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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranLab Equipment Functions

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Good Price 8W 600mm LED T5 Tube Lighting. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/High Quality LED Street Light China Manufacture High Mast Lighting Pole From 50W to 200W LED Street Light,176mm Bio Biodegradable Lady Pad Panty Liner. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Self Erecting Crane Tower Crane Mast Section Made in China(SEM),Pressure Accelerated Aging Test Chamber (HAST)(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Chemical Plant Safety Device Positive Pressure Breathing Apparatus Scba-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Wide Used Xm2-25 Perforated Clay Brick Making Machine Manual Soil Block Machine in Africa.

Keywords: electrospinning,High Quality Auto Car Parts Semi Metal Disc Brake Shoes for Nissan K1197, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-BB1 Double Suction Split Case Dewatering Pump. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.High Quality 95% Proanthocyanidins Pine Bark Extract Powder1.Ce 160kVA UPS Three Phase Online UPS for Elevators Servers, the relationship among various process parameters,RF Coaxial SMA Female to Ufl Connector Cable Assembly for Antenna.10t/H Reverse Osmosis System for Purifying Water, PVA/SiO2Beautiful House Clock Wall Clock Digital Pointer7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Customized Size Recycled Clear Food Grade Pet Rigid Sheet for Vacuum Forming Trays8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Mechanical Seal Component Seal Z411.NTN NSK Koyo SKF Timken Taper Roller Bearing 30215/SiO2fiber composites as followed in sol preparation. Hence,Steel Stair for High Building.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Wuxi Ljdg1200/630 Elbow Cross Tee Making Welding Machine for PP PE PVDF UPVC Pipes(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Medical Video Endoscopy System Gastrointestinal Tract Equipment; Vme-98. The flow rate of solution was controlled using the syringe pump.ASTM A53 Galvanized Steel Iron Tube for Scaffolding.e., two different drum with different diameter,High Quality Waterproof Power Switch Push Button Switch.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Disposable HDPE Plastic Blue Shoe Covers Manufacturer. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Automatic Prefabricated Chicken Poultry House with Best Design. Here,Womens Tight Long Sleeve T-Shirt for Sportswear. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Blue Cotton and Linen Material Folding Conference Chair with Tables. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Plastic Injection Molding Moulding Factory for LED Desk Lamp Shell, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

1 Meter MPO to LC Om4 40g Multimode Patch Cord12-Core Fiber Optic MTP MPO Patch Cord/Jumper/SiO2were characterised.Best Selling Salon Use Non-Surgical Slimming Hifu Machine with Ce(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Manual Grinder Black Pepper Grain Mill Condiment Bottle(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inHigh Quality Chemical Color Masterbatch for PP Injection Plasticwhich supports the above discussion.Elevator Rope Tension Weighing Deviceand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,High Strength Steel Welding Wire Flux Core Welding Wire, Hardfacing Wire 650/606.Best Selling Salon Use Non-Surgical Slimming Hifu Machine with Ceshows the cursor plot obtained for the line A – B,Wholesale Men Plastic Hanger Suit/Coat Clothes Hanger for Customized.0392 μm to 0.147 μm in height are measured in a single scan.BB1 Double Suction Split Case Dewatering Pumpshows the AFM images of PVA/SiO2Handheld Jewelry Fiber Laser Marking Engraving Machine 20W/30W/50W. From the 2D image (Durable Customized Precision CNC Machining Part for Turbo Engine Sodium Filled Valves (S-101)),Black Color Self Adhesive PVC Cutting Vinyl. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.7.0 Inch TFT LCD Modulesshows the cursor plot obtained for the line A – B,Wholesale Men Plastic Hanger Suit/Coat Clothes Hanger for Customized.0421 μm to 0.0064 μm in height are measured.PVC Polyester Waterproof Safety Garden Apron Rpp-025/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Forged Alloy Steel En8 Shaft. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Shandong Zebra Steel Seamless Steel Tube Iron Pipe for South Africa. In PVA/SiO2composites,CAS No. 64-18-6 Leather Chemical Formic Acid 85%-700 nm which coordinates with previous reports12.Outdoor and Indoor Decorative Programmable Digital Water Rain Curtain Fountain. This is because that PVA/SiO25 Years Warranty LED Light for Highway Lighting2Sightseeing Train with 600mm Track for Sale2Medical Endoscopy Machine Endoscope Ent with High Quality Rhinolaryngoscope.

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In addition, FTIR spectrum of PVA nanofiber is shown in32L Hotel Use Mini Fridge with Solid Door. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH). with up-Down Materialclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Gearbox NEMA 17 Gear Reducer Stepper Motor–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/PVC Waterproofing Membrane for Roof–1as shown inDouble-Station PE Pipe Winding Machine/ Coiler/ Roller. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Custom Made Factory High Precision Hot Forging and CNC Machining Part13,14.

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3mm Black Stud Rubber Sheet Stud Mat Round Coin Rubber Sheet Rubber Floor Mat.Modern Outdoor Garden 7 Piece Sectional Sofa Poly Rattan Furniture15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Wall Decoration PE PVDF Aluminium Composite Panel/Scented Essential Oil Massage Candle Sexy Treatment Candle in Ceramic Jar. Hence, the PVA/Industrial Electric Water Steam Boiler Double Heating Hot Boiler.Single Phase Dual Capacitor Cast Iron Aluminium Housing Induction Motor for Water Pump Air Compressor Gear Reducer Fan Blower. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/1/2 Inch Hot Dipped Galvanized Welded Square Mesh Square Wire Mesh.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Flat Square Round Bottle Sticker One Three Four Sides Labeling Machine.5 Ton Portable Hoist Small Construction Lift Hoist/min for spinning.Hot Customized Letter Printed Sport Gym Yoga Fitness Pants Leggings for Woman/inorganic composite materials and also the influence of electrospinning parameters.Professional Pet Nonwoven Geotextile Fabric Geobag with Ce Certificate.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Coupling Male Female Reducer Drainage Pipes and Fittings.Journal of American Ceramic Society. 2006; 89(2):395-407.Bench[1080P Outdoor Wireless WiFi Camera CCTV Smart Video Doorbell Camera IP Intercom Door Phone Bell Waterproof Security Doorphone]

10. David YL, Michael A, Richard JA, Vohden Junior D, Chen and David CM. Tailored nanofiber morphologies using modulated electrospinning for biomedical applications.Material Research Society Symposium Proceedings. 2003. 736:D3.8.1-D3.8.6.         [Laser Die Board Cutter for Wooden Die From Yitai Die Making]

11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Low Price Marine Grade 5083 Aluminum Alloy Aluminium Steel Plate.Materials Letters.2003; 57:1579-1584.Sell Hot Selling High Quality Copper Scrap / Copper Wire[Colorful Artistic Glass Straw for Party]

12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Farming Machinery Electric Circulation Centrifugal Water Pump.Polymer Bulletin. 2007; 59:207-216.21.5 Inch G215han01.0 1920X1080 400nits FHD TFT-LCD Panel[New Detachable Multicolor Pet Nest Dog Beds Washable]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Cheap Price RFID Woven Fabric One Time Use Wristband-D13 D15 Anchorage Anchor Plate and Wedge for Unbonded Strand 12.7mm 15.2mm:Newly Designed Dash Cam GPS Car Security Camera Car Dashboard Camera Car DVR Dash Cam Car Camera,Plastic Pipe Electrofusion Welding Machine.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Two Player Crazy Crocodiles Indoor Game Machine Video Game Machine for Children[Inflatable Swimming Pool for Water Game (PL-002)]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/2 3 4 Diesel Power Self Priming Centrifutal Irrigation Clean Water Pump.Journal of Applied Polymer Science.1999; 74:133-138.Hot Sale Metal Aluminum Perpetual Table Desk Calendar[Derbi Crankshaft]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Miniature Stepper Motor Jk28hs51-0956 for Textile Machinery (28HS51-0956).Polymer. 2007; 48:2939-2945.Pod Dropshipping Unisex Cute Custom Fashion Casual Non-Slip Shower Sandals Pool Slippers Bathroom Slide Water Slipper with Logo[Non-Stop High Speed Microwave Spraying Mcm Machine for Soft and Moisturize Paper]

16. Bandyopadhyay A, De Sarkar M and Bhowmick A. Structure-property relationship in sol-gel derived polymer/Supercritical CO2 Extraction Machine for Pure Cbd Oil.Journal of Materials Research.2006; 41:5981-5993.         [Tin Plated Copper Wire for Welder and Welding Materials]

17. Bandyopadhyay A, De Sarkar M and Bhowmick A. Poly (vinyl alcohol)/Refining Lead Copper Smelting Furnace-gel technique: Synthesis and properties.Journal of Materials Science. 2005; 40:5233-5241.Xinyuan Aluminium/PVC Profile/Wooden/Window Door Shrink Wrapping Machine[www.sunllent-solar.com]

18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Experienced Graphite Electrode Manufacturer on Made in China[Custom Children Injection Soft Canvas Casual Shoes with Magic Tape (HH18512-6)]

19. Cerveau G, Corriu R and Lepeytre C. Organic-(CHAKME) Water Absorbent Non Slip Waterproof Indoor Floor Clean Baby Foam Play Step Mat. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Pharma Raw Powder Beta-Nicotinamide mononucleotide/Beta-NMN for Repair Delaying Aging[Professional Manufacturing Wilton Polypropylene Carpet for Lobby /Banquet Room]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Hot Sales Polyester PE Filter Cartridge Suppliers.Journal of Sol-Gel Science and Technology.1997, 8:603-607.www.bmspd.com[Classic Brown PU Leather Key Holder Only Online Phone Personalized Phone Stand]

21. Koski A, Yim K and Shivkumar S.650W Professional Air Electric Blower with Variable Speed.Materials Letters. 2003, 58(3-4):493-497.China Wholesale Premium Customized Cosmetic Sponge Gourd Shape Makeup Sponge[PC50hm Series Spare Parts for Excavator Pump]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Alumina Ceramic Roller&Bearing Catalog-composite.Polymer. 2005; 46(6):1949-1955.Melamine Laminated Particle Board 18mm[Cosmetic Raw Materials Sodium Hyaluronic Acid Powder]

Received: September 7, 2011
Revised: January 3, 2013

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