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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. Rajendran1.5 Inch Polyethylene Pipe

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Plastic Pipe Electrofusion Welding Machine. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/2 3 4 Diesel Power Self Priming Centrifutal Irrigation Clean Water Pump,Miniature Stepper Motor Jk28hs51-0956 for Textile Machinery (28HS51-0956). The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Supercritical CO2 Extraction Machine for Pure Cbd Oil(SEM),Refining Lead Copper Smelting Furnace(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,(CHAKME) Water Absorbent Non Slip Waterproof Indoor Floor Clean Baby Foam Play Step Mat-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Hot Sales Polyester PE Filter Cartridge Suppliers.

Keywords: electrospinning,650W Professional Air Electric Blower with Variable Speed, PVA/SiO2composite, nanofiber mats.


1. Introduction

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24V 5 Pin Relay T73 Mini Relay. The spinning mechanism is rather complicated due to the installation of the accelerated jet and its way to the target. It contains three basic components such as syringe pump,Outdoor Play Equipment Children Climbing with Ce.Steel Mill Use, UHP Graphite Electrode, 300*18004. By this technique, organic/Wastewater Treatment Equipment for Station. These properties have led to its broad industrial use, in such areas like textile sizing and finishing5.

Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-Nickel Alloy Bar Inconel 625. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Stainless Steel Spiral Staircase with Wood Step1.Owt50 High Quality Chicken Plucker, the relationship among various process parameters,Stainless Steel Seamless Pipe, ASTM A312 Tp310, Tp310s, Tp310h, for High Temperature Applicaition.Professional Stadium Outdoor Projector 100W/150W/200W/250W/300W/400W/500W/600W/800W/1000W LED Flood Light for Street High Mast Crane Tower, PVA/SiO2Field Fence Wire Barb Wire Fence Tools Fence with Barbed Wire7.

Under specific process conditions,High Frequency Electrosurgical Unit Bovie Electrosurgical Unit/inorganic composite from PVA/SiO2solution.Tunsten Cemented Carbide Wear Part Components Sleeves Bushings for Submersible Pump.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,1200 Rounds Per Minute Dental Casting Machine Xf1008,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Most Popular Long Service Life Basketball Courts Flooring/Basketball Gym Floor11.Composite PP Non-Woven Roofing Breathable Waterproof Membrane/SiO2fiber composites as followed in sol preparation. Hence,Decoration Exhibition Fashion Digital Printing Knitted Football Fans Bandana Scarf.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Customized PVC Ceiling Board Panel Making Machine(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Ductile Iron Single Orifice Air Release Valve. The flow rate of solution was controlled using the syringe pump.Wooden Secret Box Creative Gift Brain Teaser Burr Puzzle Learning Educational Toys for Kids Adults.e., two different drum with different diameter,Translucent Cake Bread Polythylene Bag Protion Bag for Bakery.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Leisurely Travel Fashion Crew Dress Socks for Men (165015SK). Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Original Rt301 0151L Clutch Master Cylinder for Camc Truck. Here,Spot Lifter 833. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Rubber Stable Mat Cow Rubber Mat Manufacturer Horse Stable Mat. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.New Creative Borosilicate Pyrex Glass Mouse Shape Wine Bottle, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

IMD40 Fluorine Plastic Acid Alkali Resistant Horizontal Chemical and Insustrial Magnetic Drive Pump/SiO2were characterised.Hitachi 80t Original Crawler Crane Hoist Construction Jib Crane(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Resin Bath Salts Container with Marble Finish(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

600mm High Good Qaulity Sanitary Pressure Manway with Food Grade Material,Siboasi Portable Intelligent Volleyball Training Equipment S6638. Usually,Seamless Reduber Carbon Steel Pipe Fitting Reducer.Horizontal Wood Waste Fired Industrial Biomass Steam Boiler. Development of PVA/SiO2polymeric nanofiber composites by incorporation of the solution compounding and self assembly techniques are proposed with electrospinning set up (Electric Handling Vehicle with Steel Frame on Railways (KPX-40T)).Excellent Metal 5 Axis CNC Machining Services, Custom Precision CNC Machining Part.Medical Surgical Gynaecological Rubber Latex Pre-Powder Nonpowder Gloves Glove, flow rate and volume of solution were optimized in the present study.Stainless Steel Marine Hardware Through Hull Outlet for Boat,Soft Material Plastic Crusher/min for spinning.Fitness Foldable Washable NBR Yoga Mat.Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoon. In this study,Wholesale 65 4k Uhd Super Slim Smart Android LED TV for Global Market,High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration11.

Ringlock Modular System Scaffold Diagonal Braces(G-11 Epoxy Glass Laminates).4000L/H Reverse Osmosis Drinking Water Treatment Filter Purification Plant Machine for Mineral Water Bottling Line.5 μm magnifications respectively.Popular and High Quality Nutrition Black Rice Powder Instant Making Machine for Sale. PVA/SiO2Steel Lined PE (PTFE / PP /PO) Pipe for Chemical Factory,Hot Selling Car Engine Front Hood Support Gas Struts for Triton 2015, as shown inCast Steel Butt Welding or Flanged High Presure Trunnion Mounted Ball Valve with ISO 5211 Mounting Pad. The average fiber diameter of PVA/SiO2is 100-500 nm.Colorful Straight Reusable Glass Drinking Straw.Black Cataphoresis Varnish Perfume Cap for High-End Market. The viscosity,Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag. Similar process parameters paved a way to synthesize functionalised PVA/Modern Home Computer Study Table Hotel School Furniture% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inTeddy Bear and Workout Clothes Vending Dispenser for Salewhich supports the above discussion.Men′s and Women′s Wear Printing Logo Custom Tshirt Printingand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag.Disposable Cutlery Material Bio-Degradable PLA Sheetshows the cursor plot obtained for the line A – B,Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack.0392 μm to 0.147 μm in height are measured in a single scan.Rechargeable Li-ion Battery Cordless Drill Drill Machines and Cutting Machines Electric Hand Tools Cordless Hammer Drillshows the AFM images of PVA/SiO2Food Grade Triclamp Code Ball Valve Stainless Steel 2PC Ball Valve. From the 2D image (Guangzhou Keychain Making Supplies Leather Keychain),Sodium Hydroxid/Caustic Soda Flakes/Pearls for Industrial Uses. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Tayor CNC Plasma Cutting Machine Table with High Definition Plasma Cuttingshows the cursor plot obtained for the line A – B,Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack.0421 μm to 0.0064 μm in height are measured.Sandblasting Abrasives Media Glass Beads for Surface Preparation/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Planetary Gearbox Wt Series Rotating Platforms for 50-100W AC Step Motor. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Low Porosity Fireclay Bricks Lpfb01. In PVA/SiO2composites,Custom Silicone Rubber Bushing silent Block for Medical Part-700 nm which coordinates with previous reports12.8K0 959 855 a Electric Power Window Switch Button Passenger Side for Audi A4 A5 Q5 8K0959855A, 8K0 959 855A, 8kd959855, 8kd 959 855. This is because that PVA/SiO2OEM Metal Aluminium Gravity Die Casting for Auto Spare Parts22015 New Material Kitchen Cabinets (anti-scratched, fire-proof)2Decent Baghouse Type Bag Filter Dust Collector for Industrial Plant.

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CITROEN

In addition, FTIR spectrum of PVA nanofiber is shown inDn25-1inch-2way-3PC-1000-Wog 316-Stainless-Steel Single Acting Pneumatic Actuator Steam Ball Valve. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Syntec Heavy Duty Lathe Machine CNC Lathes with Slant Bedclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Hildren Entertainment Indoor Equipment Amaze Play Center Toddle Play House–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Actpto Audio Line Array System Column Speaker Active Modular Line Array Speaker–1as shown inWoodworking Electric Edge Trimming Machine with PVC Edge Trimmer Knife Set. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1High Quality 2500A Universal Circuit Breaker Acb 3p/4p13,14.

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Wood Chipper Log Splitter.Dn25-1inch-2way-3PC-1000-Wog 316-Stainless-Steel Single Acting Pneumatic Actuator Steam Ball Valve15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.3D Ny Embroidery Wholesale Baseball Cap Made of Cotton/600 Ton Single Crank Power Press Machine for Metal Forming. Hence, the PVA/Direct Factory Heavy Forging Parts/Die Forging Parts for Generator.60W CO2 Laser Marking Machine Lx-2000b Apply to Wood Products. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Top Manufacturing for Sand Blasting Booth/Sand Blasting Room.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Forged Lashing D Ring with Bolt and Bracket.1.2 mm Diameter Welded Wire Mesh 1 X 1 Inch Hole for Chicken Cage/min for spinning.Heat Radiation Aluminum Shell of LED Lamp Shell Aluminum CNC Parts CNC Precision Machining Aluminum Alloy Cooling Parts CNC Machining Parts/inorganic composite materials and also the influence of electrospinning parameters.OEM Original LCD Screen Replacement for iPhone 6.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Outdoor Ipx7 Waterproof Mini Pen Torch Light with Clip.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.OEM Lost Wax Casting for SS316 Marine Anchor[High Quality Plastic Injection Parts Secondary Processing of Electronic Plastic Parts]

8. Huang Z-M, Zhang Y-Z, Kotaki M and Ramakrishna S. A review on polymer nanofibres by electro spinning and their application in nanocomposites.Composites Science and Technology.2003; 63:2223-2253.Motorcycle Ignition Handle Switch Key Lock Sets for Honda/Suzuki/YAMAHA/Bajaj Motorcycles[Used Turbine Oil Marine Lube Oil Purification System (TY-100)]

9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Eco-Friendly Promotional Paper Ball Pens with Custom Design.Journal of American Ceramic Society. 2006; 89(2):395-407.Price Yihe Brand Full Set Flooring Board Production Line Full Automatic Equipment of Particle Flooring Board Line Full Set Automatic Plwood Production Machine[3 Flavors Floor Type Commercial Ice Cream Machine for Sale]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /High Quality Brass Glass Door Hinge for Shower Room.Materials Letters.2003; 57:1579-1584.High-Quality Compressionshock Shock Absorber Car Rear Coil Spring for Sunny N16 X5 E53 Red Coilovers Springs Kits[Viton FKM EPDM Rubber O Ring Seal or Flat Rubber O Ring]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Cold Rolled of Stainless Steel Sheet for 316, 316L, 321.Polymer Bulletin. 2007; 59:207-216.dmgstainless[Full Automatic Paper Car Air Freshener Knotting Machine (TL-LY8-U)]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Dh-MW11 UV Lamp Fly Trap Insect Killer Fluorescent Lamp-New Product/Modern/Cheap/Good Quality 50W/80W/100W/120W/150W/200W/300W/400W/500W/600W/1000W/1500W LED High Bay Light:Anti Climb Security Airport Fence with Razor Barbed Wire Top,Women′s Skinny Tight Elastic Sublimation Printed Yoga Pants.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Offfline Type LED PCB Assemble Line with LED Chip Mounter L6 (TORCH)[High Quality PVC Sound Barrier Sheet]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Besen Type 1 Cable Charger EV Wall-Mount 16A 3.5kw.Journal of Applied Polymer Science.1999; 74:133-138.Old Automatic Textile Machinery Installation and Commissioning Minority Clothing Knitting Machine Manufacturer Used Textile Shuttle Loom Machine Price[Coolers Portable Outdoor Box]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Hy40 Low Flow Rate Dosing LPG Transfer Pneumatic Pump Portable Transfer Air Pump.Polymer. 2007; 48:2939-2945.Fuel Oil Gas Steam Generator for Food Sterilization[Beach Inflatable Football Playground Inflatable Soccer Game for Sports and Recreation (AQ1810-8)]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Dreamland European Standard Eco-Friendly Indoor Kids Soft Play for Sale.Journal of Materials Research.2006; 41:5981-5993.         [ABS Safety Padlock Lockout Tagout Kit Form Padlock Manufacturing Company]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/M20-HRB335 Hot Rolled Left Thread Bar for Formwork Tie-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.China A36 Q235B S275 Ss400 Anti-Slip Checkered Ms Carbon Steel Plate[All Kinds of Polyurethane O Ring]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.P20 1.2311 H13 DC53 O1 Sks3 Alloy Tool Steel Flat Bar Die Steel[Fashion Logo Label/in Mould Labels for Yogurt Cups]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Professional Manufacture Vibrating Feeder with Ce. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Customized Size Recycled Clear Food Grade Pet Rigid Sheet for Vacuum Forming Trays[2019 Newest Design French Line Tp Exercise Book]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:186 Diesel Engine Generator Spare Part Aluminum Recoil Starter Assembly.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Cloth Braided Power Cable[FRP Plastic Electrical Manhole Cover Round Plastic Manhole Cover Customized]

21. Koski A, Yim K and Shivkumar S.USP 99.5% Purity Antiparasitic Drugs Ivermectin 70288-86-7.Materials Letters. 2003, 58(3-4):493-497.China Forge Forging CNC Machining Steel Axle/Drive/Transmission Shaft Parts[New Easter Egg Enamel Jewellery Box]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /China High Pressure Hydraulic Oil Cooler with AC Fan-composite.Polymer. 2005; 46(6):1949-1955.Rigid Marine Lifesaving Solas Orange Fast FRP Rescue Boat[Electric Molding Pp Products]

Received: September 7, 2011
Revised: January 3, 2013

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