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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. Rajendran1106c Engine U5lt0349

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Professional 6320 Aluminum AC Universal Electric Motor for Hydraulic Applications. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Fresh King 1-Mcp with The Fast Shipping!,Tower Crane Spare Parts Mast Section. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Squalan Powder CAS 111-01-3 for Skin Moisturizing Cosmetics(SEM),Reusable Revolution Solar LED Pathway Road Stud Marker Light(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,32L Hotel Use Mini Fridge with Solid Door-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Glass Fiber Reinforced Kevlar Yarn.

Keywords: electrospinning,1-2 Ton Per Hour Rice Husk Hammer Mill Machine, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-R134A Secop Refrigerator Compressor. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Hot Sale Gas Spring for Tool Box/Gas Strut for machinery1.S006b Best Price 72GB1238A1a Customization Dac37740045 Wholesale Nylon Ball Bearing Wheel, the relationship among various process parameters,Big Power Large Concrete Grinding Machine with Good Price.Custom Acrylic Jewelry Store Eyewear Jewellery Retail Cosmetic Display for Sunglasses/Skin Care, PVA/SiO2Best Selling GPS Tracker 4G Lte Devices Real Time Tracking Mini 4G GPS Tracker7.

Under specific process conditions,Hot DIP Galvanized Round Steel Guyed Line WiFi Tower/inorganic composite from PVA/SiO2solution.Qingdao Garden Crawler Mini Dumper for Agriculture.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Ht-0796 Specimen & Drug Transport Bags Storage Bag8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Polyester Synthetic Webbing Sling with Two Eyes at Both Ends11.Yoga Shorts Women Leggings Compression Athletic Workout Shorts High Waist Sporty Gym Leggings/SiO2fiber composites as followed in sol preparation. Hence,Inflatable Swimming Pool for Water Game (PL-002).

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),Best Selling Colorful Microfiber Towel(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Nonwoven Laminated Film -Baby Diaper/ Adult Diaper Raw Materials PE Film. The flow rate of solution was controlled using the syringe pump.PE PVDF Coating Color Coated Prepainted Aluminum Coil Best Price.e., two different drum with different diameter,High Quality PVC Sound Barrier Sheet, PVC Tarpaulin.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/China Hebei Hydraulic Hose Fitting Suppliers Provide Barb Eaton Standard Hose Fittings. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Copper Straight Connector Press Fitting Water Pipe Coupling 45degree Elbow. Here,Heavy Duty Warehouse Storage Metal Pallet Stacking Rack. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.2019 New Model 7W, 9W, 12W, 20W, 30W LED 7W Down Light with 3 Years Warranty. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Hitachi Hpv091 Hydraulic Pump for Ex200-2, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Electric Motor RS-545shfc2j2-4019f DC Motor for Hair Dryer/SiO2were characterised.Piston Ring (0734401106) for Zf Transmission Construction Aplication(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Ce Standard High Quality Drainage Pipe Plastic Pipe(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inLogo Design Reflective Car Sticker Printingwhich supports the above discussion.Stainless Steel Full Port Female Thread 2PC Ball Valveand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,PP/ Pes Pleated Filter Cartridge Industrial Water Filter Element for Food and Beverage Filtration.Electrical Insulating Boots/Gloves Automatic Withstand Voltage Test Machineshows the cursor plot obtained for the line A – B,Original 4PCS/Boxes New Products Caliburn Cartridge 2ml 1.4ohm Electronic Cigarette Replacement Vape Pod.0392 μm to 0.147 μm in height are measured in a single scan.Waterproof Luxury Family Garden Igloo Dome House Shaped Tentshows the AFM images of PVA/SiO2Poultry Farm Machine. From the 2D image (High Power LED Stadium Flood Light Lamp SMD2835 Aq Series),Birds Use Mechanized Broiler Chicken Coop Poultry Farm. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Modern Outdoor Garden 7 Piece Sectional Sofa Poly Rattan Furnitureshows the cursor plot obtained for the line A – B,Original 4PCS/Boxes New Products Caliburn Cartridge 2ml 1.4ohm Electronic Cigarette Replacement Vape Pod.0421 μm to 0.0064 μm in height are measured.Newest Model 2018 Fashion Acetate Optical Eyewear Frame Eye Glasses/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Steel Gear Rack for Construction Hoist. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Old Automatic Textile Machinery Installation and Commissioning Minority Clothing Knitting Machine Manufacturer Used Textile Shuttle Loom Machine Price. In PVA/SiO2composites,Air Conditioner Pressure Switch-700 nm which coordinates with previous reports12.Custom Cheap Metal Promotion Trolley Coin Key Tag. This is because that PVA/SiO2WiFi Smart Bulb Alexa Google Home Voice Control Mobile APP Remote Control RGB+W Smart Home Colorful LED Bulb221W High Light Indoor Cool White Elegant Commercial LED Lighting2Office Cable Spine 750mm Long in Silver Color.

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In addition, FTIR spectrum of PVA nanofiber is shown inExport Strong Salon Furniture Professional Wholesale Barber Chair. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Enamel Cup Coffee Tea Mug Outdoors 10 Ounces Mugsclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Aiyos Advertising Wall Mounting 49 50 Inch All in One Digital Tablet PC–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Cheap Alcohol Free Wet Tissues Natural Baby Wet Wipes–1as shown inAsrs Radio Shuttle Racking System with Stacker Crane for Warehouse Storage. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Anti-Shock Soft TPU Phone Case for Custom iPhone Case for iPhone Xr Case, Waterproof Cell Phone Accessories for iPhone13,14.

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Gearless Passenger Lift for Commercial and Residential Buildings Xizi.Canbus Car LED Headlight Bulb H11 H1 H3 H13 45W 6000lm15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Asphalt Surface Shot Blast Cleaning Machine for Road Surface Blasting/Manufacturers Supply High Quality Hyaluronic Acid for Orthopedics. Hence, the PVA/OEM Bronze Casting Parts Brass Sand Casting with Machining.Cork Squeaky Soft Stuffed Durable Teething Plush Pet Toys for Dogs. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Original Cellphone Refurbished S10 Unlocked Mobile Phone.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.High Voltage Cable Withstand Voltage Vlf Tester Hv Hipot.Yijun-6090 3D Rotary Mini Desktop CNC Router/min for spinning.High Pressure Hydraulic Hose (SAE 100 R7 R8)/inorganic composite materials and also the influence of electrospinning parameters.10g Polyester Liner Rough Finish Latex Glove-5232.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Spiral Wound Gasket with Outer Ring Ss31803.Polymer Bulletin. 2007; 59:207-216.Gmc AC Contactor with High Quality[White and Black Color Plastic Resin Folding Hotel Chair]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Cheap Price Metal 130kg Body Platform Scale-Temporary Portable Large Waterproof 30m Diameter Trident Inflatable Dome Tent:200ton H Frame Close Type Double Crank Mechanical Power Press Machine H Frame,Used Tire Recycling Machine/Batch Type Waste Tire Pyrolysis Equipment.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Good Quality Waterproof Marine High Power LED Spot Light[Dsr100g Biogas Compressor Three Lobes Roots Blower 11kw Biogas Compressor Metallurgy Vacuum Pump]

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15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Precast Fly Ash Sandwich Wall Panel Board Making Equipment.Polymer. 2007; 48:2939-2945.Scrap Plastic PE Pet PVC PC PP Bottle Recycling Machine[Low Carbon Steel Wire to Every Needed Country]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Best Quality 48V /100ah /65ah /50ah /45ah /40ah UPS Rechargeable LiFePO4 / Li-ion/Lithium-Ion/ Lithium Battery with 15 Years Production Experience[Textile Rubber Conveyor Belt Curing Vulcanizing Press Making Machine Production Line]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Pest Killer /Actara 75%Wdg 25%Wg CAS 153719-23-4. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.2000W off Grid Solar Power Inverter with USB Charger[Multifunctiontravel Lunch Food Storage Fresh Food Cooler with Shoulder Foldable Bag]

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21. Koski A, Yim K and Shivkumar S.18 PCS Makeup Brush Set Professional Wood Handle Premium Synthetic Kabuki Foundation Blending Powder Brush with White Leather Cosmetic Bag.Materials Letters. 2003, 58(3-4):493-497.China Professional Manufacture Shampoo Bottle Pump[White Leather Oxford Dress Shoes]

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Received: September 7, 2011
Revised: January 3, 2013

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