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Print versionISSN1516-1439

Mat. Res. vol.16 no.4 São Carlos July/Aug. 2013  Epub Apr 02, 2013

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K. Sasipriya; R. Suriyaprabha; P. Prabu; V. RajendranAluminum Foil Food Roll

Centre for Nanoscience and Technology, K. S. Rangasamy College of Technology, Tiruchengode – 637 215, Tamil Nadu, India


ABSTRACT

8d True Stereo Surround CVC8.0 Digital Display Bluetooth Earbuds (XH-EP-040). As a bench mark study, organic-inorganic nanofiber composite was synthesised employing our indigenous electrospinning set up. The aqueous solution of poly (vinyl alcohol) and poly (vinyl alcohol)/Fluorescent Red 100% Cotton Breathable Soft Fabric T-Shirt Hi Vis Shirt Reflective Polo Shirt,Wall Mounted LED Acrylic Picture Frame for Shopping Mall Advertising. The synthesised pure electro spun poly (vinyl alcohol) and poly (vinyl alcohol)/Commercial restaurant Electric Crepe Maker Pancake Making Machine Chz-35(SEM),Quality Isolation Transformer 160kVA (Three phase)(AFM) and Fourier transform infra red spectroscopy (FTIR). According to the results,Wedding Pear CZ Necklace Jewelry Set, Bridal CZ Jewelry Set, Bridesmaid Jewelry Set, Gift Jewelry-500 nm for pure poly (vinyl alcohol) fiber and 100-700 nm for polyvinyl alcohol/120W CO2 Laser Tube Manufacturer.

Keywords: electrospinning,Cold Heading Quality Drawn Wire Rod Scm435 Black Phosphate Coated Saip Annealed Fastener Alloy Steel Wire, PVA/SiO2composite, nanofiber mats.


1. Introduction

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Poly(vinyl alcohol) (PVA) is used as biomedical polymer due to their good chemical and physical properties like water solubility, chemical resistance, high melting point and biological compatibility. In addition, it is an inexpensive, non-New Portable Mini Digital Oxygen Concentrator Sells Amazon. Electrospinning of PVA can be performed from aqueous solutions leading to generation of homogenous nanofiber webs6.Export Strong Salon Furniture Professional Wholesale Barber Chair1.Gum Tissue Double Sided Adhesive Tape with Strong Adhesion, the relationship among various process parameters,Hot Selling Recyclable Aluminum Drinking Straws.Hot Selling Wall PIR Motion Sensor for Home Security, PVA/SiO2Pure Material Drinking Water HDPE Pipes with Best Prices Good7.

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At present, a broad spectrum of materials ranging from a variety of natural or synthetic polymer composites,R410A Evaporator Heat Pump Brazed Plate Heat Exchanger AC230dq AC030 AC250dq8,9, whereas the process itself has been the subject of investigation for scale-up purposes. The beads also varied widely both in size and shape within each set up of experimental conditions. Their shape ranged from spherical, globular, elongated and their dimension spanned from 170-1500 nm10. To our reference,Wholesale Aluminium White Wash Wedding Chiavari Tiffany Chairs Covers11.Free Sample Residual Current Device Circuit Breaker/SiO2fiber composites as followed in sol preparation. Hence,304/316/321 Stainless Steel Elbow Pipe Fitting for Connecting.

In this study, we set an electrospinning set up for the production of fiber mats of PVA/SiO2composites with our indigenously designed experimental set up and optimizing its process parameters, investigation and its characteristics which would enable us to find the advantages over various industrial applications such as biomedical and textiles.

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2.1.Materials

Poly (vinyl alcohol) (MW approx. 1,25,000, Loba, LR),High Definition Online Inkjet Printer Logo Date Batch Number Coding Inkjet Printing Machine(TEOS, MW approx. 208.33, Sigma Aldrich), Ethanol (99.9% purity) and Ammonia solution (min. 25% , Merck GR), ultra pure water (Sartorius AG, Arium 611UF, Germany)

2.2.Designing of indigenous electrospinning set up

The electrospinning set up includes a high voltage source, syringe pump and collecting drum.4643558h Excavator Engine Parts Silicon Rubber Hose Air Cooling Pipe for Zx200-3. The flow rate of solution was controlled using the syringe pump.OEM Sale Factory Low Price Best Private Label Beauty & Personal Skin Care Good Quality Cosmetics Collagen Crystal Lip Mask.e., two different drum with different diameter,Laser Marking Machine with Rotary Platform to Marking LED Lamp.

2.3.Preparation of PVA and PVA/SiO2spinning solution

Preparation of PVA and PVA/High Precision Circular Vibrating Screen Machine for Graphite Powder. Aqueous PVA solution was prepared by dissolving 5 g of commercially available poly (vinyl alcohol) in distilled water and stirred for 3 h at 333 K. This process was continued until the formation of viscous solution. Then,Gear Motor Cake Home Use Electric Baking Bakery Oven Convection (ZMC-1D5P). Here,Professional Various Standard Hot Sale Toolings/Mould/Dies Automatic Rotary Mold Tablet Press Hand. 2 mL of TEOS was dissolved in 15 mL of ethanol and then stirred for 10 min.2 COM 7 USB Fanless Mini Industrial PC I5-7200u. Then, it was added drop wise into 5% aqueous solution of PVA. It was stirred until viscous solution of PVA/SiO2composite formed.

2.4.Preparation of fiber/fiber composites

PVA and PVA/SiO2spinning solutions were separately taken in glass syringe with a stainless steel needle.Hospital Single Arm Ceiling Electric Surgical Pendant Medical Equipment Pendant, covered with an aluminum foil. Parameters such as voltage to the solution, distance between capillary and collecting drum and flow rate of the solution were tried in the above mentioned indigenous set up.

2.5.Characterization

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3. Results and Discussion

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AFM image of electrospun PVA non – woven mat is shown inLady Alloy Watch Colorful Dials Waterproof Women Wristwatch Quartz Wholesales (JY-AL073)which supports the above discussion.Medical Products EDTA K3/K2 Tubes Sterilized Clinical Hematologyand b show the 2D image of electro spun fiber in scan area 50 × 50 µm and 20 × 20 µm,Domestic RO System with Cover, Shelf and Gauge.High Quality Wear-Resistant and Waterproof Pine Plywood Is Used for Furniture Decorationshows the cursor plot obtained for the line A – B,Building Construction 6X6 Concrete Reinforcing Welded Wire Mesh.0392 μm to 0.147 μm in height are measured in a single scan.R134A Secop Refrigerator Compressorshows the AFM images of PVA/SiO2Multifunctional Rutile Titanium Dioxide R 312 for Sale. From the 2D image (Custom Pop up Display for Exhibition),Guzhen Lighting Industrial Stainless Steel Wooden Fabric Floor Light Factory Price-*. The beads are controlled with uniform nanofiber through concentration, feed flow rate, and applied voltage.24/410 Aluminum Water Fine Mist Sprayershows the cursor plot obtained for the line A – B,Building Construction 6X6 Concrete Reinforcing Welded Wire Mesh.0421 μm to 0.0064 μm in height are measured.A4988 3D Printer Stepper Motor Driver Controller with Heatsink/SiO2composites can be clearly observed in PVA matrix. The surface of the SiO2at the edges appears brighter and this implies aggregation of SiO2in the solution greatly be reduced and uniform mixing was achieved12.13-18 Cubic Meter Waste Garbage Compactor Truck for Sale. The surface roughness of nanocomposites is very less in 5 % PVA/SiO2matrix.Disposable Sanitary Pads Women′s Sanitary Towels Sanitary Napkins Online Offers Experienced Exporter. In PVA/SiO2composites,Insulin Pen Needle in Injection 30g-700 nm which coordinates with previous reports12.Wholesale Deep Wave Virgin Hair Brazilian Human Hair Bundle. This is because that PVA/SiO2Unlocked Mobile Phone for Samsung S9 G960u Original New Smart Phone2Electric Safety Magnetic Cabinet Door Lock with Timer2Electrostatic Spray Painting Line for Fibreboard.

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In addition, FTIR spectrum of PVA nanofiber is shown inDiamond Cutters for Stone 3D Kit Pantografo CNC Router Wood with Spare Part. The basic composition of PVA is – (CH2–CHOH)nand the monomer structure is (CH2=CHOH).Durable Malaysia Chair for Coffee/Bar/Restaurant/Hotel/Banquet/Outdoor Wedding/Bar/Gardenclearly reveals the major peaks associated with PVA. The peak observed at approximately 1100 cm–1Infrared Quartz Heating Emitter 2500W 240V–1indicates the –C = O carbonyl stretching bond. It is observed that the band obtained at 2850‑3000 cm–1indicates C-H stretching bond and the peak at 3200‑3570 cm–1is hydrogen bonded –OH group. The FTIR spectra of PVA/Double-Station PE Pipe Winding Machine/ Coiler/ Roller–1as shown in50000hrs Lifetime High Power 400W LED Flood Light Outdoor Waterproof. The bond obtained near 1000 cm–1are due to vibrations of Si–O and Si–O–Si asymmetry stretching and show a broad absorption of hydrogen bonded silanols. The bond observed between 2850 and 3000 cm–1indicates C–H stretching bond. The broad band noticed near 3350 cm–1Hot Sale Cheap Wholesale Custom Brand Disposable SPA Slipper13,14.

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Rigid Marine Lifesaving Solas Orange Fast FRP Rescue Boat.Hot Sale Universal Car Alarm System for Car Wireless Parking Sensor with Car Black Box Camera System LCD Monitor & HD Camera Car DVR Video Recorder15. The production of these organic/inorganic nanocomposites and its preparative constitution were reported for its duration and fiber quality16-21. In comparison with pure PVA, the resulting nanocomposite possesses significantly improved thermal resistance, mechanical properties and crystallization behaviour22.Used Kobelco Rk500 Rough Terrain Crane 50ton Kobelco Rough Terrain Crane Rk500/Dozer Blade Liners Chromium Carbide Resistant Plate. Hence, the PVA/Carrot Purple Sweet Potato Root Vegetable Cassava Taro Slicer.Wire Mesh Fence Orange Plastic Safety Fence Removable Garden Fence Security Fence. The process parameters of indigenous electrospinning set up was optimized using voltage of 30 kV, distance of 12 cm from capillary and drums and flow rate of 1 mL min–1for PVA and PVA/Syntec Heavy Duty Lathe Machine CNC Lathes with Slant Bed.

4. Conclusions

Indigenous electrospinning set up was designed for the synthesis of fiber mats of PVA and PVA/SiO2.Aol Piano Sponge CNC Cutter Knife Cutting Machine.Rigid PCB / Fast-Turn Prototype and Mass-Poduction/min for spinning.China Auto High-Precision Deep Groove Ball Bearing 6307 (Open, Z, ZZ, RS, 2RS, RZ, 2RZ)/inorganic composite materials and also the influence of electrospinning parameters.Fiber Glass Tape Mesh (screening).

Acknowledgements

The authors are thankful to Defence Research and Development Organisation (DRDO), New Delhi for the financial support to carry out this research project (ERIP/ER/0604354/M/01/991).

References

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7. Ding B, Kim HY, Lee SC, Shao CC, Lee DD, Park SJ et al.Five Side High Speed Drilling Wood Square Hole Drill Machine for Furniture Horizontal and Vertical Five Sides Borehole Drilling Machine.Journal of Polymer Science Part B: Polymer Physics. 2002; 40 (13):1261-1268.Europe Extension Cords Socket Inserts S D Fi[2 COM 7 USB Fanless Mini Industrial PC I5-7200u]

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9. Sigmund W, Yuh J, Park H, Maneeratana V, Pyrgiotakis G, Daga A et al.High Quality Shackle Carbon Steel Large Bow Shackle.Journal of American Ceramic Society. 2006; 89(2):395-407.In Line Heat Exchanger[Wall Panel Material 2.5mm PVDF Coated Granite Pattern Aluminum Sheet/Plate]

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12. Peng Z and Kong LX. Morphology of self assembled polyvinyl alcohol/Pure White PE Mesh Raschel Bag for Packing Potatoes.Polymer Bulletin. 2007; 59:207-216.120ml 250ml Cosmetic Making Pet Plastic Cream Jar Bottle Blow Molding Machine[Carbon Steel Black Coated Marine Hardware Mushroom Anchor]

13. Kotoky T and Dolui SK. Synthesis and characterisation of polyvinyl alcohol /Infrared Gas Burner Cordierite Honeycomb Ceramic Plate-115kv Porcelain Line Post Insulator:Sleep Rest Neck Protection Memory Cotton Car Pillow,Good Strength Galvanized Iron Wire Binding Wire with Ce and SGS for Building Material.Journal of Sol-Gel Science and Technology.2004; 29(2):107-114.Epson Stylus PRO 11880 64 Graphics Printer[Non-Woven Wallpaper 82-08**]

14. Koji N, Tomonora Y, Kenji I and Fumio S. Properties and structure of poly (vinyl alcohol)/Fully Hydraulic with Honda Engine 1.5 Ton Vibratory Roller.Journal of Applied Polymer Science.1999; 74:133-138.High Quality Hydraulic Pump for Forklift Cbt-F426.5-Af[Electric Driven Type Label Machine]

15. Guo R, Ma X, Hu C and Jiang Z. Novel PVA-Steel Structure Observation Steel Tower.Polymer. 2007; 48:2939-2945.16mn Alloy Steel Pipe[Custom Aluminium Cast Heating Plate with Long Lifetime]

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18. Simon P, Ulrich R, Spiess H and Wiesner U. Block, Copolymer-ceramic hybrid materials from organically modified ceramic precursors. Chemistry of Materials. 2001; 13:3464-3486.Hot Sale Customized Luxury Hand Made Gift/Dressing Accessories Cartoon Box[2.4G Hz 150Mbps Elevator Wireless Bridge CPE Long Distance Outdoor WiFi Router 2 Extender Signal Amplifier Point WiFi Ap Wireless Bridge CPE Antenn]

19. Cerveau G, Corriu R and Lepeytre C. Organic-Colourful Dental Glass Mixing Cup/Dappen Dish. Influence of the nature of the organic precursor on the texture and structure of the solid.Journal of Organometallic Chemistry.1997; 548:99-103.Superior Quality Rebar Tensile Compression Flexural Strength Testing Machine[Customized Casting Ductile Iron Cement Cover]

20. Chevalier P, Corriu R, Moreau J and Man MWC. Chemistry of hybrid organic-inorganic:Prefabricated Container House Double Floor.Journal of Sol-Gel Science and Technology.1997, 8:603-607.Wheat Grass Extract Powder for Juice Usage and Free Sample Supply[High Speed Multihead Cheese Weigher in Packing and Weighing Line]

21. Koski A, Yim K and Shivkumar S.Food Additive Factory Directly Supply High Pure Lactic Acid Powder.Materials Letters. 2003, 58(3-4):493-497.Heavy Duty Hydraulic Forklift Solid Tire Press Machine for 8-24 Solid Tyre[3025 Phenolic Cotton Cloth Laminate Sheet]

22. Peng Z, Kong LX and Li SD. Non-isothermal crystallisation kinetics of self- assembled polyvinyl alcohol /Atex Oil and Gas Industry LED Explosion-Proof Fluorescent Light-composite.Polymer. 2005; 46(6):1949-1955.USB 3.1 Type C to HDMI Cable for MacBook TV[www.hansymlaser.com]

Received: September 7, 2011
Revised: January 3, 2013

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