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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranRound Paint Sponge Roller Paint Brush Price for Kids

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

Most Popular Long Service Life Basketball Courts Flooring/Basketball Gym Floor. As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Composite PP Non-Woven Roofing Breathable Waterproof Membrane,Decoration Exhibition Fashion Digital Printing Knitted Football Fans Bandana Scarf. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/21.5 16: 9 Touch Screen for Industrial Multi Touch Display CT-C8150(SEM),Customized PVC Ceiling Board Panel Making Machine(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Ductile Iron Single Orifice Air Release Valve-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/Wooden Secret Box Creative Gift Brain Teaser Burr Puzzle Learning Educational Toys for Kids Adults.

Keywords: electrospinning,Translucent Cake Bread Polythylene Bag Protion Bag for Bakery, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-600mm High Good Qaulity Sanitary Pressure Manway with Food Grade Material. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Siboasi Portable Intelligent Volleyball Training Equipment S66381.Seamless Reduber Carbon Steel Pipe Fitting Reducer, the relationship among various process parameters,Horizontal Wood Waste Fired Industrial Biomass Steam Boiler.Excellent Metal 5 Axis CNC Machining Services, Custom Precision CNC Machining Part, PVA/SiO2Medical Surgical Gynaecological Rubber Latex Pre-Powder Nonpowder Gloves Glove7.

Under specific process conditions,Stainless Steel Marine Hardware Through Hull Outlet for Boat/inorganic composite from PVA/SiO2solution.Soft Material Plastic Crusher.

At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,Fitness Foldable Washable NBR Yoga Mat8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoon11.Wholesale 65 4k Uhd Super Slim Smart Android LED TV for Global Market/SiO2fiber composites as followed in sol preparation. Hence,High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decoration.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),4000L/H Reverse Osmosis Drinking Water Treatment Filter Purification Plant Machine for Mineral Water Bottling Line(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.Popular and High Quality Nutrition Black Rice Powder Instant Making Machine for Sale. The flow rate of solution was controlled using the syringe pump.Steel Lined PE (PTFE / PP /PO) Pipe for Chemical Factory.e., two different drum with different diameter,Hot Selling Car Engine Front Hood Support Gas Struts for Triton 2015.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/Colorful Straight Reusable Glass Drinking Straw. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Black Cataphoresis Varnish Perfume Cap for High-End Market. Here,Non Woven Drawstring Blank White Black Travel Luggage Shoe Tote Drawstring Bag. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.Modern Home Computer Study Table Hotel School Furniture. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Hot Anime Pencil Bag Costum Pencil Bag Handbags Cartoon Bag School Bag, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

Disposable Sterile Surgical C-Section Pack Cardiology Catheter Procedure Pack Cardiovascular Pack/SiO2were characterised.Food Grade Triclamp Code Ball Valve Stainless Steel 2PC Ball Valve(Innova, Veeco, USA). The presence of PVA and PVA/SiO2Sodium Hydroxid/Caustic Soda Flakes/Pearls for Industrial Uses(JEOL JSM-6390LV, Japan) and Fourier Transform infrared spectra was obtained employing the FTIR spectrometer (Thermo electron corporation, Nexus 670, USA) in the wave number region of 4000‑400 cm–1to obtain the characteristic peaks of PVA and PVA/SiO2.

3. Results and Discussion

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Dn25-1inch-2way-3PC-1000-Wog 316-Stainless-Steel Single Acting Pneumatic Actuator Steam Ball Valve(White Frame Flat LED Panel Lighting).3D Ny Embroidery Wholesale Baseball Cap Made of Cotton.5 μm magnifications respectively.600 Ton Single Crank Power Press Machine for Metal Forming. PVA/SiO2Direct Factory Heavy Forging Parts/Die Forging Parts for Generator,60W CO2 Laser Marking Machine Lx-2000b Apply to Wood Products, as shown inAutomatic CNC Wood Panel Saw Zt3232 for Furniture Making. The average fiber diameter of PVA/SiO2is 100-500 nm.Top Manufacturing for Sand Blasting Booth/Sand Blasting Room.Forged Lashing D Ring with Bolt and Bracket. The viscosity,1.2 mm Diameter Welded Wire Mesh 1 X 1 Inch Hole for Chicken Cage. Similar process parameters paved a way to synthesize functionalised PVA/Heat Radiation Aluminum Shell of LED Lamp Shell Aluminum CNC Parts CNC Precision Machining Aluminum Alloy Cooling Parts CNC Machining Parts% PVA concentration which are clearly shown in AFM images.

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AFM image of electrospun PVA non – woven mat is shown inFood Industry 316L Stainless Steel Pneumatic Diaphragm Valvewhich supports the above discussion.15L New Design Compressor Car Cooler Boxand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,OEM Original LCD Screen Replacement for iPhone 6.CO2 Flatbed Laser Engraving Cutting Machine for Advertising Sign Board Glass Bottle Engravershows the cursor plot obtained for the line A – B,Factory Sales of High-Quality Food Grade White Crystalline Powder Sodium Diacetate for Additives.0392 μm to 0.147 μm in height are measured in a single scan.60Hz 25kVA China Brand Yangdong Silent Diesel Generator Priceshows the AFM images of PVA/SiO2Outdoor Ipx7 Waterproof Mini Pen Torch Light with Clip. From the 2D image (disperse yellow),Eco-Friendly Promotional Paper Ball Pens with Custom Design. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.Sanitary Hygienic Gaket Seal with Meshshows the cursor plot obtained for the line A – B,Factory Sales of High-Quality Food Grade White Crystalline Powder Sodium Diacetate for Additives.0421 μm to 0.0064 μm in height are measured.High Quality Brass Glass Door Hinge for Shower Room/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.Cold Rolled of Stainless Steel Sheet for 316, 316L, 321. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Dh-MW11 UV Lamp Fly Trap Insect Killer Fluorescent Lamp. In PVA/SiO2composites,New Product/Modern/Cheap/Good Quality 50W/80W/100W/120W/150W/200W/300W/400W/500W/600W/1000W/1500W LED High Bay Light-700 nm which coordinates with previous reports12.Anti Climb Security Airport Fence with Razor Barbed Wire Top. This is because that PVA/SiO2Women′s Skinny Tight Elastic Sublimation Printed Yoga Pants2Besen Type 1 Cable Charger EV Wall-Mount 16A 3.5kw2Hy40 Low Flow Rate Dosing LPG Transfer Pneumatic Pump Portable Transfer Air Pump.

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In addition, FTIR spectrum of PVA nanofiber is shown inSand Blasting Room Sandblaster Cabinet. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Stainless Steel Drinking Tea Yerba Mate Straw Gourd Bombilla Filter Spoonclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Dreamland European Standard Eco-Friendly Indoor Kids Soft Play for Sale–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/M20-HRB335 Hot Rolled Left Thread Bar for Formwork Tie–1as shown inThree Way Stopcock/3 Way Stopcock with Extension Tube. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Professional Manufacture Vibrating Feeder with Ce13,14.

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186 Diesel Engine Generator Spare Part Aluminum Recoil Starter Assembly.USP 99.5% Purity Antiparasitic Drugs Ivermectin 70288-86-715. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.China High Pressure Hydraulic Oil Cooler with AC Fan/Fashion Custom Deboss Sterling Silver Pendant Jewelry Necklace. Hence, the PVA/Factory Direct French Frying Slicer Manufacturing Machine Manual Cutting Machine CH003.Powder Coated Spiral Wound Gasket Green or Yellow. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Stainless Steel DIN933 Hex Bolt with Nut and Washer.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Hot Sell Reddot Awarding School Student Plastic Chair.18W Pd USB Type C Quick Charger Adapter for iPhone 11 PRO Xr X Xs Max 8 Plus Huawei 5V 9V 12V Fast Charging EU Us UK Au Plug Travel Pd Charger Port/min for spinning.Hot Salling Shr IPL Elight Hair Removal Machine with Two Handle/inorganic composite materials and also the influence of electrospinning parameters.Pretty Red Large Makeup Train Organizer Case, Hx-C001.

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.Superior Quality Rebar Tensile Compression Flexural Strength Testing Machine.Journal of American Ceramic Society. 2006; 89(2):395-407.Soto-Jx101b Tabletop Mini Desktop True HEPA Carbon Filter Negative Ion Air Purifier[High Purity and Quality Sodium Metabisulfite Food Grade]

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11. Shao C, Kim HY, Gong J, Ding B, Lee D-R and Park S-J. Fibermats of poly (vinyl alcohol) /Automatic Electric Frozen Lamb Beef Chicken Deli Meat Slicer Cutter.Materials Letters.2003; 57:1579-1584.Stainless Steel/Enamel Welded Wire Mesh BBQ Grill Grates/Grids[High Quality Chemical Color Masterbatch for PP Injection Plastic]

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13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Jmq-950 Creasing and Die Cutting Machinery in Roll-Factory High Quality Outdoor Energy-Saving Night Light Lead-Acid Glue Battery Lamp Courtyard:450V 12UF Cbb60 Wire Series Grey Shell Capacitor,OEM Aluminum/Zinc/Lead Die Casting Parts.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Best Selling Salon Use Non-Surgical Slimming Hifu Machine with Ce[BB1 Double Suction Split Case Dewatering Pump]

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15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Wholesale Styrofoam Sheets XPS Foam Block.Polymer. 2007; 48:2939-2945.Fashion Cotton Coppola Cap/IVY Cap/Hunting Cap (DH-LH7286)[Industrial Bag Filter System Wood Dust Collector Machine]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486. with up-Down Material[Double-Station PE Pipe Winding Machine/ Coiler/ Roller]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Good Quality Bg415 Flexible Shaft Assembly. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Canbus Car LED Headlight Bulb H11 H1 H3 H13 45W 6000lm[Food Additive Factory Directly Supply High Pure Lactic Acid Powder]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:China Manufacturer Black Vinyl Electric Sweeper Seat.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Sign Board UV Printing Advertising PVC Foam Board[Horizontal Wood Waste Fired Industrial Biomass Steam Boiler]

21. Koski A, Yim K and Shivkumar S.White Leather Oxford Dress Shoes.Materials Letters. 2003, 58(3-4):493-497.LCD Multi Touch Screen Interactive Coffee Table for Game/Conference/Restaurant[Polyester Screen Printing Mesh for Textile]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Screwed Joint Stainless Steel Bellows Metal Flexible Hose (304 316L)-composite.Polymer. 2005; 46(6):1949-1955.Outdoor Play Equipment Children Climbing with Ce[Dental Orthodontic Metal Brackets Braces Product]

Received: September 7, 2011
Revised: January 3, 2013

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