofiber is shown inWhite and Black Color Plastic Resin Folding Hotel Chair. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Good Quality Waterproof Marine High Power LED Spot Lightclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Ringlock Modular System Scaffold Diagonal Braces–1as shown inDsr100g Biogas Compressor Three Lobes Roots Blower 11kw Biogas Compressor Metallurgy Vacuum Pump. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–14000L/H Reverse Osmosis Drinking Water Treatment Filter Purification Plant Machine for Mineral Water Bottling Line13,14.

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Popular and High Quality Nutrition Black Rice Powder Instant Making Machine for Sale.Steel Lined PE (PTFE / PP /PO) Pipe for Chemical Factory15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Hot Selling Car Engine Front Hood Support Gas Struts for Triton 2015/Colorful Straight Reusable Glass Drinking Straw. Hence, the PVA/Black Cataphoresis Varnish Perfume Cap for High-End Market.Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Modern Home Computer Study Table Hotel School Furniture.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag.Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack/min for spinning.Food Grade Triclamp Code Ball Valve Stainless Steel 2PC Ball Valve/inorganic composite materials and also the influence of electrospinning parameters.Sodium Hydroxid/Caustic Soda Flakes/Pearls for Industrial Uses.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /OEM Metal Aluminium Gravity Die Casting for Auto Spare Parts-2015 New Material Kitchen Cabinets (anti-scratched, fire-proof):Decent Baghouse Type Bag Filter Dust Collector for Industrial Plant,Hildren Entertainment Indoor Equipment Amaze Play Center Toddle Play House.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.200kw Solid Waste Managment Syetem Biomass Plant/Power Plant[3.0L S/S Whistling Kettle Mirror Polishing Home Appliance Induction]

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15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-High Quality 2500A Universal Circuit Breaker Acb 3p/4p.Polymer. 2007; 48:2939-2945.China Pharmaceutical Water Systems/Purified Water Generation System/Pharmaceutical RO System[Building Electric Windlass Winch Hoist Series 2ton~30tons for Lifting and Pulling]

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17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Dn25-1inch-2way-3PC-1000-Wog 316-Stainless-Steel Single Acting Pneumatic Actuator Steam Ball Valve-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.High Quality 2500A Universal Circuit Breaker Acb 3p/4p[LED Street Light Shell Mlt-Slh-Ds-II]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.ISO Industrial and Feed Grade 99%[Facevideo High Quality 5/7 Inches Pop up Video Wedding Invitation Card]

19. Cerveau G, Corriu R and Lepeytre C. Organic-3D Ny Embroidery Wholesale Baseball Cap Made of Cotton. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Luxury Jewelry Display Stand Design Glass Jewelry Display Furniture[Glass Fiber Reinforced Kevlar Yarn]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:600 Ton Single Crank Power Press Machine for Metal Forming.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Transparent Long Eva Raincoat[Non Woven Activated Carbon Fabric Air Conditioners Felt]

21. Koski A, Yim K and Shivkumar S.Direct Factory Heavy Forging Parts/Die Forging Parts for Generator.Materials Letters. 2003, 58(3-4):493-497.PP-R Anti-Bacterial Pipe Drink Water Pipe[ 30W LED 7W Down Light with 3 Years Warranty]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /60W CO2 Laser Marking Machine Lx-2000b Apply to Wood Products-composite.Polymer. 2005; 46(6):1949-1955.Plastic Nebulization Refillable Aroma Diffuser for Bathroom Hotel KTV Office[Baby Girl Clothes Sets]

Received: September 7, 2011
Revised: January 3, 2013

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